1、Designation: D7932 17Standard Specification forPrinted, Pressure-Sensitive Adhesive Labels for Use inExtreme Distribution Environments1This standard is issued under the fixed designation D7932; the number immediately following the designation indicates the year oforiginal adoption or, in the case of
2、 revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification provides a standard means to test andmeasure performance characteristics of
3、printed, pressure-sensitive adhesive labels for containers, particularly containersto be used in extreme distribution environments (for example,hazardous materials labels, aerospace, military containers). Forthe purposes of this specification, an extreme distributionenvironment is one in which it ca
4、n be reasonably expected toexperience direct exposure to deteriorating chemicals, weather,elevated/cold temperatures, and other environmental andphysical elements for an extended period of time.1.2 UnitsThe values stated in either SI units or inch-pound units are to be regarded separately as standar
5、d. Thevalues stated in each system may not be exact equivalents;therefore, each system shall be used independently of the other.Combining values from the two systems may result in non-conformance with the standard.1.3 This standard does not purport to address all of thesafety concerns, if any, assoc
6、iated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety, health, and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accor-dance with internationally rec
7、ognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2A666 Specification
8、for Annealed or Cold-Worked AusteniticStainless Steel Sheet, Strip, Plate, and Flat BarD374/D374M Test Methods for Thickness of Solid Electri-cal InsulationD975 Specification for Diesel Fuel OilsD996 Terminology of Packaging and Distribution Environ-mentsD1000 Test Methods for Pressure-Sensitive Adh
9、esive-Coated Tapes Used for Electrical and Electronic Applica-tionsD2244 Practice for Calculation of Color Tolerances andColor Differences from Instrumentally Measured ColorCoordinatesD3611 Practice for Accelerated Aging of Pressure-SensitiveTapesD3951 Practice for Commercial PackagingD4332 Practice
10、 for Conditioning Containers, Packages, orPackaging Components for TestingD4814 Specification for Automotive Spark-Ignition EngineFuelD6210 Specification for Fully-Formulated Glycol Base En-gine Coolant for Heavy-Duty EnginesD6252/D6252M Test Method for PeelAdhesion of Pressure-Sensitive Label Stock
11、s at a 90 AngleG195 Guide for Conducting Wear Tests Using a RotaryPlatform Abraser2.2 Department of Defense Standards:3MIL-STD-810 Environmental Engineering Considerationsand Laboratory TestsMIL-STD-2073-1 Standard Practice for Military PackagingMIL-DTL-83133 Turbine Fuel, Aviation, Kerosene Type,JP
12、-8 (NATO F-34), NATO F-35, and JP-8+100 (NATOF-37)2.3 Society of Automotive Engineers Standards:4SAE J183 Engine Oil Performance and Engine ServiceClassificationSAE J300 Engine Oil Classification1This specification is under the jurisdiction of ASTM Committee D10 onPackaging and is the direct respons
13、ibility of Subcommittee D10.14 on Tape andLabels.Current edition approved Sept. 1, 2017. Published September 2017. Originallyapproved in 2014. Last previous edition approved in 2014 as D7932 14. DOI:10.1520/D7932-17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM
14、 Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Copies of these documents are available from DLA Document Services,Building 4/D, 700 Robbins Ave., Philadelphia, PA 19111-5094, http:/quicksearc
15、h.dla.mil.4Copies of these documents are available from Society ofAutomotive Engineers(SAE), 400 Commonwealth Dr., Warrendale, PA 15096-0001.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in a
16、ccordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.12.4 Other:ISO/IEC 15415 Info
17、rmation Technology Automatic Iden-tification and Data Capture Techniques Bar Code PrintQuality Test Specification Two Dimensional Symbols5ISO/IEC 15416 Information Technology Automatic Iden-tification and Data Capture Techniques Bar Code PrintQuality Test Specification Linear Symbols5ISO/IEC 15426-1
18、 Information Technology AutomaticIdentification and Data Capture Techniques Bar CodeVerifier Conformance Specification Part 1: Linear Sym-bols5ISO/IEC 15426-2 Information Technology AutomaticIdentification and Data Capture Techniques Bar CodeVerifier Conformance Specification Part 2: Two-Dimensional
19、 Symbols5ANSI MH10.8.1 Linear Bar Code then subtract to obtain the labelthickness only.11.5 Abrasion ResistanceExposure to abrasion shall beconducted as specified in Guide G195. Label samples shall beattached to the test plates such that maximum barcode printedarea will be in the abrasion path. Labe
20、l samples do not have tobe adhered to test plates using adhesive for the purposes of thistest. Label samples shall be abraded at a speed of 60 cycles/minusing the CS-10 or CS-10F abrading wheel and a 250 g weighton each wheel. Vacuum level shall be set to 100 %. Durationshall be 500 cycles for Type
21、I and 100 cycles for Type II labels.Following completion, label samples shall meet the minimumprint quality requirements of 11.2.11.5.1 Hot and Cold ConditioningFor the purpose ofdetermining abrasion resistance at hot and cold atmosphericconditions, label samples shall be conditioned in the desert a
22、ndcryogenic conditioning atmospheres, respectively, described inTable 1 of Practice D4332 for a period of not less than 24 hbefore testing. The abrasion shall be conducted in standardatmospheric conditions as soon as possible after removal of thelabel sample from the desert or cryogenic conditioning
