1、Designation: D1000 10D1000 17Standard Test Methods forPressure-Sensitive Adhesive-Coated Tapes Used forElectrical and Electronic Applications1This standard is issued under the fixed designation D1000; the number immediately following the designation indicates the year oforiginal adoption or, in the
2、case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope*Scope
3、1.1 These test methods cover procedures for testing pressure-sensitive adhesive-coated tapes to be used as electrical insulation.These tapes are classified as follows:1.1.1 Class 1Non-elastomeric backings made from materials such as:Paper, flat or creped,Fabric, uncoated or coated,Cellulose ester fi
4、lms,Polyethylene terephthalate (polyester) films,Fluorocarbon polymer films,Composite filament films,Polyamide films,Polyimide films, andCombinations thereof.1.1.2 Class 2Elastomeric backings that are characterized by both high stretch and substantial recovery. These backings aremade from materials
5、such as:Vinyl chloride and co-polymers,Vinylidene chloride and co-polymers, andPolyethylene and co-polymers.1.2 Test laminates of Class 1 and Class 2 backings according to Class 1 test methods.1.3 The procedures appear in the sections indicated below and in alphabetical order:Adhesion Strength to St
6、eel and Backing at Room Temperature 46 53Adhesion Strength to Steel and Backing at Low Temperatures 46 53Bond Strength After Solvent Immersion 110 115Breaking Strength and Elongation at Room Temperature 37 45Breaking Strength and Elongation at Low Temperatures 37 45Conditioning 6 8Curling and Twisti
7、ng 140 146Dielectric Breakdown Voltage 83 90Effect of Accelerated Aging on High-Temperature Tapes 97 103Flagging 66 76Flammability 104 109Hazards/Precautions 3Insulation Resistance at High Humidity 91 96Length of Tape in a Roll 28 36Oil Resistance 116 122Puncture Resistance 123 128Resistance to Acce
8、lerated Aging (Heat and Moisture) 129 139Sampling 4Specimen Preparation 5Thermosetting Properties 77 82Thickness 21 27Unwind Force at Room Temperature 54 65Unwind Force at Low Temperatures 54 65Width 11 201 These test methods are under the jurisdiction ofASTM Committee D09 on Electrical and Electron
9、ic Insulating Materials and are the direct responsibility of SubcommitteeD09.07 on Flexible and Rigid Electrical Insulating Materials.Current edition approved Jan. 1, 2010July 1, 2017. Published February 2010July 2017. Originally approved in 1948. Last previous edition approved in 20092010 asD1000D1
10、000 10.09. DOI: 10.1520/D1000-10.10.1520/D1000-17.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible to adequately depict all changes accura
11、tely, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor D
12、rive, PO Box C700, West Conshohocken, PA 19428-2959. United States1NOTE 1These procedures apply to both Class 1 and Class 2 tapes except as noted above.1.4 This is a firetest response standard.fire-test response standard (see Section 104).1.5 The values stated in SI units are the standard, unless ot
13、herwise noted. If a value for measurement is followed by a valuein inch-pound or English units in parentheses, it is likely that the second value maywill only be approximate and it is forinformation only. The first stated value is the preferred unit.NOTE 2These test methods are similar to IEC 604543
14、, but may differ sometimes in some details.1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibilityof the user of this standard to establish appropriate safety and health practices and determine the applicability of regulator
15、ylimitations prior to use. For specific hazards see Section 3.1.7 This international standard was developed in accordance with internationally recognized principles on standardizationestablished in the Decision on Principles for the Development of International Standards, Guides and Recommendations
16、issuedby the World Trade Organization Technical Barriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2A167A666 Specification for Stainless and Heat-Resisting Chromium-Nickel Steel Plate, Sheet, and StripAnnealed orCold-Worked Austenitic Stainless Steel Sheet, Strip, Plate, and
