1、 KS M ISO 2592KSKSKSKSSKSKSKS KSKSKS SKSKS KSKS SKS KS KS M ISO 2592: 2007 2007 6 29 http:/www.kats.go.kr KS M ISO 2592: 2007 : () ( ) GS () SK() () ( ) : (http:/www.standard.go.kr) : :2007 6 29 20070331 : : ( 02-509-7270) (http:/www.kats.go.kr ). 7 5 , . KS M ISO 2592: 2007 Determination of flash a
2、nd fire pointsCleveland open cup method 2000 2 ISO 2592, Determination of flash and fire points Cleveland open cup method , . 1 . 79 , KS M ISO 2719 . , . 2 . 2 . . ( ) . KS M 2001, KS M ISO 3171, 3 . 3.1 101.3 kPa KS M ISO 2592: 2007 2 3.2 101.3 kPa , 5 4 . . . . 5 . (barometric pressure) (standard
3、 atmospheric pressure) . 5 5.1 . ( ) , . 5.2 C.2 . 5.3 . 6 6.1 A . , A . , . , . 6.2 460 mm, 610 mm . KS M ISO 2592: 2007 3 6.3 B B , . 6.4 kPa , . . 7 7.1 ( 1 2 ) (6.1) . . 1 , . 2 , (fume hood) . 7.2 (5.1) . . , (5.3) . 7.3 56 . 7.4 6 mm , (arc) . , 2 mm . 6 mm . 7.5 7.5.1 (CRM)(5.2) , 1 . CRM 2/R
4、 . R (14. ). KS M ISO 2592: 2007 4 2 (SWSs) (5.2). CRM SWS SWS C . 7.5.2 , . 8 8.1 KS M 2001, KS M ISO 3171 . 8.2 . , 85 % 95 % . 8.3 . 30 . 9 9.1 (subsampling) 56 . , 50 % (10.1 ). 9.2 , . . 9.3 . 10. . 9.4 56 . . 10. . 10 10.1 50 % , . 10.2 (6.4) . KS M ISO 2592: 2007 5 0 . 10.3 (9.4 ) (meniscus)
5、. , . , . . , . 10.4 (bead) 3.2 mm 4.8 mm . 10.5 1417 /min . 56 , (235) 56 /min . (7.1 2 ). 10.6 (235) (6.3) 2 . , 150 mm 1 . 2 mm . . , . 10.7 , , . (halo) . 10.8 18 . 18 , . 11 , 10. 56 /min . 2 5 . 5 , . A.2 . 12 KS M ISO 2592: 2007 6 12.1 (kPa) , kPa . hPa 0.1 = kPa mbar 0.1 = kPa mmHg 0.133 3 =
6、 kPa 12.2 101.3 kPa, Tc . )3.101(25.00pTTc += T0 : ( ) p : (kPa) 98.0104.7 kPa . 13 . 14 14.1 KS M ISO 4259 14.2 14.3 . 14.2 , r 20 1 . , r = 8 , r = 8 14.3 , R 20 1 . , R = 17 , R = 14 15 . KS M ISO 2592: 2007 7 a) b) c) (13. ) d) e) KS M ISO 2592: 2007 8 A ( ) A.1 A.1 . . A.2 , , (wrought iron) ,
7、( ). A.1 . , . A.3 . A.3 . 1.6 mm (orifice) 0.8 mm . 150 mm . 2 mm . 3.24.8 mm , . A.4 , , . . , . . A.5 . KS M ISO 2592: 2007 9 : mm 1 7 2 8 ( ) 3 9 (filling mark) 4 3.24.8 mm 10 5 11 6 0.8 mm A.1 A.6 . KS M ISO 2592: 2007 10 A.7 ( ) A.2 . : mm 1 2 a A.2 KS M ISO 2592: 2007 11 B ( ) B.1 6400 mm 25
8、2 10 20 2(260 ) 4(260 ) (expansion chamber) 400 mm (3105) mm (7.01.0) mm (5.250.75) mm mm 0 (505) (22515) IP 28C/ASTM 11C . KS M ISO 2592: 2007 12 C ( ) C.1 2 (SWS) (CRM) SWS . ( ) KS A ISO Guide 344 ISO Guide 355 CRM C.2.2 /SWS . KS A ISO Guide 333 KS M ISO 42592 . 95 % . C.2 C.2.1 (CRM) KS A ISO G
9、uide 34 KS A ISO Guide 35 . C.2.2 2 (SWS) . a) , CRM 3 b) 3 . . SWS , 10 . C.3 C.3.1 SWS CRM . C.1 . SWS CRM . SWS CRM . KS M ISO 2592: 2007 13 C.1 Tetradecane 116 Hexadecane 139 C.3.2 1 1 , 10. CRM(C.2.1) . C.3.3 , 10. SWS(C.2.2) . C.3.4 12. . 0.1 . C.4 C.4.1 SWS CRM . C.4.1.1 C.4.1.2 , KS A ISO Gu
10、ide 35 SWS CRM KS M ISO 4259 . R . C.4.1.1 CRM SWS , SWS CRM . 2Rx x: : SWS CRM R: C.4.1.2 CRM SWS n , SWS CRM n . 21Rx x : : CRM SWS KS M ISO 2592: 2007 14 R1:nrR1122 . R : r : n : CRM SWS C.4.2 , . C.4.3 SWS , CRM . , SWS . C.4.4 , . , CRM . , . , . KS M ISO 2592: 2007 15 1 KS M ISO 2719: 2003, 2
11、KS M ISO 4259: 2003, 3 KS A ISO Guide 33: 2005, 4 KS A ISO Guide 34: 2005, 5 KS A ISO Guide 35: 2005, 16 KS M ISO 2592: 2007 . 1 KS , (ISO) , . 2 2000 ISO 2592(Determination of flash and fire points Cleveland open cup method) , , “ ” . , . SI . 3 . , . . . 5 . . , 79 . A B , C , . 135513 7017 (02)60094114 (02)600948878 http:/ KS M ISO 2592: 2007KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Determination of flash and fire points Cleveland open cup method ICS 75.080 Korean Agency for Technology and Standards http:/www.kats.go.kr