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2、 - , - 325342013 1 Diphenylol propane. Determination in air 20140801 1 ) 25 3 25 3 - ( ) . 2 : 12.1.00588 . 177074 . , , , - . 222295 . 670972 . 1067876 . 2916991 ( 64877) . 2922791 ( 835-181) . . 1. - , 1 , - . ( ), - ( ) . , , , , . 3 ( 2 = k ) % 15 U = . 15 % 95 , 0 = P . 4 4.1 , - . 325342013 2
3、4.2 : . . , . 4.3 , , . - . 4.4 . - , . 5 , 5.1 ( , Pye Unicam 100A Rheodyne 7125 c 20- , Pye Unicam LC-XP - ) ( , Metrohm 656 - Metrohm 641, 1,2 Ag/AgCl). 150 4,6 ( , Spherisorb ODS- 2, 150 4,6 , 5 , Phase Sep., UK.). 53228. 20 100 . ( ) 2 29169 0,02 . 5 29227 0,03 . 2 10 2 500 1770 0,1, 5,0 - . 50 500 1770 0,12 0,5 - , . . 5.2 , 98 % ( , Fluka, Buchs, Switzerland). , 6709. 2222. 99 % ( , .). 85 % 10678. , - , . 5.3 2 3 ( , SKC Model 224-17). 13 ( , Millipore, Type AE) - ( , Millipore), . pH- ( , HANNA Instruments pH-210), - pH- .