GOST 32835-2014 Juice products Determination of mycotoxins by tandem high performance liquid mass spectrometry (HPLC-MS MS)《果汁产品 采用串联高效液相质谱分析 (HPLC-MS MS) 测定霉菌毒素》.pdf

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GOST 32835-2014 Juice products Determination of mycotoxins by tandem high performance liquid mass spectrometry (HPLC-MS MS)《果汁产品 采用串联高效液相质谱分析 (HPLC-MS MS) 测定霉菌毒素》.pdf_第1页
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GOST 32835-2014 Juice products Determination of mycotoxins by tandem high performance liquid mass spectrometry (HPLC-MS MS)《果汁产品 采用串联高效液相质谱分析 (HPLC-MS MS) 测定霉菌毒素》.pdf_第5页
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1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32835 2014 - (-/) 2015 328352014 II , - 1.092 . 1.22009 . -, . , , , 1 - ( ) 2 3 , (- 25 2014 . 45-2014) : ( 3166) 004 97 ( 3166) 004 97 AM BY KG RU 4 19 2014 . 896- 328352014 1 2016 . 5 : - CODEX STAN 247 2005 Codex Gen

2、eral Standard For Fruit Juices And Nectars of the Codex Ali-mentarius Commission ( - ); - Regulation of the Commission of the European Union of 23.02.2006 . No. 406/2006/ Laying down the sampling methods and methods of analysis for the official control of the levels of mycotoxins in foodstuffs ( 23.

3、02.2006 . 406/2006/ ); - AIJN Code of Practice for Evaluation of Quality and Authenticity of Fruit and Vegetable Juices of the European Fruit Juice Association ( - ). 6 - , . () - - . , , 2015 -, - 328352014 1 - (-/) Juice products. Determination of mycotoxins by tandem high performance liquid mass

4、spectrometry (HPLC-MS/MS) 2016 01 01 1 -, , - 0,1 100,0 /3 0,1 20,0 /3. - . 2 - : 12.1.00491 . . 12.1.00776 . - 12.1.01076 . . - 12.1.01979 . . - 6175 . . OIML R 76-12011 . - . 1. . 177074 ( 104283, 478880) . -, , , . ISO 36962013 . - 5725-12003 ( ) -. 1. 5725-22003 ( ) -. 2. 578978 . . 1631787 . 20

5、01588 . 2533682 . . 2631384 . , 2667185 , -. 328352014 2 2903091 . - 2922791 ( 835/181) . . 1. / 170252009 - 32689.12014 . - 1. 32689.22014 . - 2. 32689.32014 . - 3. - , 1 , - . (), - () . , , , , . 3 -/ -; ; ; ESI (Electrospray Ionization); IARC ; LOD ; LOQ ; SRM (Selected Reaction Monitoring). 4 -

6、 , , - -/ . 5 , , -, -/* - 10 3000 (. . .), 0,1 . . , , , - / 1000:1. , , , - 50 , - 5 18 150 3 . 0,1 100,0 /3. , - 250 400 , 0,1 %. * -/ . 328352014 3 OIML R 76-1, 0,01 . . 4000 5000 / 50 3. 10000 12000 / - 1,5 2,0 3. , 200 . 16317. . 20 1000 3 2,5 %. ( , 13 , 0,2 0,4 ). 1 . - 98 %. 61, . . . . . ,

7、 . . , , . . 20015, . . 5789, . . . 1 ISO 3696. 2- 1, 2, 5, 10 3 2- 29227. 2- 5, 10, 25, 50, 100 1000 3 2 2 1770. 10, 25 3. 1,5 2,0 3. 100 400 3. 2- 25, 50, 250 3 1770. 50 3 125 150 . 3 3. 25336. 50, 100, 250 3 25336. 10, 20, 50, 100 200 3 25336. , , , - , , . 6 26313. 26671, 32689.1, 32689.2 32689.3. 7 7.1 , - 32689.1, 32689.2 32689.3. 328352014 4 7.2 7.2.1 1000 3 1 3 , 100 3 . . . 7.2.2 1000 3 1 3 . . . - (). 7.2.3 1 99 . . 1 6 . 7.3 . 180 200 6 10 . , 30 40 oC 2 3 . 7.4 7.4.1 7.4.1.1 200 /3 2,0 , 0,01 , 10 3 . 0

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