1、 13898-12006102005/195 - - , 1 ISO 13898-1:1997Steel and iron Determination of nickel, copperand cobalt contents Inductively coupled plasma atomicemission spectrometric method Part 1: General requirementsand sample dissolution(IDT) 27 2002 . 184- , 1.02004 . 1 145 - 2 - 21 2006 . 326-3 13898-1:1997
2、. , . . 1. (ISO 13898-1:1997 Steel andiron Determination of nickel, opper and cobalt contents Inductively coupled plasma atomic emissionspectrometric method. Part 1: General requirements and sample dissolution). - 1.52004 ( 3.5). - , 4 , - . () . - , , 2007 , - - II 13898-12006 - , 1 Steel and iron.
3、 Inductively coupled plasma atomic emission spectpometric method for determination of nickel,copper and cobalt contents. Part 1. General requirements 200801011 - - , , 1. 1 , %0,001 0,300,001 0,400,001 0,10 , - , - 13898-2, 13898-3, 13898-4. - .2 -: 385-1:1984 . . 1. 648:1977 . 13898-2:1997 . , . -
4、. 2. - 13898-3:1997 . , . - . 3. - 13898-4:1997 . , . - . 4. - 14284: 1996 . 1 13898-12006 3 , . - . - . 2. 2 , 231,60324,75 327,40228,62361,38 424,68 ( )371,03 ( )4 , , , .4.1 , 0,0001 % .4.2 c114c1871,19 /3, 1 : 1.4.3 c114c1871,40 /3, 1 : 1.4.4 , 1 /3. 1 1,534 99,98 %, - 500 3 40 3 (4.3). - 1000 3
5、, .13 1 .4.5 , 1 /3. 1 1,270 99,98 %, - 500 3 50 3 (4.2). 1000 3, .13 1 .4.6 . 13898-2, 13898-3, 13898-4.5 , 385-1 648 .2- 250.5.1 - - 7.4.1 , 5.1.1 5.1.3. . - ( ), - . -, .2 13898-120065.1.1 .1.3 ( ). - - . 0,4 % - .5.1.2 , , .1.1 .1.2 ( )., , , . , 3. 3 , , , / 3 , / 3Ni 231,60Cu 324,75Co 228,621,
6、50,80,80,040,020,045.1.3 .2. . 0,999.6 14284.7 7.1 1,000 1 .7.2 ,- , , .7.3 7.3.1 (7.1) 200 3, 10 3- (4.3), - . 10 3 (4.2) . - 200 3. , 2 3 (4.4) 10 3 (4.5). .7.3.2 13898-2, 13898-3 13898-4.7.4 7.4.1 - . :- (, -);- ;- ;- ;3 13898-12006- , 2;- . - . - (361,68 ) (371,03 ) . . 5.1.1 5.1.3.7.4.2 1 . . 2
7、3 3 . -, .:, , . -. . , 5.1.1. - .- I0 Ii, ININ= Ii I0. (1)7.4.3 : Y ; (/3). . -, 5.1.3.8 8.1 - (7.4.3) .Wc113,%, WWWmmc113c113c113c114c114 c114c114c113c113 c113c113c61c215c61c43c43( ) ( ), ,10610200101005000,(2) c114c113,1 , /3;c114c113,0 , /3;m , ;Wc113,0 , %.8.2 , 13898-2, 13898-3, 13898-4, , .4 13898-120069 :) , , ;b) , ;) ;d) , , , .5 13898-12006 () .1 (DL), , (), - , . . . - 15 . - , . , , - 10, (10 c180DL), 1000,
