1、Designation: D5966 10D5966 12Standard Test Method forEvaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine1This standard is issued under the fixed designation D5966; the number immediately following the designation indicates the year oforiginal adoption or, in the case of re
2、vision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.INTRODUCTIONThis test method is continually undergoing changes to reflect refinements in procedure, obsoles-ce
3、nce of parts or reagents. These changes or updates, as well as general information regarding the testmethod, are issued as information letters by the ASTM Test Monitoring Center (TMC). Copies ofinformation letters pertaining to the test method may be obtained by contacting the ASTM TestMonitoring Ce
4、nter.2The test method can be used by any properly equipped laboratory, without assistance of anyone notassociated with that laboratory. However, TMC provides reference oils and an assessment of the testresults obtained on those oils by the laboratory. By this means, the laboratory will know whether
5、theiruse of the test method gives results statistically similar to those obtained by other laboratories.Furthermore, various agencies require that a laboratory utilize the TMC services in seekingqualification of oils against specifications. For example, the U.S. Army imposes such a requirement,in co
6、nnection with several military lubricant specifications.Accordingly, this test method is written for use by laboratories which utilize the TMC services.Laboratories that choose not to use these services may simply ignore those portions of the testprocedure which refer to the TMC.1. Scope Scope*1.1 T
7、his engine lubricant test method is commonly referred to as the Roller Follower Wear Test. Its primary result, rollerfollower shaft wear in the hydraulic valve lifter assembly, has been correlated with vehicles used in stop-and-go delivery serviceprior to 1993. It is one of the test methods required
8、 to evaluate lubricants intended to satisfy the API CG-4 performance category.This test has also been referred to as the 6.2 L Test.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.2.1 ExceptionsWhere there is no direct S
9、I equivalent, such as pipe fittings, thermocouple diameters, and NPT screw threads.Also, roller follower wear is measured in mils.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibilityof the user of this standard to establi
10、sh appropriate safety and health practices and determine the applicability of regulatorylimitations prior to use.1.4 Table of Contents:SectionScope 1Referenced Documents 2Terminology 3Summary of Test Method 4Significance and Use 5Reagents 7Guidelines on Substitution 7.1Apparatus 61 This test method
11、is under the jurisdiction of ASTM Committee D02 on Petroleum Products and Lubricants and is the direct responsibility of Subcommittee D02.B0.02on Heavy Duty Engine Oils.Current edition approved May 1, 2010Dec. 1, 2012. Published August 2010March 2013. Originally approved in 1996. Last previous editi
12、on approved in 20092010 asD596609.10. DOI: 10.1520/D5966-10. 10.1520/D5966-12.2 ASTM Test Monitoring Center, 6555 Penn Ave., Pittsburgh, PA 15206-4489. This edition incorporated revisions contained in all Information Letters through No. 06-1.This document is not an ASTM standard and is intended only
13、 to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versio
14、nof the standard as published by ASTM is to be considered the official document.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1Preparation of Apparatus 8New Engine Prep
15、aration 8.1Installation of Auxiliary Systems andMiscellaneous Components8.2Test Procedure 9Description of Test Segments and Organizationof Test Procedure Sections9.1Engine Parts Replacement 9.2Engine Starting Procedure 9.3Normal Engine Shutdown Procedure 9.4Emergency Shutdown Procedure 9.5Unschedule
16、d Shutdown and Downtime 9.6New Engine Break-In 9.7Pretest Procedure 9.8Fifty-Hour Steady State Test 9.9Periodic Measurements 9.10Oil Sampling and Oil Addition Procedures 9.11End of Test (EOT) Procedure 9.12Calculation and Interpretation of Test Results 10Environment of Parts Measurement Area 10.1Rol
17、ler Follower Shaft Wear Measurements 10.2Oil Analysis 10.3Assessment of Test Validity 10.4Final Test Report 11Reporting Calibration Test Results 11.1Report Forms 11.2Interim Non-Valid Calibration Test Summary 11.3Severity Adjustments 11.4Precision and Bias 12Precision 12.1Precision Estimate 12.2Bias
