ASTM D6544-2011 3125 Standard Practice for Preparation of Textiles Prior to Ultraviolet (UV) Transmission Testing《紫外线(UV)透射试验前纺织品制备的标准操作规程》.pdf

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1、Designation: D6544 11Standard Practice forPreparation of Textiles Prior to Ultraviolet (UV)Transmission Testing1This standard is issued under the fixed designation D6544; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of

2、last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers standardized exposures to launder-ing, simulated sunlight, and chlorinated pool water to whichclo

3、th, labeled as ultraviolet-(UV) protective, must be exposedprior to testing for UV transmission.1.2 This practice leads to measurement of the residual levelof UV-protection in fabrics or garments labeled as sun- orUV-protective, after exposure to conditions that relate to abouttwo years of seasonal

4、use. The UV transmission measurementsmay be done in accordance with AATCC Test Method 183using fabrics prepared in accordance with this practice. Thismeasurement may be used in support of a label statementregarding UV protection.1.3 The values stated in SI units are to be regarded as thestandard. Th

5、e values given in parentheses are for informationonly.1.4 This standard does not purport to address the safetyconcerns, if any, associated with its use. It is the responsibilityof the user of this standard to establish appropriate safety andhealth practices and determine the applicability of regulat

6、orylimitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D123 Terminology Relating to TextilesD2905 Practice for Statements on Number of Specimens forTextiles3D3938 Guide for Determining or Confirming Care Instruc-tions for Apparel and Other Textile ProductsD6544 Practice for Preparati

7、on of Textiles Prior to Ultra-violet (UV) Transmission TestingD6603 Guide for Labeling of UV-Protective TextilesE122 Practice for Calculating Sample Size to Estimate,With Specified Precision, the Average for a Characteristicof a Lot or Process2.2 AATCC Test Methods and Documents:4AATCC 16E Colorfast

8、ness to LightAATCC 135 Dimensional Changes in Automatic HomeLaundering of Woven or Knit FabricAATCC 162 Colorfastness to Water: Chlorinated PoolAATCC 172 Colorfastness to Non-chlorine Bleach in HomeLaunderingAATCC 183 Transmittance or Blocking of ErythemallyWeighted Ultraviolet Radiation through Fab

9、ricsGlossary of AATCC Standard Terminology3. Terminology3.1 DefinitionsFor definitions of other textile terms usedin this practice, refer to Terminology D123 and the Glossary ofAATCC Standard Terminology.4. Summary of Practice4.1 This practice directs the exposure of cloth, labeled asUV-protective,

10、to conditions of laundering, simulated sunlight,and chlorinated pool water generally known to affect UVtransmittance.4.2 This practice directs selection and sequencing of expo-sure conditions for UV-protective fabrics and garments.5. Significance and Use5.1 The significance of this practice is that

11、cloth, labeled asUV-protective, which will ultimately be submitted for UVtransmittance testing will be in a state that simulates theircondition at the end of two years of normal seasonal use.Therefore, the UV-protection level ultimately placed on a labelestimates the maximum UV transmittance of the

12、garmentfabric during a two-year life cycle.6. Sampling and Test Specimens6.1 Primary Sampling UnitConsider rolls or bolts offabric, or cartons of garments to be the primary sampling unit,as applicable.1This practice is under the jurisdiction ofASTM Committee D13 on Textiles andis the direct responsi

13、bility of Subcommittee D13.65 on UV Protective Fabrics andClothing.Current edition Jan. 1, 2011. Published February 2011. Originally approved in2000. Last previous edition approved in 2007 as D6544 00(2007). DOI: 10.1520/D6544-11.2For referenced ASTM standards, visit the ASTM website, www.astm.org,

14、orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Withdrawn. The last approved version of this historical standard is referencedon www.astm.org.4Available from American Association

15、 of Textile Chemists and Colorists(AATCC), P.O. Box 12215, Research Triangle Park, NC 27709, http:/www.aatcc.org.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.6.1.1 Take the number of primary sampling units from eachlot, shipment,

16、or production run in accordance with PracticeE122.6.2 Laboratory Sampling Unit:6.2.1 Take the number of laboratory sampling units from theprimary sampling unit in accordance with Practice E122.6.2.2 Rolls or Bolts of FabricTake from each primarysampling unit one full-width piece of fabric that is ab

