1、BRITISH STANDARDBS EN ISO 13503-2:2006Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operationsICS 75.100g49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g
2、44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58A1:2009+National forewordThis British Standard is the UK implementation of EN ISO 13503-2:2006+A1:2009. It is identical to ISO 13503-2:2006, incorporating amendment 1:2009. It su
3、persedes BS EN ISO 13503-2:2006 which is withdrawn.The start and finish of text introduced or altered by amendment is indicated in the text by tags. Tags indicating changes to ISO text carry the number of the ISO amendment. For example, text altered by ISO amendment 1 is indicated by !“.The UK parti
4、cipation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemical and natural gas industries, to Subcommittee PSE/17/-/3, Drilling and completion fluids and well cements.A list of organizations represented on this subcommittee can be obtain
5、ed on request to its secretary. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. BS EN ISO 13503-2:2006+A1:2009This British Sta
6、ndard was published under the authority of the Standards Policy and Strategy Committee on 30 November 2006 BSI 2010Amendments/corrigenda issued since publicationDate Comments 31 January 2010 Implementation of ISO amendment 1:2009 with CEN endorsement A1:2009ISBN 978 0 580 70414 7EUROPEAN STANDARDNOR
7、ME EUROPENNEEUROPISCHE NORMEN ISO 13503-2November 2006ICS 75.100English VersionPetroleum and natural gas industries - Completion fluids andmaterials - Part 2: Measurement of properties of proppants usedin hydraulic fracturing and gravel-packing operations (ISO13503-2:2006)Industries du ptrole et du
8、gaz naturel - Fluides decompltion et matriaux - Partie 2: Mesurage desproprits des matriaux de soutnement utiliss dans lesoprations de fracturation hydraulique et de remplissage degravier (ISO 13503-2:2006)Erdl- und Erdgasindustrie - Komplettierungsflssigkeitenund -materialien - Teil 2: Messung der
9、Eigenschaften vonSttzmaterialien zum Einsatz bei hydraulischenFraktionierungs- und in Kiespackungsvorgngen (ISO13503-2:2006)This European Standard was approved by CEN on 22 September 2006.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giv
10、ing this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official version
11、s (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus
12、, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EU
13、ROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2006 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN ISO 13503-2:2006: EForeword This document (EN ISO 13503-2:2006) has been
14、prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“, the secretaria
15、t of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2007, and conflicting national standards shall be withdrawn at the latest by May 2007. According to the CEN/CENELEC
16、 Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
17、Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of ISO 13503-2:2006 has been approved by CEN as EN ISO 13503-2:2006 without any modifications. Foreword to amendment A1 This document (EN ISO 13503-2:2006/A1
18、:2009) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural
19、gas industries” the secretariat of which is held by AFNOR. This Amendment to the European Standard EN ISO 13503:2006 shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2010, and conflicting national standards shall be
20、withdrawn at the latest by May 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations
21、, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands
22、, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 13503-2:2006/Amd 1:2009 has been approved by CEN as a EN ISO 13503-2:2006/A1:2009 without any modification. BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006
23、+A1:2009Reference numberISO 13503-2:2006(E)INTERNATIONAL STANDARD ISO13503-2First edition2006-11-01Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations Industries du ptrole et du
24、 gaz naturel Fluides de compltion et matriaux Partie 2: Mesurage des proprits des matriaux de soutnement utiliss dans les oprations de fracturation hydraulique et de remplissage de gravier BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006+A1:2009ii iiiContents Page Foreword. v Introduction . vi 1 Sc
25、ope . 1 2 Normative references . 1 3 Abbreviations 1 4 Standard proppant sampling procedure 2 4.1 General. 2 4.2 Particle segregation 2 4.3 Equipment . 2 4.4 Number of required samples Bulk 4 4.5 Sampling Bulk material 5 4.6 Sampling Bagged material 5 5 Sample handling and storage 5 5.1 Sample reduc
26、tion 5 5.2 Sample splitting 5 5.3 Sample and record retention and storage . 5 6 Sieve analysis . 6 6.1 Purpose 6 6.2 Description 6 6.3 Equipment and materials . 6 6.4 Procedure 6 6.5 Calculation of the mean diameter, median diameter and standard deviation 7 6.6 Sieve calibration . 9 7 Proppant spher
27、icity and roundness . 11 7.1 Purpose 11 7.2 Description 12 7.3 Apparatus capability. 12 7.4 Procedure 12 7.5 Alternate method for determining average sphericity and roundness . 13 8 Acid solubility . 13 8.1 Purpose 13 8.2 Description 13 8.3 Equipment and materials . 14 8.4 Procedure 14 9 Turbidity t
