1、1P-C-444B%P%K!%RP-C-444AApril 27, 1967FEDERAL SPECIFICATIONCLEANING COMPOUNO, SOLVENT SOLUBLE,GREASE EMULSIFYINGTMs specification was approved by the Assistant Administrator,Office of Federal Supply and Services, General Services Administration,for use of all Federal agencies.1. SCOPE”ANO CLASSIFICA
2、TIONThis specification covers two“ *-soluble c ean ng compounds used to remove oi1,from various surfaces.1.2 Classification.1.2.1 T e.+Clcaning compounds furnishedbe of the o owing types, as specified (see 6types of emulsifyinq solventgrease and other foreign matterunder this specification shall.2):
3、Type I - Non-phenolicTyPe 11 - Phenolic2. APPLICABLE OLXJJWENTS2.1 Government publications. The fol1owing documents, of the issues ineffect on date of invitation for bids or request for proposal, form a part ofthis specification to the extent specified herein:Federal SpecificationsQQ-A-2!W4 - Alumin
4、um Al1oy 2024, P1ate and SheetQQ-A-250/5 - Aluminum Alloy AlClad 2024, Plate andQQ-A-250/l2 - Aluminum Al1oy 7075, P1ate and SheetQQ-M-44 - Magnesium Alloy Plate and Sheet (Az31b)QQ-PA$l6 - PIsting, Cadmium (Electrodeposited)TT-L-32 - Lacquer, Cellulose Nitrate, Gloss,forAircraft Usel-r-P-1757 - Pri
5、mer COating, Zinc Chromate, LowMoisture-SensitivitySheetFSC 6850II Provided by IHS Not for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444BTT-T-291 -PPP-B-636 -PPP-C-96 -PPP-D-729 -PPP-P-704 -.Thinner; Paintl Mineral Spirits, Regular andOdorlessBoxes, Shipping, Fib
6、erboardCans, Metal, 28 Gage and LighterOrums, Shipping and Storage, Steel 55 Gallon(208 Liters)Pail, Metal (Shipping, Steel, 1 Through _12Gallon)Federa1 StandardsFEO-STO-313 - Material Safety Oata Sheets, Preparation andthe Submission ofFEIJ-STD-595 - Colors(Activities outside the Federal Government
7、 may obtain copies of Federalspecifications, standards, and commercial item descriptions, as outlined underGeneral Information in the Index of Federal Specifications, Standards andCommercial Item Descriptions. The Index, which includes cumulative bimonthlysupplements as issued, is for sale on a subs
8、cription basis by theSuperintendent of 00cuments, U.S. Government Printing Office, Washington, OC20402.(Single copies of this specification, and other Federal specifications andcommercial item descriptions required by activities outside the FederalGovernment for bidding purposes are available withou
9、t charge from GeneralServices Administration Business Service Centers in Boston, MA; few York, NY;Philadelphia PA; Washington, DC; Atlanta, GA; Chicago, IL; Kansas City, MO;Fort Worth, TX; Houston, TX; Denver, CO; San Francisco, CA; Los Angeles, CA;and Seattle, WA.(Federal Government activities may
10、obtain copies of Federal standardizationdocuments and the Index of Federal SPecifications, Standards; and cOMneCCialItem Descriptions from established distribution points in their agencies.)Military Specifications,MIL-M-3171 - MagnesiurnAlloy, Processes for Pretreatmentand Prevention of Corrosion on
11、MIL-A-8625 , Anodic Coatings for Aluminum and AluminumAl10YSMiL-T-9046 - Titanium and Titanium Al10Y, Sheet, Strip andP1ateMIL-P-23377 - Primer Coating, Epoxy Polyamide, Chemical andSolvent ResistantMIL-L-35078 - Loads, Unit, Preparation of NonperishableSubsistence Items, General Specification forMI
12、L-C-83286 - Coating, Urethane, Aliphatic Isocyanate, forAerospace Applications2.-.Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444L3Military StandardsMIL-STD-105 - Sampling Procedures and Tables forInspection by AttributesMIL-STO-129 - Marking
13、 for Shipment and Storage(Copies of military specifications and standards, required by contractorsin connection with specific procurement functions should be obtained frum theprocuring activity or as directed by the contracting officer. )Code of Federal Regulationsfor oh:CFR, Title 49, 100-199 - Tra
14、nsportationCode of Federal Regulations (CFR) and the Federal Register (FR) areon a subscription basis b.vthe Suerintendent of Oocuments. U.S.Government Printing Office, Washinton, OC” 20402. . When indicated,jreprints.of certain regulations may be obtained from the Federal agency responsible forissu
15、ance thereof. )2.2 Other publications. The following documents form a part of thisspecification to the extent specified herein. Unless a specific issue isidentified, the issue in effect on date of invitation for bids or request forproposal shal1 apply.American Society for Testinq and Materials (PSTM
16、) StandardsASTM A 109 - Steel, Carbon, Cold-Rolled StripASTM O 56 - Flash Point by Tag Closed TesterASTM O 97 - Pour Point of Petroleum Oi1sASTM O 605 - Magnesium Silicate “PigmentASTM 08Ztl -. Chemical Analysis of Soaps Containing SyntheticDetergentsASTM F 483 - Total Immersion Corat;s for copies s
