1、Designation: D 3310 00 (Reapproved 2006)Standard Test Method forDetermining Corrosivity of Adhesive Materials1This standard is issued under the fixed designation D 3310; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of l
2、ast revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method is intended to determine whether anadhesive material, cured or uncured, is corrosive to a metal. Itis
3、 a general test method intended to screen out those materialsthat give a visible sign of corrosion.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are provided forinformation purposes only.1.3 This standard does not purport to address all of thesa
4、fety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D 907 Terminology of Adhesives
5、G15 Terminology Relating to Corrosion and CorrosionTesting3. Terminology3.1 DefinitionsDefinitions of terms in this test methodmay be found in Terminologies D 907 and G15.3.1.1 corrosivity, nthe tendency to cause corrosion.4. Summary of Test Method4.1 The metal of interest is enclosed in a glass con
6、tainerwith the adhesive material. The containers are stored intemperature-controlled ovens at various temperatures with andwithout water present.4.2 Controls, glass jars containing samples (strips) of thesame metal with and without water but no adhesive stored inthe same oven for comparison.5. Signi
7、ficance and Use5.1 This test method is a subjective test in that determina-tions of degree of corrosivity is based upon a visual inspectionfor a green discoloration or other evidence of corrosion.6. Apparatus6.1 Glass Jars, wide-mouth, with screw cap (8-oz size). Thecap liner shall be TFE- or FEP-fl
8、uorocarbon.6.2 Forced Draft Circulating Air Oven, capable of main-taining 71 6 2C (160 6 4F); 93 6 2C (200 6 4F); 12162C (250 6 4F). Other temperatures can be used withagreement of interested parties.6.3 Open Glass Jars or Cups, 1-oz size.6.4 Metal or metals being checked for corrosion.7. Procedure7
9、.1 Place 5 to 10 g of the adhesive in a small glass jar withthe metal being evaluated partly embedded in the adhesive.Place this small uncovered jar in a large jar. Screw the cap ofthe large jar tightly in place. Then place the jar in the oven ata temperature as specified in 6.2.NOTE 1Here metal is
10、exposed during cure rather than after cure.7.2 Same as 7.1, except place a small jar half filled withdistilled water in a large jar with the jar containing adhesiveand metal. However, do not use water above 71C.7.3 Same as 7.1 and 7.2, except cure the adhesive inaccordance with manufacturers instruc
11、tions before placing itin the large jar.NOTE 2Hot-melt or air-dried materials are considered to be in thecured state.8. Control8.1 Place a metal specimen similar to the specimen beingevaluated in a screw cap jar with no adhesive. Tighten thescrew cap in place, and place the jar in the same oven at t
12、hesame time as the specimen being evaluated. Store another largejar with a control metal specimen and including a small jar withwater in it in the oven in a similar manner.1This test method is under the jurisdiction of ASTM Committee D14 onAdhesives and is the direct responsibility of D14.80 on Meta
13、l Bonding Adhesives.Current edition approved Oct. 1, 2006. Published October 2006. Originallyapproved in 1974. Last previous edition approved in 2000 as D 3310 00.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book
14、 of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.9. Cleanliness9.1 Clean the jars and covers so that no foreign matter ispresent.9.2
15、 Abrade the metal strips that are exposed with 600-gritmesh emery paper to achieve a shiny surface.9.3 Expose the metals with corrosion preventive treatmentsas treated.10. Observations10.1 Periodically, make observations of the control andexposed specimens. Note the following information on a scaleo
16、f five as follows:10.1.1 (1) Exposed sample less tarnished than control,10.1.2 (2) Exposed sample same as control,10.1.3 (3) Exposed sample slightly worse than control,10.1.4 (4) Exposed sample significantly worse than control,10.1.5 (5) Exposed sample badly corroded,10.1.6 Where possible remove the
17、 adhesive so that thecorrosive condition in the embedded area may be reported.11. Report11.1 Report the following information:11.1.1 Identification of the adhesive evaluated and curecycle.11.1.2 Identification of the metal in detail (that is, specificalloy, temper and special treatment such as cold
18、working, etc).11.1.3 Description of the condition of test (that is, whetherexposure was during cure, after cure and with or without waterbeing present).11.1.4 Storage time and temperature.11.1.5 Degree of corrosion on scale of five after convenientintervals. (If corrosion is rapid and severe initial
19、 report may beafter 1 h. Otherwise, observations may be made and recordedafter 1, 3, and 7 days.)11.1.6 Any unusual aspect of corrosion such as pitting,cracking, and adhesive cure inhibition, etc.12. Precision and Bias12.1 Precision and bias statements can not be established,because the test is subj
20、ective. The degree of corrosion presenton the test specimen is determined by visual comparison tocontrols, a judgment evaluation. This is not a practical basis forstatements of this nature.13. Keywords13.1 adhesives; corrosion; corrosivity; moisture; waterASTM International takes no position respect
21、ing the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This stan
22、dard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM Internatio
23、nal Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.
24、This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D 3310 00 (2006)2