17、 Flat Bar (Withdrawn 2014)D149 Test Method for Dielectric Breakdown Voltage and Dielectric Strength of Solid Electrical Insulating Materials atCommercial Power FrequenciesD257 Test Methods for DC Resistance or Conductance of Insulating MaterialsD295 Test Methods for Varnished Cotton Fabrics Used for
18、 Electrical InsulationD374D374/D374M Test Methods for Thickness of Solid Electrical Insulation (Metric) D0374_D0374MD1711 Terminology Relating to Electrical InsulationD3487 Specification for Mineral Insulating Oil Used in Electrical ApparatusD5032 Practice for Maintaining Constant Relative Humidity
19、by Means of Aqueous Glycerin SolutionsE691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method2.2 IEC Standard:IEC 60454-3 Specification for Pressure-Sensitive Adhesive Tapes for Electrical Purposes33. Hazards3.1 The following specific substances are flammabl
20、e liquids. Do not use them in the vicinity of open flames or electricalcontacts: acetone (see 50.1 and 94.1), heptane (see 50.1 and 94.1), and toluene (see 70.6).They must be stored in closed containers,and it is imperative to clean apparatus in a well-ventilated area.3.2 As toluene is a toxic subst
21、ance, use toluene only where adequate ventilation is provided and in such manner as to avoid anyabsorption through the skin (see 70.6).3.3 WarningIt is possible that lethal voltages will be present when conducting test methods which evaluate electricalproperties. It is essential that the test appara
22、tus, and all associated equipment electrically connected to it, be properly designedand installed for safe operation. Solidly ground all electrically conductive parts that any person might come in contact with duringthe test. Provide means for use, at the completion of any test, to ground any parts
23、which: were at high voltage during the test; havethe potential to acquire an induced charge during the test; or have the potential to retain a charge even after disconnection of thevoltage source. Thoroughly instruct all operators in the proper way to conduct tests safely. When making high voltage t
24、ests,particularly in compressed gas or in oil, it is possible that the energy released at breakdown will be suffcient to result in fire,explosion, or rupture of the test chamber. Design test equipment, test chambers, and test specimens so as to minimize the possibilityof such occurrences and to elim
25、inate the possibility of personal injury.SAMPLING4. Sample and Specimen Requirements4.1 The producer and consumer shall agree upon the number of rolls selected. Unless otherwise specified a minimum of threerolls per lot shall be selected.4.2 For sampling purposes, a lot consists of identifiable mate
26、rials of the same type, manufactured in one production run andoffered for delivery at the same time.2 For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Doc
27、ument Summary page on the ASTM website.3 Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http:/www.ansi.org.International ElectrotechnicalCommission, 446 Main St., Worcester, MA 01608, http:/www.iec.ch.D1000 1724.3 All test methods in this
28、standard are intended to produce a test value for a single roll. Any reference to averaging ofmeasurements refers to the averaging of measurements on a single roll and not to the average of all sample rolls.4.4 See Table 1 for a summary of standard requirements for the number of test specimens to se
29、lect from each sample roll, thenumber of test measurements to make per test specimen, and the value to be reported.4.5 Include in every report the complete identification of the tape tested.SPECIMEN PREPARATION5. Test Specimen Preparation5.1 Place any roll of tape to test on a freely revolving mandr
30、el. Except for determination of length of tape in a roll, remove anddiscard a minimum of three layers before removing tape for preparation of test specimens.5.2 Remove sufficient length of tape, at the rate of approximately 50 mm/s (2 in./s), to provide the specimens required for alltests. Cut the t
31、ape with a sharp razor blade or scissors, unless otherwise specified. Place the tape on a smooth clean surface,adhesive side up, or suspend it from one end in free air. Protect the adhesive surface from dust. Do not allow the adhesive surfaceto contact the operators fingers or other foreign objects.
