1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS P ISO 9693 KS P ISO 9693:2009 2009 1 6 http:/www.kats.go.krKS P ISO 9693:2009 : ( ) ( ) () ( ) : () ( ) () () () () KS P ISO 9693:2009 : (http:/www.standard.go.kr) ： ：1997 12 2 ：2009 1 6 2009-0003 ： ： ( 025097266) (http:/www.kats.go.kr). 10 5 , . KS P ISO
2、 9693:2009 i ii .1 1 1 2 1 3 .1 4 2 4.1 2 4.2 3 4.3 .3 5 4 5.1 .4 5.2 .4 6 4 6.1 .4 6.2 .6 6.3 .7 7 12 8 , .12 8.1 .12 8.2 12 14 KS P ISO 9693:2009 ii . KS P 5316： 2003 . . , , . , , . KS P ISO 9693:2009 - Metal-ceramic dental restorative systems 1999 2 ISO 9693, Metal-ceramic dental restorative sys
3、tems Amendment 1(2005) . 1 - - . . 2 . . ( ) . KS M ISO 3696, KS P ISO 6872, ISO 6892： 1998, Metallic materials Tensile testing at ambient temperature ASTM B 265 03, Standard specification for titanium and titanium alloy strip, sheet and plate ASTM B 348 03, Standard specification for titanium and t
4、itanium alloy bars and billets 3 . 3.1 / (alloy/metal conditioning) 3.2 (coating agent) (bonding agent) KS P ISO 9693:2009 2 / 3.3 (dental dentine ceramic) 3.4 (dental enamel ceramic) 3.5 (firing schedule) , , 3.6 (heating rate) ( ) 3.7 (metallic material) 3.8 (opaque bonding dental ceramic) 4 4.1 4
5、.1.1 0.5 % 8.2.2 c) . 20 % 2 % . 2 % 20 % 1 % 8.2.2 c) . 8.2.2 d) . 0.02 % . KS P ISO 9693:2009 3 6.1.1 . ASTM B 265 03( , , ) B 348 03( , ) . . . 4.1.2 KS P ISO 6872, 5.1 5.2 . KS P ISO 6872 . 4.2 . 4.3 4.3.1 1 . 1 , Rp0.2MPa % 250 3 25 8.2.2 g) . (0.510 6) K 1 8.2.2 h) . 0.5 g/cm3 8.2.2 i) . 6.1.2
6、, 6.1.3 6.3.1 . . , . 8 . 4.3.2 2 . KS P ISO 9693:2009 4 2 MPa ( ) g/cm2 50 50 50 100 100 100 (0.510 6) K 1 8.2.3 e) . 20 8.2.3 f) . 6.2.1, 6.3.1 6.3.2 . 4.3.3 / 25 MPa . / 25 MPa . 6.3.3 . . 5 5.1 . . 5.2 . , , . 6 6.1 6.1.1 . 4.1.1 . KS P ISO 9693:2009 5 6.1.2 6.1.2.1 1 2 6 - . . 15 . . . 6.1.2.2
7、6.1.2.3 . 6.1.2.2 6.1.2.1 ISO 6892 . (1.50.5) mm . 0.2 % . 4 1 5 MPa . 1 4 . 1 4 . ： mm (key) 1 150.1 1 KS P ISO 9693:2009 6 ： mm (key) 1 150.1 2 6.1.2.3 6.1.2.2 ISO 6892 % . 4 1 1 % . 1 4 . 1 4 . 6.1.3 (DTA) . 6.2 6.2.1 6.2.1.1 KS P ISO 6872 . KS M ISO 3696 3 . 6.2.1.2 KS P ISO 6872 . 6.2.1.3 KS P
8、ISO 9693:2009 7 KS M ISO 3696 3 (1505) 4 . 0.1 mg 0.5 cm2 . 250 mL 4 %( ) ( ) (KS M ISO 3696 3 ) 100 mL . (803) . (803) 16 . . KS M ISO 3696 3 (1505) . 6.2.2 6.2.2.1 KS P ISO 6872 . 10 8 2 . 5 . 6 7 10 10 9 ( 16 ). 6.2.2.2 (cm2) (g) . 2 . 6.3 - 6.3.1 6.3.1.1 6.3.1.1.1 . 6.3.1.1.2 6.3.1.1.3 6.3.1.2 2