18、 12.3Keywords 13ANNEXESGuidelines for Test Part Substitution or Modification Annex A1Guidelines for Units and Specification Formats Annex A2Detailed Specifications of Apparatus Annex A3Calibration Annex A4Final Report Forms Annex A5Illustrations Annex A6Kinematic Viscosity at 100C Procedure for theR
19、oller Follower Wear TestAnnex A7Enhanced Thermal Gravimetric Analysis (TGA)Procedure for Soot MeasurementAnnex A8Sources of Materials and Information Annex A9APPENDIXESPC-9 Reference Diesel Fuel Properties Appendix X1Diagnostic Data Review Appendix X22. Referenced Documents2.1 ASTM Standards:3D86 Te
20、st Method for Distillation of Petroleum Products at Atmospheric PressureD93 Test Methods for Flash Point by Pensky-Martens Closed Cup TesterD97 Test Method for Pour Point of Petroleum ProductsD130 Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip TestD235 Specification
21、for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)D287 Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer Method)D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)D446 Specifications
22、 and Operating Instructions for Glass Capillary Kinematic ViscometersD482 Test Method for Ash from Petroleum ProductsD524 Test Method for Ramsbottom Carbon Residue of Petroleum ProductsD613 Test Method for Cetane Number of Diesel Fuel OilD664 Test Method for Acid Number of Petroleum Products by Pote
23、ntiometric TitrationD976 Test Method for Calculated Cetane Index of Distillate FuelsD1319 Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator AdsorptionD2274 Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)D2500 Test Method for Cloud
24、 Point of Petroleum Products3 For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.D5966 122D2622 Test Method for Su
25、lfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence SpectrometryD2709 Test Method for Water and Sediment in Middle Distillate Fuels by CentrifugeD4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density MeterD4175 Terminology Relating to Petrol
26、eum, Petroleum Products, and LubricantsD4485 Specification for Performance of Active API Service Category Engine OilsD4737 Test Method for Calculated Cetane Index by Four Variable EquationD5185 Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils
27、 andDetermination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)D7422 Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel EngineE29 Practice for Using Significant Digits in Test Data to Determine Conformanc
28、e with Specifications2.2 American National Standards Institute (ANSI):4MC96.1 Temperature Measurement Thermocouples3. Terminology3.1 Definitions:3.1.1 blowby, nin internal combustion engines, that portion of the combustion products and unburned air/fuel mixture thatleaks past piston rings into the e
29、ngine crankcase during operation.3.1.2 BTDC (before top dead center), nused with the degree symbol to indicate the angular position of the crankshaft relativeto its position at the point of uppermost travel of the piston in the cylinder.3.1.3 calibrate, vto determine the indication or output of a de
30、vice (e.g., thermometer, manometer, engine) with respect to thatof a standard.3.1.4 candidate oil, nan oil which is intended to have the performance characteristics necessary to satisfy a specification andis tested against that specification. D41753.1.5 engine oil, na liquid that reduces friction or
31、 wear, or both, between the moving parts within an engine; removes heat,particularly from the underside of pistons; and serves as a combustion gas sealant for piston rings.3.1.5.1 DiscussionIt may contain additives to enhance certain properties. Inhibition of engine rusting, deposit formation, valve
32、 train wear, oiloxidation and foaming are examples. D41753.1.6 light-duty, adj in internal combustion engine operation, characterized by average speeds, power output, and internaltemperatures that are generally much lower than the potential maximums. D44853.1.7 light-duty engine, n in internal combu
33、stion engine types, one that is designed to be normally operated at substantiallyless than its peak output. D44853.1.8 lubricant, nany material interposed between two surfaces that reduces friction or wear, or both, between them. D41753.1.9 lubricating oil, na liquid lubricant, usually comprising se
34、veral ingredients, including a major portion of base oil andminor portions of various additives. D41753.1.10 reference oil, nan oil of known performance characteristics, used as a basis for comparison.3.1.10.1 DiscussionReference oils are used to calibrate testing facilities, to compare the performa