28、est . 15 9.1 Purpose 15 9.2 Description 16 9.3 Equipment and materials . 16 9.4 Equipment calibration 16 9.5 Procedure 16 10 Procedures for determining proppant bulk density, apparent density and absolute density 17 10.1 Purpose 17 10.2 Description 17 10.3 Bulk density. 17 10.4 Apparent density. 19
29、10.5 Absolute density. 21 BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006+A1:2009iv 11 Proppant crush-resistance test . 21 11.1 Purpose 21 11.2 Description. 21 11.3 Equipment and materials . 22 11.4 Sample preparation. 22 11.5 Crush-resistance procedure 23 12 Loss on ignition of resin-coated propp
30、ant. 25 12.1 Objective 25 12.2 Apparatus and materials 25 12.3 Loss-on-ignition procedure for whole-grain proppant . 25 Annex A (informative) Formazin solution preparation 27 Bibliography .32 BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006+A1:2009Annex (informative) Proppant specifications . 28 vF
31、oreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a te
32、chnical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters
33、of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated
34、 to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible f
35、or identifying any or all such patent rights. ISO 13503-2 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. ISO 13503 consists of th
36、e following parts, under the general title Petroleum and natural gas industries Completion fluids and materials: Part 1: Measurement of viscous properties of completion fluids Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations Part 3: Testing of
37、 heavy brines Part 4: Procedure for measuring stimulation and gravel-pack fluid leakoff under static conditions Part 5: Procedures for measuring the long-term conductivity of proppants BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006+A1:2009vi Introduction This part of ISO 13503 is a compilation an
38、d modification of API RP 56 1, API RP 58 2and API RP 60 3. The procedures have been developed to improve the quality of proppants delivered to the well site. They are for use in evaluating certain physical properties used in hydraulic fracturing and gravel-packing operations. These tests should enab
39、le users to compare the physical characteristics of various proppants tested under the described conditions and to select materials useful for hydraulic fracturing and gravel-packing operations. The procedures presented in this part of ISO 13503 are not intended to inhibit the development of new tec
40、hnology, material improvements or improved operational procedures. Qualified engineering analysis and judgment are required for their application to a specific situation. In this part of ISO 13503, where practical, US Customary (USC) units are included in brackets for information. Annex A of this pa
41、rt of ISO 13503 is for information only. BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006+A1:20091Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations 1 Scope This part of ISO 1
42、3503 provides standard testing procedures for evaluating proppants used in hydraulic fracturing and gravel-packing operations. NOTE “Proppants” mentioned henceforth in this part of ISO 13503 refer to sand, ceramic media, resin-coated proppants, gravel-packing media and other materials used for hydra
43、ulic fracturing and gravel-packing operations. The objective of this part of ISO 13503 is to provide a consistent methodology and specifications for testing performed on hydraulic fracturing and/or gravel-packing proppants. 2 Normative references The following referenced documents are indispensable
44、for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ASTM E11-04, Standard Specification for Wire Cloth and Sieves for Testing Purposes 3 Abbreviations API
45、 American Petroleum Institute ASTM American Society for Testing and Materials ASG apparent specific gravity FTU formazin turbidity unit HCI hydrochloric acid HF hydrofluoric acid LOI loss on ignition NTU nephelometric turbidity unit !“! “BS EN ISO 13503-2:2006+A1:2009EN ISO 13503-2:2006+A1:20092 4 S
46、tandard proppant sampling procedure 4.1 General Before any sample is taken, consider what tests will be performed, as each test requires a different volume. It is very important that both the supplier and customer obtain the best representative sample possible. Unless the sample is truly representat
47、ive of a total shipment or container, testing and correlation with specifications/standards is very difficult. It is unlikely that sampling/testing methods in the field duplicate the producers system. The standard procedures included within this part of ISO 13503 are to assist in obtaining represent
48、ative samples. However, there are inherent variations associated with sampling, testing equipment and the procedures that can lead to inconsistent results. A sample that is representative of a truckload 23 000 kg (50 700 lb) or a railcar load 90 000 kg (198 000 lb) can be an initial source of wide v
49、ariation when making comparisons. All parties shall take care to insure uniform sampling. The customer and the supplier shall agree on sampling and testing methods/techniques. For the best representation, continuous sampling is ideal. Although many proppant suppliers utilize automatic sampling, it is usually impractical at the job site. If sampling is conducted while unloading a container or at the site, consideration should be given to the number or frequency of samples. If bulk containers are filled from a flowing st
