KS H ISO 1854-2006 Whey cheese-Determination of fat content-Gravimetric method(Reference method)《乳清干酪 脂肪含量的测定 重量法(参考方法)》.pdf

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1、 KSKSKSKS SKSKSKS KSKSKS SKSKS KSKS SKS KS 2006 11 29 http:/www.kats.go.krKS H ISO 1854 () KS H ISO 1854: 2006 (2011 ) H ISO 1854: 2006 : ( ) ( ) ( ) ( ) : (http:/www.standard.go.kr) : :2001 12 22 :2006 11 29 :2011 12 29 2011-0652 : : ( 02-509-7273) (http:/www.kats.go.kr). 10 5 , . ICS 67.100.30 KS

2、() H ISO 1854: 2006(2011 ) Whey cheeseDetermination of fat content Gravimetric method(Reference method) 1999 3 ISO 1854 Whey cheese Determination of fat content Gravimetric method(Reference method) . ISO 1854 ISO/TC 34 (SC 5), (IDF) (AOAC International) , . 3 2 (ISO 1854: 1987) , 2 . A B . , . , . .

3、 1. . ( .) , WeibulBerntop (ISO 8263 3 ) . 2. . . KS H ISO 3889 3. . 3.1 . %(m/m) . 4. , . . (Rse Gottlieb) . 5. , , . (9.2.2 ) , . H ISO 1854: 2006 2 5.1 25 % (NH3) ( 20= 910 g/L). , (9.4.3 ). 5.2 (C2H5OH) 94 % (A.5 ). 5.3 (congo red) 100 mL (6.14) 1 g , . (9.4.4 ). . 5.4 (C2H5OC2H5) (A.3 ) 2 mg/kg

4、 , (9.2.2, A.1 A.4 ) . . . 5.5 3060 , 36 (CH3CH23CH3) (9.2.2, A.1 A.4 ) . . 5.6 (5.4) (5.5) . 6. . . 6.1 0.1 mg . 6.2 (6.6) , 8090 g 500600 . (9.4.7 ). 6.3 100 (9.4.14 ) . 6.4 (1022) , . 6.5 . 6.6 KS H ISO 3889 . B (siphon) . PTFE(polytetrafluoroe- thylene) . (5.4) 60 15 , . 6.7 ( )(6.6) . 6.8 , (5.

5、6) . 6.9 125250 mL , 250 mL 80100 mm, 50 mm H ISO 1854: 2006 3 . 6.10 , ( ). 6.11 5 mL 25 mL 6.12 10 mL 6.13 , . 6.14 6.15 100 mL 7. , KS H ISO 707 . . 8. (6.14) . , 2 . . , . . . . . 9. 1. (11.2) , 9.19.4 2 . 2. (6.6 ) , B . 9.1 (8.) . (6.6) 3 g 1 mg . . 9.2 9.2.1 9.4.1 10 mL (A.2 ). 1.0 mg , (9.2.

6、2) . 2.5 mg . 9.2.2 9.2.1 . , 9.3 . 1.0 mg (A.1 ). 1.0 mg 100 mL . 1.0 mg . . 1 g . 100 mL 1 g . , . , . H ISO 1854: 2006 4 9.3 (6.9) (6.10) , 102 (6.4) 1 . 1. , . ( 1 , 30 ). 2. . , 1.0 mg . 3. . 9.4 9.4.1 . 1011 mL (655) 10 mL (9.1). . . 9.4.2 , (6.5) 20 . . 9.4.3 (5.1) (5.1 ) 2 mL . . 9.4.4 (5.2)

7、 10 mL . . (5.3) 2 . . 9.4.5 (5.4) 25 mL . (6.6) 1 . . . (5.6) . (6.8) . 9.4.6 (5.5) 25 mL . ( ) . 9.4.4 30 9.4.5 . 9.4.7 8090 g 15 . (6.2) 30 (6.7) . . 9.4.8 (5.6) . (6.8) . ( 1 ) . 1 2 KS H ISO 3889 , . 9.4.9 (9.3 ) ( 2 ) . (6.10)( ) . 9.4.10 (5.6) , . H ISO 1854: 2006 5 . 9.4.14 . 9.4.11 (5.2) 5

8、mL . 9.4.4 . 9.4.12 9.4.59.4.9 2 . (5.4) (5.5) 25 mL 15 mL . , . ( 1 ) ( 2 ). 9.4.13 9.4.59.4.9 3 . (5.4) (5.5) 15 mL . . ( 1 ) ( 2 ). 3 3 % . 9.4.14 , (6.3) , ( ) . (5.6) . 9.4.15 102 (6.4) 1 . . . ( .) ( 1 , 30 ). . , 1.0 mg . 9.4.16 102 (6.4) 30 . 9.4.15 1 2 2, 3 1 2, 3 1 H ISO 1854: 2006 6 . 1.0

9、 mg . . 10. 10.1 . wf=04321)()(mmmmm 100 % wf: (%) m0: (9.1) (g) m1: 9.4.16 (g) m2: (9.3) (g) m3: (9.2) 9.4.16 (g) m4: (9.2) (9.3) (g) 10.2 . 11. 11.1 ISO 5725(1) ( 6 ). 95 % , . (1) ISO 5725: 1986( ) . 11.2 2 , 5 % 0.2 % . 11.3 2 5 % 0.3 % . 12. . ( ) 2.5 mg H ISO 1854: 2006 7 A() A.1 (9.2.2 ) . .

10、(10.1 m3 m4) , 1.0 mg . . 1 g . 100 mL 1 g . . A.2 (9.2.1 ) (m1 m2) (9.4.16 9.3) . ( , , ) 0.5 mg , . 2.5 mg . . 2.5 mg , (12.) . 1.0 mg , , (9.2.2 A.1 ). A.3 10 mL 10 % ( .) 1 mL 1 . . . ( ) 3 . 1 L 80 cm2 . , 1 L 10 g 98 %(m/m) 2 mL 1 . , . . A.4 1 kg 1 mg . . 1 kg 7 mg . H ISO 1854: 2006 8 . . A.

11、5 . H ISO 1854: 2006 9 B() B.1 , . 6.6 ( B.1 ) . B.2 B.2.1 8. B.2.2 (6.6 B.1 ) 9.1 . . B.2.3 9.2 A.2 . B.2.4 9.3 B.2.5 B.2.5.1 . (655) 10 mL (B.2.2) . . B.2.5.2 (6.5) . 20 . B.2.5.3 (5.1) (5.1 ) 2 mL . . B.2.5.4 (5.2) 10 mL , . (5.3) 2 . B.2.5.5 (5.4) 25 mL . (6.6) . 1 . . (5.6) . (6.8) . B.2.5.6 (5.5) 25 mL . ( ) . B.2.5.5 30 . B.2.5.7 8090 g 15 . , 30 (6.7) . . B.2.5.8 (5.6) . (6.8) . B.2.5.9 . 4 mm . . (9.3 ) . , (6.10)( ) . . H ISO 1854: 2006 10 , (rubber bulb) . B.2.5.10 (5.6) . . 9.4.14 . B.2.5.11 5 mL . . B.2.5.4 . B

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