1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS I ISO 9096 KS I ISO 9096:2009 2009 12 18 http:/www.kats.go.krKS I ISO 9096:2009 : ( ) ( ) () ( ) : (ISO/TC146) () ( ) () : (http:/www.standard.go.kr) : :1998 3 26 :2009 12 18 2009-0830 : : (ISO/TC146) ( 02-509-7266) (http:/www.kats.go.kr). 10 5 , . KS I I
2、SO 9096:2009 Stationary source emissions Manual determination of mass concentration of particulate matter 2003 2 ISO 9096, Stationary source emissions Manual determination of mass concentration of particulate matter , . 1 201 000 mg/m3 ( ) . (AMS) . , . (in-stack) (out-stack) . 2 . . ( ) . KS A ISO
3、5725 ( ), ( ) KS I ISO 10780, KS I ISO 12141, ( ) 3 . 3.1 , (particulate matter, dust) , 1 , ( ) . , KS I ISO 9096:2009 2 (: ) . 2 . ( ) . 3.2 (filtration temperature) 3.3 (in-stack filtration) 3.4 (out-stack filtration) ( ) 3.5 (isokinetic sampling) (vn) (Vs) 1 vn/vs . vs vn 1 KS I ISO 9096:2009 3
4、3.6 (hydraulic diameter) dh ssh4lAd (1) As: ls: 3.7 (sampling plane) 2 1 2 3 4 5 2 3.8 (sampling line) . KS I ISO 9096:2009 4 2 3.9 (sampling point) 3.10 (standard conditions) , 101.325 kPa 101.3 kPa , 273.15 K 273 K . 3.11 (overall blank) , . . (mg/m3) . . 3.12 (weighing control procedure) / (7.2 )
5、 , . . 3.13 (measurement series) 3.14 (limit value) (: ) , . 4 4.1 . ( ) . . . . KS I ISO 9096:2009 5 . . a) 5 b) , , c) d) e) f) g) , h) i) . j) / . k) . 4.2 a) . , (FGDS) (CaSO4) (SO2) (NH4SO4) (NH3) 7.1 a) . b) 1) . , (HF) (6.2.5 ) 2) . , (8.1 ). 5 5.1 . . . 5.2 ( ) . ( , ) . 5.3 KS I ISO 9096:20
6、09 6 5.4 B . a) 15 ( KS I ISO 10780: 2008 C ). b) . c) (Pitot , 5 Pa ). d) 3: 1 . , (7.4.6 ). 5 , 2 ( 5 ) . . 5.4 . . 1 2 . ( B ). 5 cm (d 1.5 m ) 3 % (d1.5 m ) . . 1 2 . . (5.2 ) , 1 2 . 7.3.2 . 1 , m () 0.35 1a 1a 0.350.70 2 3 2 5 4 0.701.00 2 5 4 9 8 1.002.00 2 7 6 13 12 2.00 2 9 8 17 16 a 1 . KS
7、 I ISO 9096:2009 7 2 , m2 a 0.09 1b0.090.38 2 4 0.381.50 3 9 1.50 4 16 a , 2 . b 1 . 5.5 B . . 125 mm 100 mm250 mm . ( 0.7 m ) ( F ). 5.6 , . (cexp) (m) . expncmV (2) Vn( ) Qa(L/min) t(min) . : Vn tQa . tanQV taexpQcm (3) 6 6.1 , , Pitot KS I ISO 10780 Pitot (: S Pitot ) . 0.05 kg/m3 KS I ISO 9096:2
8、009 8 . / , ( ) / O2/CO2 . 3 . 6.2 . a) ( ) b) . ( ) ( ) . . c) 6.2.1 a) “ ” ( 3): . ( ) . . ( ) . KS I ISO 9096:2009 9 1 10 2 11 3 Pitot 12 4 13 5 14 6 15 7 16 8 ( ) 17 9 3 “ ” b) “ ” ( 4): ( ) . . KS I ISO 9096:2009 10 1 10 2 11 3 Pitot 12 4 13 5 14 6 15 7 16 8 ( ) 17 9 4 “” . . , . , , . (: ) . .
9、 . . . 6.2.2 KS I ISO 9096:2009 11 . ( ) . A 3 . . . a) 10 mm . 7.3.3 b) 30 . c) 30 mm . d) 50 mm 30 . e) 1) . 2) 50 mm . . 10 % . 8 mm 4 mm . 6.2.3 ( ) (7.3.1 ). (7.3.4). 6.2.4 “ ” , (7.3.4). . . 6.2.5 0.3 m 99.0 % . . (7.3.3 ). . KS I ISO 9096:2009 12 a) SO3 . , . b) . c) PTFE(polytetrafluoroethyl
10、ene) . d) . . . e) , . (: 0.5 m/s 10 kPa 3 kPa ). f) . g) “ ” ( , ) . h) , . i) (: PTFE ) . 6.2.6 / ( ) , . 6.2.7 , (: ) . . ( ) 3 . . a) ( 5 ) 1) 10 g/m3 / 2) 3) , (orifice) 4) 2 % , 1 % KS I ISO 9096:2009 13 1 5 2 6 3 7 4 8 5 b) ( 6 ) 1) 10 g/m3 / 2) 3) 2 % , 1 % 4) , 1 6 2 7 3 8 4 9 5 6 c) ( 7 ) 1) 2) 3) ( ) ( ) 1 % , 2 % . KS I ISO 9096:2009 14 1 2 3 4 5 6 7 , ( 4 ) 6.3 6.3.1 6.3.2 10 mg/L 6.3.3 (: 250 mL) 6.3.4 . . 6.4 6.4.1 . 6.4.2 , ( , ) 6.4.3 5 6.4.4 , 0.010.1 mg , , , , . 6.4.5 6.4.6 6.4.7 7 7.1 KS I ISO 9096:2009 15 . (: ) . . , , . / .