9、 4 , 4 , 4 . 30 mm2 . 6.3.1.3 6.1.2.1 . 2 (51) /min 550 . 25 500 (25 500 ) . KS P ISO 9693:2009 8 4.3.1 6.3.1.4 4 , 4 , 4 . 2 1 1 , 2 3 1 . 5 /min . 25 500 ( 500 25 ) . 6.3.1.5 25 500 , 25 500 ( 500 25 ) (25 500 ) . 10 6K 1 (0.110 6) K 1 8.2.3 e). 6.3.2 6.3.2.1 6.3.1.4 . 6.3.2.2 , , 8.2.3 f). 6.3.3
10、- (Schwickerath ) 6.3.3.1 6.3.3.1.1 3 20 mm, (1.50.5) mm/min . 1.0 mm . 6.3.3.2 6 / (251) mm(30.1) mm(0.50.05) mm . ( , , ) . . . KS P ISO 9693:2009 9 3 mm (80.1) mm . (1.10.1) mm ( 3 ). . . . . ： mm 3 6.3.3.3 ( 20 mm, 1 mm). (1.50.5) mm . Ffail( N) . 6 . 6.3.3.4 Ffail k . k dM(0.50.05) mm EM 4 . k
11、4 EM dM k . / b . failbFk 4 4.3.3 . 4.3.3 4 . 4.3.3 4 . KS P ISO 9693:2009 10 4 dM EM k 6.3.3.5 / b 5 . KS P ISO 9693:2009 11 EM(Gpa), dM(mm), Ffail(N)dM(1)=0.44, dM(2)=0.5, dM(3)=0.56 k EM k (1) = 1.818 10-5 EM2 1.873 10-2 EM+ 7.802k (2) = 1.695 10-5 EM2 1.521 10-2 EM+ 6.131k (3) = 1.614 10-5 EM2 1
12、.3 10-2 EM+ 4.986 EM dM k A, B, C : D1 = dM(1), S1 = k (1)D2 = dM(2), S1 = k (2)D3 = dM(3), S1 = k (3)DET = D2 D3 (D2 D3) + D3 D1 (D3 D1) + D1 D2 (D1 D2)A = 1/DET (D3 S2 D2 S3 + D1 S3 D3 S1 + D2 S1 D1 S2)B = 1/DET (D22S3 D32S2 + D32S1 D12S3 + D12S2 D22S1)C = 1/DET S1 D2 D3 (D2 D3) + S2 D3 D1 (D3 D1)
13、 + S3 D1 D2 (D1 D2)bb = Ffail(A dM2+ B dM+ C) b (MPa) 5 / 6.3.3.6 4 4.3.3 . 4.3.3 4 . 4.3.3 4 . KS P ISO 9693:2009 12 7 . , 1 . . 8 , 8.1 . 8.2 8.2.1 . a) b) (g) 8.2.2 . . a) j) . . a) b) / c) 1 % 2 % %, d) . ASTM B 265 03( , , ) ASTM B 348 03 ( , ) d) 0.1 % 0.02 % , ( ) . . e) (“ ” “ ”) f) 0.2 % (M
14、Pa), (GPa), (%) g) ( )( ) h) 25 500 (10 6K 1) i) (g/cm3) KS P ISO 9693:2009 13 j) . , 8.2.3 . a) b) / c) ( ) d) e) 2 4 , 25 500 ( 500 25 ) (10 6K 1) f) 2 4 , , , ( ) KS P ISO 9693:2009 14 1 KS P ISO 1562, 2 KS P ISO 1942 2, 2： 3 KS P ISO 6871 1, (1) 4 ISO 6871 2, Dental base metal casting alloys Par
15、t 2： Nickel-based alloys 5 KS P ISO 7405, 6 ISO 8891, Dental casting alloys with noble metal content of at least 25% but less than 75 % 7 KS P ISO 10993 1, 1： 8 C. Nordling and J. sterman, Physics Handbook, 1987, Chartwell Bratt Ltd., UK - 135513 7017 (02)60094114 (02)600948878 http：/ KS P ISO 9693:2009 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Metal-ceramic dental restorative systems ICS 11.060.10 Korean Agency for Technology and Standards http:/www.kats.go.kr
