1、 545912011 (VI) 27 2002 . 184- , 1.02004 . 1 - - ( )2 3 6 2011 . 715-4 . () - . , , 2012 , - - II 5459120111 12 13 14 25 26 .27 27.1 27.2 27.3 . 27.4 1:1 27.5 1,5-27.6 .38 38.1 (VI) 38.2 (VI) , .39 310 .4III 545912011 (VI)Leather and fur. Method of chromium (VI) content determination 201301011 , , (
2、VI).2 : 529582008 . , - 532282008 . 1. - . 938.075 . . 938.167 . 177074 ( 104283, 478880) ., , , . 420477 . . 422075 . . 655280 . . 670972 . 1202676 . 1364668 . 2393290 . 2533682 . , - 2922791 ( 835181) . . 1. - - - , 1 , , . (), - () . , , - , , .3 :3.1 (VI): (VI) , - . (VI) (/) .1 545912011 4 (VI)
3、 . (VI) 1,5- - , 540 .5 5.1 4204, . .5.2 4204, 1:1.5.3 6552, . .5.4 4220, . .5.5 1,5-, . . .5.6 6709.6 6.1 250 3 25336.6.2 100 3, 1000 3 1770.6.3 29277.6.4 , 540 .6.5 3,0 20903.6.6 53228.6.7 25336, 1.6.8 12026.7 7.1 7.1.1 938.0.7.1.2 52958.7.1.3 938.0 52958 - (, , , , - - ; ), .7.2 2,8285 , 105 C, -
4、 1000 3 .13 1 (VI). .7.3 10,0 3 - 1000 3 . 1 3 0,01 (VI). .7.4 1:150 3 200 3 50 3 (5.1). 30 . - - 5 C 20 C.7.5 1,5-0,5 1,5- 100 3 2 3 1:1. - 5 C 8 C . .2 5459120117.6 (7.3). 100 3 0,5, 1,0, 1,5, 2,0, 2,5, 3,0, 3,5, 4,0, 4,5,5,0 3 (V1), 1,0 3 1:1 (7.4), 0,3 3 (5.3), 2,0 3 1,5- (7.5), . 5 - (6.4) 540
5、(6.5) 3,0 . , - , (7.3). - 100 3, 2/3 , 1,0 3 1:1 (7.4), 0,3 3 (5.3), 2,0 3 1,5- (7.5), . (VI) r,/3, , -, r=VV112, 1 (VI) (7.3), /3;V1 (7.3), , 3;V2 , (7.3), 3. , X - (VI) /3,Y .8 8.1 (VI) (2,00 c177 0,01) , (7.1), 0,001 250 3. 100 3 , , , - , (20 c177 3) C 18 . (6.7) .8.2 (VI) , , (8.1), 50,0 3(V1)
6、 100 3(V2). 1,0 3 1:1 (7.4), 0,3 3 (5.3), 2,0 3 1,5- (7.5). - , 5 540 (6.5) 3,0 . (VI) r. (VI) , - (8.1). , 8.1, (V1) , 1,5-.9 (VI) , /, =VC VVmCr21, V , (VI) , 3;V1 ( ), , 3;V2 (VI), 3;r (VI), , /3;m , .3 545912011 - , . c177 10 % =0,95. (VI) .=D, D .D =100100 c45W, W (), 938.1, %.10 :- (VI), 9;- ;- (7.1) ();- , 3,0 ;- , (/) 0,0001 /;- . 681.1:675.621:006.354 59.140.30 19 : , , , (VI), , 545912011 . . . . 26.09.2012. 24.10.2012. 60 c180 8418. . . . 0,93. .-. . 0,58. 114 . . 926. , 123995 , ., 4.www.gostinfo.ru infogostinfo.ru . . , 105062 , ., 6.