23、 atmo-sphere. The maximum permissible time from conditioningchamber removal to start of abrasion shall be 3 min.11.6 High TemperatureExposure to high temperature shallbe conducted in accordance with MIL-STD-810, Method501.6, Procedure I, Storage. The temperature cycle shall be inaccordance with indu
24、ced conditions of Table 501.6-III and theexposure duration shall be seven 24-h cycles.FIG. 2 Type II Test SequenceD7932 17611.7 Low TemperatureExposure to low temperature shallbe conducted in accordance with MIL-STD-810, Method502.6, Procedure I, Storage. The temperature shall be inaccordance with D
25、esign Type C3, Severe Cold, and theexposure duration shall be 4 h. A ramp up and ramp down timeof12 h each, independent of 4 h test time, shall be used totransition the label test specimen from ambient to cold andagain from cold to ambient.11.8 RainExposure to rain shall be conducted in accor-dance
26、with MIL-STD-810, Method 506.6, Procedure II, Exag-gerated Rain. Label test specimen standoff distance shall be amaximum of 19 in. (48 cm) and exposure duration shall be 40min. The label test specimen shall be positioned in the verticalY-direction and rain spray shall be in the horizontal X-directio
27、nto avoid pooling effects.11.9 Salt FogExposure to salt fog shall be conducted inaccordance with MIL-STD-810, Method 509.6. A 5 6 1 % saltsolution shall be used. The label test specimen shall be exposedto alternating 24-h periods of salt fog exposure and dryingconditions for four 24-h cycles.11.10 B
28、lowing DustExposure to blowing dust shall beconducted in accordance with MIL-STD-810, Method 510.6,Procedure I.11.11 HumidityExposure to humidity shall be performedin accordance with MIL-STD-810, Method 507.6, inducedconstant high humidity Cycle B1. Exposure duration shall be45 days.11.12 Freeze/Tha
29、wExposure to a freeze/thaw cycle shallbe conducted in accordance with MIL-STD-810, Method524.1, Procedure III, Rapid Temperature Change. The tempera-ture range shall be from a minimum of 14F to at least 72F.The exposure shall consist of three cycles and shall begin andfinish in the warm condition.11
30、.13 Accelerated AgingExposure to accelerated agingconditions shall be conducted in accordance with PracticeD3611. The label test specimen shall be exposed to anenvironment of 66C (150F) and 80 % relative humidity for aperiod of 96 h (4 days).11.14 Contamination by FluidsExposure to contamina-tion by
31、 fluids (chemical resistance) shall be conducted inaccordance with MIL-STD-810, Method 504.2, Procedure II.The application method shall be by immersion only.11.14.1 The contamination sequence shall be as follows: 1 himmersion time, visual inspection, 7 h immersion time, dryingtime not to exceed 24 h
32、, examination in accordance with 11.2and 11.3 (see 10.6).11.14.2 Test chemicals and respective adhesion require-ments shall be as described in Table 3.11.14.3 Several test chemicals, such as gasoline, may par-tially or fully evaporate before completion of 8 h immersiontime. In this case do not refil
33、l or reapply any additional testchemical to the label test sample and allow sequence toproceed as specified in 11.14.1.11.15 Solar RadiationExposure to solar radiation (sun-shine) shall be conducted in accordance with MIL-STD-810,Method 505.6, Procedure II. Exposure duration shall be fifty-six 24-ho
34、ur cycles. The label test specimen shall be examinedand photographed after every 10 cycles to document anychanges. A solar test system utilizing xenon arc or metal halidebulbs with proper filters is recommended to meet the spectralirradiance requirements.12. Report12.1 Report fully all the steps tak
35、en. At a minimum, thereport should include:12.1.1 Reference to this specification.12.1.2 Description of product (for example, manufacturer,backing material, adhesive, batch/lot number(s), etc.) andshipping unit.12.1.3 Test plan.12.1.4 Assurance levels and rationale.12.1.5 Number of samples tested.12
36、.1.6 Conditioning used.12.1.7 Acceptance criteria.12.1.8 Variation from recommended procedures.12.2 Military ShipmentsIn addition to 12.1.2 12.1.8, thecomplete report shall include the following:12.2.1 Party, other than contractor, performing testing.12.2.2 Testing facility used, other than contract
37、ors.12.2.3 Government representative witnessing testing.13. Certification13.1 When specified in the purchase order or contract (see6.1.7) the purchaser shall be furnished with a certificationstating that the samples representing each lot of labels havebeen tested and inspected as directed in this sp
38、ecification andthe requirements have been met.14. Rejection14.1 Material that fails to conform to the requirements ofthis specification may be rejected. Rejection shall be reportedto the producer or supplier promptly in writing.15. Preparation for Delivery15.1 Unless otherwise specified in the purch
39、ase order orcontract (see 6.1.10), labels shall be packaged and packed inaccordance with Practice D3951. Such packaging shall ensurearrival at destination in satisfactory conditions and shall beacceptable to the carrier used at the lowest rate.15.2 Military ShipmentsWhen specified (see 6.1.10) ship-
40、ments to the Department of Defense shall be packaged andpacked in accordance with MIL-STD-2073-1 at the levelsspecified in the purchase order or contract.16. Keywords16.1 labels; pressure-sensitive adhesives; shipping contain-ers; distribution environmentsD7932 177ASTM International takes no positio
41、n respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.
42、This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM I
43、nternational Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address sho
44、wn below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 178
