1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS C IEC 60589 KS C IEC 60589:2008 2008 11 28 http:/www.kats.go.krKS C IEC 60589:2008 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : : 2008 11 28 2008-0833 : : ( 02-509-7294) (http:/www.kats.go.kr). 10 5 , . KS C IEC 60589:2008 i ii .1 1 .1 2 .1 3 1 4 1 4.1 1
2、4.2 2 5 3 6 .3 A 4 B KCl .5 KS C IEC 60589:2008 6 KS C IEC 60589:2008 ii . , , . , , . KS C IEC 60589:2008 Methods of test for the determination of ionic impurities in electrical insulating materials by extraction with liquids (KS) (IS) 1977 1 IEC 60589, Methods of test for the determination of ioni
3、c impurities in electrical insulating materials by extraction with liquids , . 1 / . , . 2 ex . SI S m 1 . S cm 1 . 3 250 mL (m 1) (cm 1) k 5 % , 50 Hz 3 000 Hz 1 M . , 100 V 1 T . , B , k (KCl) . 4 4.1 KS C IEC 60589:2008 2 4.1.1 (Test water) . 210 4S m 1 . pH 6.8 7.2 . pH . . pH 5.7 5.9 . pH 6.4 ,
4、 pH = 7 . pH . 4.1.2 , . 20 g . (50.1) g , 3. 3 100 mL . 4 . (605) . . 4.1.3 . . 2 . . (231) . , . 4.2 4.2.1 , . 0.5 10 9 S m 1 . 1 10 11S m 1 . . 1 % (Fullers earth) . 5 m 15 m . 1 120 . 2 , KS C IEC 60589:2008 3 . , . 3 . 4.2.2 20 g 80 100 2 . (50.1) g 3. 3 100 mL . 4 . (605) . . 10 % , . 4.2.3 .
5、. . 2 . (231) 1 . , . 5 . )11(1BSexexRRk = ex: S m 1(S cm 1) ex: - ( - ) k : m 1(cm 1) RS : () RB : () 6 . KS C IEC 60589:2008 4 A . 10 mL 3 g (IV): H2(PtCl6) 6H2O 0.02 g (II): Pb(CH3COO) 3H2O 4 V . . . . . 1 , 10 . 2 1 2 . , 2 % 5 % . , . . , . . . KS C IEC 60589:2008 5 B KCl 0.1 N, 0.01 N 0.001 N
6、. KCl . 105 2 . 0.1 N 7.455 5 g, 0.01 N 0.745 6 g (KCl) (232) . 1 000 mL 1 L (4.1.1 ). 0.001 N . 0.01 N KCl 100 mL 1 000 mL 1 L (4.1.1 ). 23 : 0.1 N KCI 1.24 S m 10.01 N KCI 0.136 S m 10.001 N KCI 0.014 1 S m 1 k . k KCI R R () . KCl (stopper) . . KS C IEC 60589:2008 6 KS C IEC 60589:2008 , . 1 1.1
7、(IEC) (KS) . (WTO/TBT ) , IEC 60589 (KS A 0001: 2008) . 2 (TC) 2.1 : TC 112( ) 2.2 IEC 60589 KS C IEC . . 3 3.1 , . / (,) / (.) . 3.2 . 4 , . (www.standard.go.kr ) . . 5 KS C IEC 60589:2008 7 . . IEC KS C IEC 1 conductivity 2 control sample 3 apparatus 4 rinse 135513 7017 (02)60094114 (02)600948878 http:/ KS C IEC 60589:2008 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Methods of test for the determination of ionic impurities in electrical insulating materials by extraction with liquids ICS 17.220.99; 29.035.01 Korean Agency for Technology and Standards http:/www.kats.go.kr