17、hould be addressed to the Anerican TruckingTraffic Department, 1616 P Street, N.kl.;41ashingtonOC20036.) “UniforfnClassification Cormnittee,AgentUniform Freight Classification Rules.3Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444B(Applicatio
18、n for copies should be addressed to the Uniform ClassificationConmittee, Room 1106, 222 Riverside Plaza, Chicago, IL 60606.)3. REQUIREMENTSspec;+;ca$;il;?;i?”The cleaning compound furnished under thise a product which is qualified for listing on theapplicahle qualified products 1ist at the time set
19、for opening of bids (see4.3 and 6.3).3.2. Material. The formulation of the cleaning compound shall beoptional w-manufacturer, but the material shal1 conform to therequirements specified herein.3.2.1 Toxicity. The cleaning compound shall have no adverse effect onthe health of personnel when used for
20、its intended purpose. Questionspertinent to this effect shall be referred by the procuring activity to theappropriate medical service who wil1 act as adviser to the procuringactivity. The manufacturer shall certify that the cleaning compound containsno substance known to be toxic to the user under n
21、ormal conditions of use (see4.3.3).3.3 Chemical and physical properties.3.3.1 Phenolic content.3.3.1.1 Phenolic (Phenols and cresols) content (type 1). The type Icleaning compound, when tested as specified in 4.5.1, shal1 contain less than0.01 percent by weight of phenolic material.3.3.1.2 Cresol co
22、ntent (type 11). The type 11 cleaning compound, whentested as specified in 4.5.1, shal1 contain not less than 12 percent nor morethan 25 percent by weight of cresol material.3.3.1.3 Phenol content (type 11). The type II cleaning compound, whentested as specified in 4.5.1, shall contain less than 3.0
23、 percent by weightphenol (C6H50H).of3;3.2 Free alkali. The cleaning compound, when tested as specified in4.5.2, shall contain no free alkali.3.3.3 Volatile matter. When the cleaning compound is tested as specifiedin 4.5.3, the volatile matter shal1 not exceed 10.0 percent.The cleaning compound, when
24、 tested in the closed cuas s$iewshall have a flash point of not ,ess than 43C (llOF.4Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444B3.3.5 Pour point. When the cleaning compound is tested as specified in4.5.5, the pour point shall not exceed
25、2C (35”F).3.3.6 Form. The cleaning compound shal1 be a 1iquid at roomtemperature-en exposed as specified in 4.5.6, stirring the cleaningcompound shal1 readilY dissolve any surface skin which may have formed.3.3.7 Volubility in mineral spirits. When tested as specified in 4.5.7,the cJeaning compound
26、shal1 dissolve readilY, be clear and show no evidence ofseparation or undissolved matter.3.3.8 Volubility in hard water. When tested as specified in 4.5.8, thecleanina comoound shal1 readilV dissolve or emulsify and show no evidence ofemulsio breakdown such as sep9 Emulsion stability. When tested as
27、cleaning compound shal1 form an emulsion whichsolvent 1ayer or other evidence of breakdown.creamy top layer shal1 be permissible.or ol phase. The floating outspecified in 4.5.9, theshows no free oi1, clearCreaming or floating out of a3.3.10 Cleaning perfonnance. When tested as specified in 4.5.10, t
28、hecleaning compound shal1 remove oi1 and carbon with no visible evidence ofsoil, soap film or other residue.3.3.11 Total imnersion corrosion. When tested as specified in 4.5.11,the cleaning compound shal1 not show evidence of corrosion nor cause a weightchange in any test panel specimen greater than
29、 that listed in Table VI.3.3.12 Effects on acrylic base plastic (type I only). The type Icleanng compound, when tested as specified in 4.5.12, shall cause no crazing,cracking or other kinds of attack on acrylic base plastic.3.3.13 Effect on lacquered surfaces (type I only). The type I cleaningcomoou
30、nd. when tested as sueclfled in 4.5.13. shall cause no “oennanentsoftenin,loss of gloss, discoloration, bleeding or any filmirregularity onlacquered surfaces.The cleaning compound, when tested as specifiedin 4?!; sits original condition. .-3.3.15 Storaqe stability. The cleaning compound, after stora
31、ge assnecified in 4.5.15. shall be stable to the extent that it shal1 not rewireagitation prior to use. lhere shall be no evidence of layer formation,gelation or heavy precipitation.5Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444BI 3.4 Workm
32、anship. The ingredient materials shall be assembledprocessed to producea homogeneous1iquid cleaning compound free ofmaterial.I 4. QUALITY ASSURANCE PROVISIONSandforeign4.1 Responsibility for inspection. Unless otherwise specified in.thecontract, the contractor is responsible for the performance ofal
33、1 inspectionrequirements as specified herein. Except as otherwise specified in thecontract, the contractor may use his own or any other facilities suitable forthe performance of the inspection requirements specified herein, unlessdisapproved by the Government. The Government reserves the right to pe