35、nce of other oils, or to evaluate other materials (suchas seals) that interact with oils. D41753.1.11 used oil, nany oil that has been in a piece of equipment (for example, an engine, gearbox, transformer, or turbine),whether operated or not. D41753.1.12 wear, nthe loss of material from a surface, g
36、enerally occurring between two surfaces in relative motion, and resultingfrom mechanical or chemical action, or a combination of both. D74224. Summary of Test Method4.1 A pre-assembled GM V8 diesel test engine is installed on a test stand and operated for 50 h.4.2 The test engine operating condition
37、s are generally more extreme than typical service operating conditions. These conditionsprovide high soot loading and accelerated roller follower shaft wear while maintaining correlation with wear levels found in thefield.4 Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
38、 4th Floor, New York, NY 10036.D5966 1234.3 At the end of the test, the performance of the engine oil is determined by measuring the level of wear on the roller followershafts.5. Significance and Use5.1 This test method is used to determine the ability of an engine crankcase oil to control wear that
39、 can develop in the field underlow to moderate engine speeds and heavy engine loads.torques. Side-by-side comparisons of two or more oils in delivery van fleetswere used to demonstrate the field performance of various oils. The specific operating conditions of this test method weredeveloped to provi
40、de correlation with the field performance of these oils.5.2 This test method, along with other test methods, defines the minimum performance level of the Category API CG-4 forheavy duty diesel engine lubricants. Passing limits for this category are included in Specification D4485.5.3 The design of t
41、he engine used in this test method is not representative of all modern diesel engines.This Consider this factor,along with the specific operating conditions used to accelerate wear, shall be considered when extrapolating test results.6. Apparatus6.1 A listing and complete description of all apparatu
42、s used in the test is found in Annex A3. Information concerningprocurement of apparatus can be found in Appendix X1.7. Reagents7.1 Guidelines on SubstitutionNo substitutions for the reagents listed in 7.1.1-7.1.3 are allowed.7.1.1 Cleaning Solvent, For cleaning parts, use only mineral spirits meetin
43、g the requirements of Specification D235, Type II,Class C forAromatic Content (volume fraction (0 to 2) %), Flash Point (61C, min) and Color (not darker than +25 on the SayboltScale or 25 on Pt-Co Scale. (WarningCombustible. Health hazard.) Obtain a Certificate of Analysis for each batch of solventf
44、rom the supplier.7.1.2 Engine CoolantThe engine coolant is a solution of demineralized water whichthat has less than 0.03 g/kg dissolvedsolids and an ethylene glycol based anti-freeze mixed at the following concentration70 % antifreeze and 30 % water by volume.7.1.2.1 Demineralized Water, is used as
45、 a generic term to describe pure water. Deionized or distilled water may also be usedas long as the total dissolved solids content is less than 0.03 g/kg.7.1.3 FuelApproximately 600 L of PC9 Reference Diesel Fuel are required for each test.5 (WarningCombustible. Healthhazard. Use adequate safety pro
46、visions.)7.1.3.1 Fuel Batch AnalysisEach fuel shipment does not need to be analyzed upon receipt from the supplier. However,laboratories are responsible for periodic checks for contamination. Any analysis results for parameters tested should be within thetolerances shown on Form 20. If any results f
47、all outside the tolerances shown on Form 20, the laboratory should contact the TestMonitoring Center (TMC)2 for help in resolving the problem.7.1.3.2 Fuel Batch StorageThe fuel should be stored in accordance with all applicable safety and environmental regulations.7.1.4 Break-In OilApproximately 8 k
48、g of break-in oil are necessary for new engine break-in. Break-in oil is defined as anySAE 15W-40, API CG-4 quality oil.7.1.5 Non-Reference Test OilA minimum of 20 kg of new oil are required to complete the test. A25 kg sample of new oil isnormally provided to allow for inadvertent losses.7.1.6 Cali
49、bration Test OilA22A 22 kg sample of reference oil is provided by the TMC for each calibration test.8. Preparation of Apparatus8.1 New Engine PreparationParagraphs 8.1.1 through 8.1.88.1.7 describe preparations that are only performed on a newengine before conducting the new engine break-in.8.1.1 Engine Front Cover InstallationInstall the front cover to the front of the engine block with the gasket supplied andtorque all bolts to 40 Nm.8.1.2 Oil Sump Drain LocationInstall a drain in the sump as described in A3.9.3.7.8.1.3 Glow Plug ReplacementRe