1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS B ISO 13503 3 3: KS B ISO 13503 3: 2007(2012 ) 2007 11 30 http:/www.kats.go.krKS B ISO 13503 3: 2007 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : :2007 11 30 :2012 12 20 20120737 : : ( 02-509-7274) (http:/www.kats.go.kr). 10 5 , . KS B ISO 13503 3: 2007 (
2、2012 ) 3: Petroleum and natural gas industries Completion fluids and materials Part 3: Testing of heavy brines 2005 1 ISO 13503 3, Petroleum and natural gas industries Completion fluids and materials Part 3: Testing of heavy brines , . 1 , . . , (淸度 ), , ( ) , pH . , , , . 2 . . ( ) . ISO 10414 1, P
3、etroleum and natural gas industries Field testing of drilling fluids Part 1: Water-based fluids ASTM E77, Standard Test Method for Inspection and Verification of Thermometers NIST SRM 185h, Potassium Hydrogen Phthalate, pH Standard NIST SRM 185g, Potassium Dihydrogen Phosphate, pH Standard NIST SRM
4、191C, pH Standards NBS(NIST) Circular 555, Testing of Hydrometers, 22 Oct 1954 3 . 3.1 KS B ISO 13503 3: 2007 2 3.1.1 ACS (American Chemical Society) 3.1.2 , , 3.2 ACS (American Chemical Society) API (American Petroleum Institute) ASTM (American Society for Testing and Materials) CAS (Chemical Abstr
5、acts Service) FCTA (first crystal to appear) LCTD (last crystal to dissolve) NIST (National Institute of Standards and Technology) NTU (nephelometric turbidity unit) psi (pounds per square inch) TCT (實 ) (true crystallization temperature) TD (to deliver) USC (United State Customary) V (volts) (: g/c
6、m3) 1 2 7070 F(21 ) (: lb/gal) 2121 (70 F) (: g/cm3) A SI (: g/cm3) A USC (: lb/gal) m cf (: lb/ft3) SI (: kg/m3) SI 2121 (70 F) (: kg/m3) USC (: lb/gal) W , (F) 1 , (F) 2 , (F) m , (F) cflb/ft3 (: psi/ft) SI (: kPa/m) USClb/gal (: psi/ft) Bc C (: g/cm3/) C (: lb/gal/100 F) Cp (: lb/gal/1 000 psi) C
7、SI (: kg/m3/) KS B ISO 13503 3: 2007 3 CUSC (: lb/gal/F) h ( ), (: ft) h2 ( ), (: ft) R R1 R2 V (: cm3) V1 (原 ) (: cm3) Zc 4 4.1 . 4.2 . 5 5.1 5.1.1 . . 5.1.2 , , . 5.1.3 . 5.1.4 , , , . 5.1.5 . 5.1.6 . 5.2 5.2.1 ACS . 6 . KS B ISO 13503 3: 2007 4 5.2.2 ASTM D 1126 , . 5 g/cm3 . 5.3 5.3.1 . . . . .
8、5.3.2 . ASTM E 77 NBS(NIST) Circular 555 NIST . 5.3.3 , KS ISO ASTM 1, 4 6 . . 5.3.4 . 5.3.5 NIST . 5.4 5.4.1 . 5.4.2 . , . . 5.4.3 . 5.4.4 KS B ISO 13503 3: 2007 5 . . . 5.5 5.5.1 5.5.1.1 4 L(1 gal) . 1 . 5.5.1.2 . 5.5.1.3 1 4 . 5.5.1.4 . 0.1 (0.2 F) . 5.5.1.5 , 5.5.1.1 5.5.1.4 . 5.5.1.6 . . . 5.5.