34、rformany of the inspections set forth in the specification where such inspectionsare deemed necessary to assure that supplies and services conform toprescribed requirements.4.2 Classification of examinations and tests. The examinati.onsand testsof the solvent soluble cleaning compound shal1 be class
35、ified as follows:(a) Qualification inspection (see 4.3).(b) Quality conformance inspection (see 4.4).4.2.2 Inspection conditions. Unless otherwise specified, al1examinations and tests shal1 be conducted at 21 to 27C (70 to 81F).4.3 Qualification inspection. The qualification inspection shall consist
36、of al1 the examinations and tests specified herein.4.3.1 Retention of qualification. In order to retain qualification of aproduct approved for 1isting on the qualified products list (QpL), themanufacturer shal1 verify by certification to the qualifying activity that themanufacturers product complies
37、 with the requirements of this specification.The time of periodic verification by certification shall be in two-yearintervals from the date of original qualification. The Government reservesthe right to re-examine the qualified product whenever deemed necessary todetermine that the product continues
38、 to meet any or all of the specificationrequirements.4.3.2 Qualification samples. The qualification sample shall consist ofone gallon of each type of cleaning compound for which qualification isdesired. Samples shal1 be forwarded to the Cormnander,Naval Air DevelopmentCenter, Warminster, PA 18974, A
39、lTN: Director, Aircraft and Crew SystemsTechnology Directorate, Code 60622. Samples shall be plainlyProvided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444Bidentified by securely attached durable tags with the following information:Sample for qualifi
40、cation inspectionCleaning Compound, Solvent Soluble, Grease GnulsifyingManufacturers formula numberDate compoundedManufacturers nameBatch or lot numberSubmitted by (name) (date) for qualification inspection in accordancewith the requirements of P-C-444B under authorization of (referenceauthorizing l
41、etter) (see 6.3).4.3.3 Inspection report. The manufacturer shal1 submit a report, induplicate, to accompany the qualification inspection sample. This reportshal1 include the results of the manufacturers tests, reportedquantitatively, where applicable, in the units specified for al1 of therequirement
42、s specified herein, except storage stabi1ity. Tests not conducteddue to lack of special test facilities or materials shall be so noted in thereport. Material safety data sheets (see 3.2.1) shal1 be prepared inaccordance with FED-STD-313. One copy of each shall be forwarded to thequalifying laborator
43、y, the preparing activity of this specification and to theactivity specified in 6.5. In addition, the manufacturer shal1 submit acomplete statement of the formulation including the chemical name and weightpercent of each ingredient.4.4 Quality conformance inspection. The quality conformance inspecti
44、onshal1 consist of al1 the examinations and tests specified in table I.TABLE I. Quality conformance inspection CharacteristicsPhenolic ContentFree alkaliVolatile matterFlash pointFormVolubility in mineral spiritsSolubiIity in hard waterEmulsion stabilityTotal itmnersioncorrosionEffect on acrylic pla
45、stic (tYPe 1)Effect on lacquered surface (type II)ParaqraphRequirement3.3.13.3.23.3.33.3.43.3.63.3.73.3.83.3.93.3.113.3.123.3.13Test4.5.1.24.5.24.5.34.5.44.5.64.5.74.5.84.5.94.5.114.5.124.5.13Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-P-C-444B4.
46、4.1 Lot formation. A lot shall consist of all the cleaning ccmpoundproduced by one manufacturer, at one .P1ant, from the samemat.erals, and underessentially the same conditions provided .the operation is continuous and does $not exceed 24 hours. In the event the process is a batch operation, each. I
47、 batch shall constitute a lot (see 6.4).4.4.2 Sampling for tests. Quality conformance test samples shal1 beselected in accordance with table II. Unless otherwise specified, two1-gallon composite samples, consisting of equal parts of the sample unitselected, shall be subjected to the”tests in table I
48、. The sample shall beclearly identified by the manufacturers formula number as specified in4.3.2. The manufacturer shall furnish with each lot a certificate to theeffect that the material has been processed in the same manner and degreeusing the same base ingredients as the approved qualification sa
49、mple. The lotshal1 be unacceptable if a sample fails to meet any of the test requirements.TPBLE II. Net contentLot size (containers)up to 5051 - 500501 -35,00035,001 and overSample size (containers)578114.4.3 Examination of enditems. The contents of each container shal1 beexamined for the defects listed in table III. The sample size shall be inaccord
