1、 . (ISO 1138:2007, IDT) , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)ISO 11382013, 1.092 . 1.22009 . , - . , , -, 1 160 - , - () - , 42 (-)3 , (- 27 2013 . 59-) : ( 3166) 00497 ( 3166) 00497 AMBYKGMDRUTJUA - 4 ISO 1138:2007 Rubber compoundingingredients Carbon black De
2、termination of sulfur content ( . -. ), Amd.1:2012. SC 3 ( ) ISO/TC 45 (ISO). (en). , - , , , . . - . (IDT)5 19 2014 . 199- ISO 11382013 - 1 2016 .6 II ISO 11382013 - , - . () - . , , 2014 -, III ISO 113820131 12 13 14 35 4 () 5IV ISO 11382013 . Rubber compounding ingredients. Carbon black. Determin
3、ation of total sulfur content 201601011 , :- A ;- B ;- C . - . A ( ) - .2 . - ( ).ISO 15671 Rubber and rubber additives Determination of total sulfur content using an automaticanalyser ( . - )3 3.1 -, . . , . .3.2 . . ., - .3.2.1 , 100 /3. 100 (BaCl2c2152H2O) 1 3.3.2.2 , c11420= 1,19 /3.3.2.3 , , ,
4、 . - .1 ISO 11382013 3.2.4 ( ) .3.3 , , .3.3.1 ( ), - , , , , , 19 C35 C 0,02 C.3.3.2 - .3.3.3 30 3.3.3.4 , (125 c177 1) C c1775 C.3.3.5 , (925 c177 25) C.3.3.6 , 60.3.4 3.4.1 (3.3.4) 125 C 1 .3.4.2 (3.3.1) 0,1 0,5 - . - . , .3.4.3 5 3. (3.2.4) ( 3 ).3.4.4 2 3 . - , , , - , . 2 . . , 5 . - . 5 2 C.
5、 ( , .) 10 . 1 .3.4.5 , 250 3. 400 3, 5 3. 53 (3.2.2), 5 3 (3.2.3) 10 3 (3.2.1). - 15 . - 10 3 , -.3.4.6 (3.3.3), 0,1 . 30 (3.3.5), (925 c177 25) C. , 0,1 .3.5 , %, =01373210,( )mmmc45c215100, (1) m2 , ;m1 , ;m0 , .2 ISO 113820133.6 :) ;b) , ;) .4 4.1 - 1425 C. , , -, . , . .4.2 . . ., - .4.2.1 2 (c
6、11420= 1,19 /3) 13 .4.2.2 , ( ) 1,1125 (KIO3), 100 (KI) 5 () 500 3. 1 3. . 30 .4.2.3 , 2,5 5 (II) (HgI2)13.4.2.4 ( ) .4.3 , , .4.3.1 , (1425 c177 25) C.4.3.2 75 .4.3.3 () . 1 (1425 c177 25) C.4.3.4 .4.3.5 , - , (H2SO4, c11420=1,84 /3), - , , .4.3.6 - .4.3.7 500 3.4.3.8 - .4.3.9 , , - (105 c177 2) C.
7、4.4 4.4.1 (4.3.9) - (105 c177 2) C 1 . 1 1 (4.3.3).4.4.2 (4.3.7) (4.2.1), - 2 (4.2.3) , (4.2.2). - (4.3.6) .3 ISO 113820134.4.3 , , 1425 C 1 3/ (.4.4.4). - - . , (4.2.2), . , - 3 , , .4.4.4 - 30 (1425 c177 25) C.4.5 , %, =Vm20,(2) V , (4.2.2), - , 3;m , .4.6 :) ;b) , ;) .5 ISO 15671, - . - .4 ISO 11382013 () .1