9、2 5.5.2.1 NIST . 5.5.2.2 5.5.2.9 . 5.5.2.2 1 . 5.5.2.3 . . . 0.2 (0.5 F) . NIST 5 . 5.5.2.4 . . 4 5 . 5.5.2.5 5.5.2.3 5.5.2.4 . 5.5.2.6 R1 . 1 . 5.5.2.7 5.5.2.3 5.5.2.4 . R2 2 . KS B ISO 13503 3: 2007 6 5.5.2.8 . 1221c)(0001 =RRZ (1) Zc: R1: R2: 1: 2: F . 5.5.2.9 . Bc (Zc 1)1 000(R1 1) (2) Bc: Zc: R
10、1: 1: 5.5.2.10 Zc, Bc . 6 6.1 6.1.1 . , . . , . , (downhole) . 6.1.2 . g/cm3, kg/m3 lbm/gallon . . ( ) . . . 6.1.3 21 (70 F) . . . 6.1.4 . ISO 10414 1 . ( ) . 1 . KS B ISO 13503 3: 2007 7 1 7 2 8 3 9 4 10 5 11 6 1 6.1.5 ( 2 ) ( ) , . . ISO 10414 1 . 6.1.6 5 kg/m3(0.005 g/cm3, 0.05 lb/gal) 10 kg/m3(0
11、.01 g/cm3, 0.1 lb/gal) . . (6.2.1 6.2.3 ). KS B ISO 13503 3: 2007 8 1 5 2 6 3 7 4 8 2 6.2 6.2.1 . 0.002 , . . 5. . 21 (70 F) . 60 F 60 F . 60 F/60 F . 6.2.2 : . 2.54 cm(1.0 in) . 2.54 cm(1.0 in) . 6.2.3 1 (2 F) , 0 (32 F) 105 (220 F) 6.2.4 6.2.5 KS B ISO 13503 3: 2007 9 21 1 (70 F2 F) 6.3 6.3.1 . .
12、. 6.3.2 . 6.3.3 . 6.3.4 3 ( ) . 6.3.5 . 1 2 3 3 6.4 21 (70 F) 6.4.1 21 (70 F) . 1 . USC (3) . CUSC ( 5.965 910 4) (6.95410 3R) (4.79910 3R2) (1.26310 3R3) (3) KS B ISO 13503 3: 2007 10 R : 1 21 kg/m3SI 21 g/cm321 70 F lb/gal 70 kg/m3/ CSI g/cm3/ C lb/gal/F CUSC 1019 1.019 8.5 0.60 0.000 61 0.002 84
13、1078 1.078 9.0 0.63 0.000 63 0.002 91 1138 1.138 9.5 0.64 0.000 64 0.002 97 1198 1.198 10.0 0.65 0.000 65 0.003 02 1258 1.258 10.5 0.66 0.000 66 0.003 07 1318 1.318 11.0 0.67 0.000 67 0.003 13 1378 1.378 11.5 0.69 0.000 69 0.003 18 1438 1.438 12.0 0.70 0.000 70 0.003 24 1498 1.498 12.5 0.71 0.000 71
14、 0.003 30 1558 1.558 13.0 0.73 0.000 73 0.003 37 1618 1.618 13.5 0.74 0.000 74 0.003 44 1678 1.678 14.0 0.76 0.000 76 0.003 53 1738 1.738 14.5 0.78 0.000 78 0.003 63 1797 1.797 15.0 0.81 0.000 81 0.003 74 1857 1.857 15.5 0.83 0.000 83 0.003 86 1917 1.917 16.0 0.86 0.000 86 0.004 00 1977 1.977 16.5 0
15、.90 0.000 90 0.004 16 2037 2.037 17.0 0.94 0.000 94 0.004 34 2097 2.097 17.5 0.98 0.000 98 0.004 54 2157 2.157 18.0 1.03 0.001 03 0.004 76 2217 2.217 18.5 1.08 0.001 08 0.005 01 2277 2.277 19.0 1.14 0.001 14 0.005 28 (3) 1 21 (70 F) . a) () , kg/m3 (4) . SI 21 999R (m 21)CSI (4) SI 21: 21 (kg/m3) R
16、: m: () CSI: 1 b) () , g/cm3 (5) . 21 0.999R ( m 21)C(5) 21: 21 (g/cm3) R : KS B ISO 13503 3: 2007 11 m: () C : 1 c) (F) , lb/gal (6) . 70 8.337R ( m 70)CUSC(6) 70: 70F (lb/gal) R : m: (F) CUSC: 1 (3) 6.4.2 2 . (7) g/cm3/ (C) . 2121=C (7) C : 1: (g/cm3) 2: (g/cm3) 1: () 2: () 6.4.3 . 21 (70 F) . ( ,
17、 ). 6.4.4 , . . . 6.5 kg/cm3 6.5.1 kg/m3 . USC SI0.008 345 (8) USC: (lb/gal) SI: (kg/m3) cf SI0.062 43(9) cf: (lb/ft3) KS B ISO 13503 3: 2007 12 SI: (kg/m3) SI0.001 (10) : (g/cm3) SI: (kg/m3) 6.5.2 )017102.0(Si= (11) SI: (kPa/m) : (g/cm3) 24.19USCUSC= (12) USC: lb/gal (psi/ft) USC: (lb/gal) 144cfcf= (13) cf: lb/ft3 (psi/ft) cf: (lb/ft3) (12) (13) . 6.6 6.6.1 . . , . . . . 12 . 2 . . ( ) , ( ) . KS B ISO 13503 3