17、out 1 m(1 yd) in length along the selvage (machine direction), afterremoving a first 1-mm length. For narrow fabrics, a longersample length may be required to meet the test specimenrequirements.6.2.3 GarmentsTake from each primary sampling unitone entire garment. For small garments, such as children

18、s,where sufficient material is not available to meet the three testspecimens requirement, take a pair of garments and treat as onesampling unit.6.3 LaunderingUnless exempt from laundering, launderthe laboratory sampling unit or a section of it that is at least 380by 380 mm (15 by 15 in.) using expos

19、ure conditions asdescribed in 8.1. If the laboratory sampling unit does not havethe minimum 380-mm dimension, then take a section that is atleast 1450 cm2(225 in.2). For small samples, it may benecessary to seal the edges to prevent raveling during launder-ing.6.4 Test SpecimensAs test specimens, ta

20、ke from eachlaboratory sampling unit at least three specimens of each fabrictype in accordance with Practice D2905.6.4.1 For simulated sunlight and chlorinated water testing,cut test specimens 125 by 180 mm (5 by 7 in.).6.4.2 Cut specimens representing a broad distribution di-agonally across the wid

21、th of the laboratory sampling unit.Ensure specimens are free of folds, creases, or wrinkles. Avoidgetting oil water, grease, and so forth on the specimens whenhandling. For printed fabrics, ensure that all colors in thepattern are contained in the test specimen.6.4.3 For fabric widths 125 mm (5 in.)

22、 or more, take nospecimen closer than 25 mm (1 in.) from the selvage edge.6.4.4 For fabric widths less than 125 mm (5 in.) use theentire width for specimens.6.4.5 When a garment is the laboratory sampling unit, taketest specimens from various areas of the garment. Avoid takingspecimens along seams.6

23、.4.6 When the required minimum of three specimenscannot be taken from one garment as might be the case withchildrens garments, then take two specimens from each of twogarments, the pair of garments constituting a laboratory sam-pling unit.6.4.7 When a garment is made from different fabrics, atleast

24、three test specimens are required of each fabric thatcovers 10 % or more of the body surface covered by thegarment.7. Procedure7.1 For garments other than swimwear and fabrics intendedto be made into garments other than swimwear, launder 40times using the exposure conditions described in 8.1 and the

25、ntake specimens from these fabrics and expose to 100 AATCCFading Units of simulated sunlight in accordance with theconditions described in 8.2.7.2 For swimwear and fabric intended for swimwear, laun-der 40 times in accordance with the exposure conditionsdescribed in 8.1. Then take specimens from the

26、 launderedfabrics or garments and expose those specimens to 100AATCCFading Units of simulated sunlight in accordance with theconditions described in 8.2 and then to chlorinated water inaccordance with the conditions described in 8.3.7.3 Garments and fabrics intended for use in garments otherthan swi

27、msuits that are sold with the expectation they will notbe laundered (such as disposable or limited-use garments forpesticide application) need only be exposed to simulatedsunlight.8. Exposure Conditions8.1 Laundering:8.1.1 Conditions of ExposureHand washing or automaticmachine washing, wash water te

28、mperature, agitation cycle inautomatic laundering, drying method and temperature if ma-chine drying, and use of bleach must be those that will beconveyed to the consumer on the care label attached to thefabric/garment. Those conditions should have been determinedby following Guide D3938.8.1.1.1 Care

29、 procedures determined in accordance withGuide D3938 may be modified when it is established that thoseprocedures increase the UV-transmittance of the fabric.8.1.1.2 Follow one of the washing and drying procedures inAATCC 135 or AATCC 172 that matches the care instructionsof the fabric or garment.8.1

30、.2 The specimens to be laundered may be garments,one-yard lengths of fabric, or areas of fabric having minimumdimensions of 380 by 380 mm (15 by 15 in.) or whenapplicable 1450 cm2(225 in.2).8.2 Simulated Sunlight:8.2.1 A xenon-arc lamp must be used which limits the testconditions to those described

31、in AATCC 16 E.8.2.2 For directions for preparing the specimens to beexposed to UV radiation, refer to the test preparation section ofTest Method AATCC 16E noting that only two specimens arerequired and that the specimens are to be cut from thelaundered specimens and omitting the section which refers

32、 tothe testing of yarns, not fabrics.8.3 Chlorinated Pool Water:8.3.1 For preparation of the specimens to be exposed tochlorinated pool water, refer to the procedure section of TestMethod AATCC 162. Ignore the reference to colored speci-mens as white specimens may also be exposed to chlorinatedpool

