1、 - (O-FID)(EN 1601:1997, IDT) , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)EN 16012012, 1.092 . 1.22009 . , - . , , -, 1 - ( ) , 42 31 3 , (- 24 2012 . 41) : ( 3166) 00497 ( 3166) 00497 AZBYKZKGMDRUTJUZ -4 EN 1601:1997 Liquidpetroleum products Unleaded petrol Determina
2、tion of organic oxygenate compounds and totalorganically bound oxygen by gas chromatography (O-FID) . -. (-FID). 16012007 . - . - - (-FID). . (en). , - , , , - . - . - . (IDT)5 19 2013 . 170- 1 2014 .6 II EN 16012012 -, - . () . , - - , 2013 -, III EN 160120121 12 13 14 .25 .26 .37 .38 .59 610 611 .
3、6 () 15 .7 () (O-FID) 12 15 () .15IV EN 16012012 - (O- FID)Liquid petroleum products. Unleaded petrol. Determination of rganic oxygenate compounds and total organicallybound oxygen content by gas chromatography method using the oxygen flame-ionization detector (O-FID) 201407011 - 0,17 % . 15 % . 3,7
4、 % . - , 220 . , . - , . , .2 . -().EN ISO 3170 Petroleum liquids Manual sampling ( . )(IS 3170:2004)EN ISO 3171 Petroleum liquids Automatic pipeline sampling ( . - ) (IS 3171:1988)3 - () , -. pea- , , - (O-FID) (O-FID) - .1 EN 16012012 4 .4.1 4.1.1 - , , . - , .4.1.2 . 4 %. 75 %. , , -.4.2 99,0 % .
5、 - : (3) ( , ); (32) ( , tO);-1- (CH3CH2CH2OH) ( , NPA);-2- (H)2 ( , IPA);-1- CH3(CH)3OH ( , NBA);-2- (H3()23)(- , SBA);2-2- (3)3 (- , );2-1- (CH3)2CHCH2OH ( , IBA);-2- 3()223(- , SAA);- (3)33(- , );- (3)2(3)23(- , TAME);- (CH3)2C(OCH2C3)CH23(- , ); (3)2; (C2CH2COCH3) (, );- (CH3)3COCH2,CH3(- , ).4.
6、3 , 4.2. , , -, .4.4 , , , .5 , :5.1 5.1.1 - .5.1.2 , . , -.2 EN 16012012 , 1. R ( 1) R = 1,18c162 c45 c162c45ttWWBAAB,(1) c162tB ;c162tA ;WA , ;W , .tN , , - (, ) .5.1.3 -, .5.1.4 () / (-) , , .5.2 .5.3 10 100 3, ( PTFE) .6 , , ISO 3170 ISO 3171, / , .7 7.1 7.1.1 - .3 EN 160120121; 2 ; 3 ; 4 1 7.1.
7、2 - - , - , 5.1.2. -. - , - .7.2 7.4, (4.2) , (4.3), (4.4). ( ), . . , .i-x - f ( ) fi=MAAMiistst,(2) i i- , ;st , , 2;Ai , i- , 2;Mst , . , .7.3 c114 15 - 1, 2 3 0,1 /3.7.4 5 10 . - (5.3) 0,1 , . (4.3) 0,1 , . mst, , 2 % . 5 % . s, 0,050 . ( 5 100 3) . - 0,1 . s0,1 . (% .). ,- .7.5 (7.4) -. , .7.6 - (7.2).4 EN 160120128 8.1 mi, ,