32、Allow flexible specimens to relax for at least two minutes. From this tapematerial, prepare specimens as required in the individual test methods. See also Table 1.5.3 Use test specimens that are the width of the tape as received, if possible. If it is necessary to prepare narrower specimensas prescr
33、ibed in the test method, use extreme care since hand trimming has the potential to materially affect the test results. Tworecommended procedures are (1) to slit the specimen with a sharp razor blade free of nicks while the specimen is held down witha pattern of the desired width, or (2) to slit with
34、 mounted parallel sharp razor blades free of nicks to the desired width.CONDITIONING6. Terminology6.1 Definitions:6.1.1 conditioning, nthe exposure of a material to the influence of a prescribed atmosphere for a stipulated period of time oruntil a stipulated relation is reached between material and
35、atmosphere.7. Significance and Use7.1 The physical and electrical properties such as adhesion, elongation, breaking strength, and dielectric breakdown will varywith temperature and moisture content. Actual service results are influenced by these factors. In order that test methods yieldconsistent an
36、d reproducible results, control the temperature and moisture content of the sample or specimen.TABLE 1 Testing and ReportingTest Sec-tion Tests perSpecimenA Specimensper RollA ReportBWidth 14, 19 3 1 avgThickness 26 3 1 avgLength of tape in a roll 35 1 1 valueBreaking strength 44 1 3 avgElongation 4
37、4 1 3 avgAdhesion strength 52 1 3 avgUnwind forceFast rate of removal 64 1 1 valueSlow rate of removal 64 3 1 avgFlaggingClass 1 Tape 71 3 1 avgClass 2 Tape 75 1 3 avgThermosetting properties 81 1 3 avgDielectric breakdown voltage 89 3 3 avgInsulation resistance at high humidity 95 5 1 medEffect of
38、accelerated aging 102 3 2 avgFlammability 108 1 3 avgBond strength after solvent immersion 114 1 3 avgOil resistance 121 1 4 avgPuncture resistance 127 1 5 avgResistance to accelerated aging 129, 133 1 6 avgCurling and twisting 140 1 3 avgA When referee testing is involved, use an average of 5 deter
39、minations wherever1 or 3 are specified above.B Minimum and maximum values are also occasionally required when averagevalues are reported.D1000 1738. Conditioning for Room Temperature Measurements8.1 Condition all rolls of tape for a minimum of 24 h to a temperature of 23 6 5 C 5C (73 6 9 F) 9F) befo
40、re removingspecimens for test.8.2 Condition all test specimens for a period of 1 h in a controlled atmosphere at 23 6 5 C 5C (73 6 9 F) 9F) and 50 610 % relative humidity prior to testing.8.3 Unless otherwise specified, testing shall be conducted at 23 6 5 C 5C (73 6 9 F) 9F) and 50 6 10 % relative
41、humidity.8.4 For referee testing purposes, subject all sample rolls to a controlled laboratory temperature of 23 6 1C (73.4 6 1.8 F)1.8F) for a minimum period of 24 h before removing specimens for test.8.5 Unless otherwise specified, condition all referee test specimens for a period of 1 h in a cont
42、rolled laboratory atmosphereat 23 6 1C (73.4 6 1.8 F) 1.8F) and 50 6 2 % relative humidity.8.6 Unless otherwise specified, referee testing shall be conducted at 23 6 1C (73.4 6 1.8 F) 1.8F) and 50 6 2 % relativehumidity.9. Conditioning for Low Temperature Measurements9.1 Elastomeric backings of Clas
43、s 2 tapes have the potential to be subject to cold temperature tests. Condition elastomericbackings of Class 2 tapes for cold temperature tests by placing prepared specimens or rolls of tape in a cold room for at least 2h at the desired temperature (example temperatures: 10 C, 0 C, 10C, 0C, -10 C, -
44、18 C).-18C).10. Apparatus for Low Temperature Conditioning10.1 Cold room or cold chamber capable of maintaining the desired cold temperatures during testing.WIDTH OF TAPEMethod ASteel Ruler11. Apparatus11.1 A steel scale having divisions at 0.5 mm or 164-in. intervals.12. Test Specimens12.1 Select t
45、est specimens of approximately 450 mm (18-in.) lengths of tape taken from each sample roll in accordance with5.2 and conditioned in accordance with Section 8.13. Procedure13.1 Place the test specimen, after conditioning, without tension or pressure, adhesive side down on a hard smooth surface.Measur
46、e the width perpendicular to the edge with the steel scale at three approximately equally-spaced points along the length.14. Report14.1 Report the average width in millimetres or inches, plus the maximum and minimum, if specified.15. Precision and Bias15.1 This test method has been in use for many y
47、ears, but no statement of precision has been made and no activity is plannedto develop such a statement.15.2 This test method has no bias because the value for width is defined in terms of this test method.Method BCaliper16. Apparatus16.1 A pair of calipers with a scale length larger than width of t
48、he roll of tape, having divisions at 0.5-mm or 164-in. intervals.17. Test Specimen17.1 One roll of tape, conditioned in accordance with Section 8. Unless damaged, no outer layers need to be removed.18. Procedure18.1 The outer turns of the roll must have clean and sharp edges. Discard any damaged or
49、crushed edges. After conditioningthe roll of tape, place it on a table in a vertical position. Open the jaws of the calipers and slide them over the cut edges of thetape so that the scale shaft is parallel to the table. Close the caliper jaws slowly so as to just touch the sides of the tape roll. BeD1000 174careful not to crush the edges and keep the caliper jaws perpendicular to the edges of the tape. Measure the width perpendicularto the edges in mm (in.) to the nearest 0.5 mm (164 in.) a