33、water conditions.8.3.2 The specimens are those previously laundered andexposed to simulated sunlight.8.3.3 For the exposure procedure, follow the procedureprovided in the procedure section of Test Method AATCC 162with the exception that the chlorine concentration in milligramsper kilogram should be

34、adjusted so it is equal to the unit massof the fabric specimen.D6544 1129. Report9.1 Report that the specimens were prepared for UV trans-mission testing as directed in this practice. Describe thematerial or product samples.9.2 Specific Conditions of Each Exposure:9.2.1 Use Table X1.1 to report all

35、applicable informationabout laundering conditions.9.2.2 Use Table X1.2 to report all applicable informationabout simulated sunlight exposure.9.2.3 Use Table X1.3to report all applicable chlorinatedpool water exposure conditions.9.3 Deviations from Specified Conditions:9.3.1 Report any deviation from

36、 laundering conditionsspecified in AATCC 135 into Table X1.1.9.3.2 Report any deviation from AATCC Test Method 16E or the performance of the reference standard used in TableX1.29.3.3 Report any deviation from AATCC 162 in Table X1.3.10. Keywords10.1 care labeling; chlorinated pool water effects; lau

37、nder-ing effects; simulated sunlight exposure effects; sunbathing;swimwear; UV-protective fabrics; UV transmission testingANNEX(Mandatory Information)A1. UV PROTECTIVE TEST METHODSINTRODUCTIONManufacturers and producers of UV protective textile materials or products, or both, must be awareof the pro

38、per existing standards and test methods to meet published voluntary standards for labelingUV protective clothing for the United States.A1.1 There are three published voluntary standards:A1.1.1 ASTM D6544 Practice for Preparation of TextilesPrior to Ultraviolet (UV) Transmission TestingA1.1.2 ASTM D6

39、603 Guide for Labeling of UV Protec-tive TextilesA1.1.3 AATCC 183 Transmittance or Blocking ofErythemcally Weighted Ultraviolet Radiation Through FabricsA1.2 To summarize at a high level, these three standardsare used in conjunction with one another to develop the properUPF values to properly label

40、products as “UV Protective.”A1.2.1 Evaluate UV transmission of original specimen(“unprepared”) or “laundered once” specimen usingAATCC 183. The value reported is theAATCC 183 UPF value.A1.2.2 Refer to ASTM D6544 to determine the exposureconditions depending on the product end use. Section 7 liststhr

41、ee options for exposure conditions. Exposure conditionsmay reference the following test methods and reflect a combi-nation of multiple exposure conditions following these testmethods:A1.2.2.1 ASTM D3938A1.2.2.2 AATCC 16A1.2.2.3 AATCC 135A1.2.2.4 AATCC 162A1.2.2.5 AATCC 172A1.2.3 After subjecting the

42、 specimens to the specifiedexposure conditions of ASTM D6544, evaluate UV transmis-sion using AATCC 183. This specimen is referred to as the“prepared-for-testing” specimen, based on the end use of thegarment/fabric.A1.2.4 Refer to ASTM D6603 for additional calculationsthat need to be performed on th

43、e values obtained fromAATCC 183.A1.2.5 Classification for labeling the UPF value are out-lined in ASTM D6603, Section 8.D6544 113APPENDIX(Nonmandatory Information)X1. EXPOSURE REPORT FORMSX1.1 See Table X1.1, Table X1.2, and Table X1.3.TABLE X1.1 Laundering Exposure Report FormOperators name_Date_Sa

44、mple identification_Check exposures used:Machine Cycle: Washing temperature, C (F)ADrying procedure:BNormal /cotton/sturdy 27 6 3(806 5) Tumble cotton studyDelicate 41 6 3 (105 6 5) Tumble, delicatePermanent press 49 6 3 (120 6 5) Tumble, permanent press60 6 3 (140 6 5) LineDripScreenADeviations fro

45、m washing machine conditions as described in Table II AATCC 135-1995.BDeviations from drying settings in Table III AATCC 135-1995.TABLE X1.2 Chlorinated Pool Water Exposure FormOperators name_Date_Sample Identification_Deviations from the procedure in AATCC 162:D6544 114ASTM International takes no p

46、osition respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsib

47、ility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to

48、ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-

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