1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS EN ISO 13678:2012Petroleum and natural gasindustries Evaluation andtesting of thread compoundsfor use with casing, tubing, linepipe and drill stem elements(ISO 13678:2010)BS E
2、N ISO 13678:2012 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN ISO13678:2012. It is identical to ISO 13678:2010. It supersedes BS EN ISO13678:2009 which is withdrawn.The UK participation in its preparation was entrusted to TechnicalCommittee PSE/17/-/5, Casing
3、, tubing and drill pipe.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. The British Standards Institution 2012ISB
4、N 978 0 580 72301 8ICS 75.180.10Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and Strategy Committee on 31 January 2012.Amendments issued since publicationDate Text affectedEUROPEAN STAND
5、ARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13678 January 2012 ICS 75.180.10 Supersedes EN ISO 13678:2009English Version Petroleum and natural gas industries - Evaluation and testing of thread compounds for use with casing, tubing, line pipe and drill stem elements (ISO 13678:2010) Industries du ptro
6、le et du gaz naturel - valuation et essais des graisses pour filetage utilises pour les tubes de cuvelage, les tubes de production, les tubes de conduites et les lments de garnitures de forage (ISO 13678:2010)Erdl- und Erdgasindustrie - Beurteilung und Prfung von Gewindefetten zur Verwendung an Futt
7、er-, Steig- und Leitungsrohren und an Bohrgestngeteilen (ISO 13678:2010) This European Standard was approved by CEN on 3 December 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national
8、standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version
9、in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
10、 Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COM
11、IT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 13678:2012: EBS EN ISO 13678:2012EN ISO 13678:2012 (E) 3 Forew
12、ord The text of ISO 13678:2010 has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 13678:2012 by Technic
13、al Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorseme
14、nt, at the latest by July 2012, and conflicting national standards shall be withdrawn at the latest by July 2012. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any
15、 or all such patent rights. This document supersedes EN ISO 13678:2009. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denma
16、rk, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 13678:2010 has been
17、 approved by CEN as a EN ISO 13678:2012 without any modification. BS EN ISO 13678:2012ISO 13678:2010(E) ISO 2010 All rights reserved iiiContents Page Foreword iv Introduction.v 1 Scope1 2 Conformance .1 2.1 Dual citing of normative references 1 2.2 Units of measurement.1 3 Normative references2 4 Te
18、rms and definitions .2 5 Thread compound characteristics.3 5.1 Product characteristics.3 5.2 Physical and chemical characteristics4 6 Thread compound performance properties8 6.1 Small-scale test .8 6.2 Frictional properties8 6.3 Extreme surface contact pressure (gall resistance) properties for casin
19、g, tubing and line pipe .9 6.4 Fluid sealing properties for casing, tubing and line pipe .10 7 Quality assurance and control.10 8 Marking requirements.11 8.1 Marking.11 8.2 Labelling.11 Annex A (informative) API modified thread compound 12 Annex B (normative) Casing, tubing and line pipe reference s
20、tandard formulation.16 Annex C (normative) Penetration test 18 Annex D (normative) Evaporation test .19 Annex E (normative) Oil separation test 20 Annex F (normative) Application/adherence test21 Annex G (normative) Gas evolution test 22 Annex H (normative) Water leaching test.26 Annex I (informativ
21、e) Frictional properties test .29 Annex J (informative) Extreme surface contact pressure (galling) test for casing, tubing and line pipe .39 Annex K (informative) Fluid sealing test for casing, tubing and line pipe40 Annex L (informative) Corrosion inhibition tests 43 Annex M (informative) Compound
22、high-temperature stability test44 Bibliography45 BS EN ISO 13678:2012ISO 13678:2010(E) iv ISO 2010 All rights reservedForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Stan
23、dards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also t
24、ake part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees
25、is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibil
26、ity that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13678 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and
27、natural gas industries, Subcommittee SC 5, Casing, tubing and drill pipe. This third edition cancels and replaces the second edition (ISO 13678:2009), of which it constitutes a minor revision. It is the intent of ISO/TC 67 that the second and third editions of ISO 13678 both be applicable, at the op
28、tion of the purchaser, for a period of six months from the first day of the calendar quarter immediately following the date of publication of this third edition, after which period the second edition will no longer be applicable. BS EN ISO 13678:2012ISO 13678:2010(E) ISO 2010 All rights reserved vIn
29、troduction This International Standard is based on API RP 5A39, second edition, July 2003, with errata and inclusion of all clauses of API RP 7A11)13, first edition, November 1992, incorporated into Annex I. This International Standard specifies requirements and gives recommendations for the manufac
30、ture, testing and selection of thread compounds for use on casing, tubing, line pipe and drill stem elements based on the current industry consensus of good engineering practice. It is intended that the words casing and tubing apply to the service application, rather than to the diameter of the pipe
31、. The performance requirements of thread compounds for use with casing, tubing, line pipe, premium connections and rotary shouldered connections include: a) consistent frictional properties that allow both proper and uniform connection engagement; b) adequate lubrication properties to resist galling
32、 or damage of connection contact surfaces during make-up and breakout; c) adequate sealing properties for thread-type seal connections and/or not inhibiting the sealing properties of non-thread sealing connections (e.g. metal-to-metal seals, polytetrafluoroethylene seals, etc.) depending upon servic
33、e requirements; d) physical and chemical stability both in service and in expected compound storage conditions; e) properties that allow effective application to the connection contact surfaces in expected service conditions and environment. In addition, compounds for rotary shouldered connections p
34、rovide: lubrication of the connection members during make-up to achieve the proper axial bearing stress; an effective seal between connection shoulders to prevent wash-out by drilling fluids; more uniform distribution of circumferential bearing stress if shoulders are not parallel; resistance to add
35、itional make-up down hole. When evaluating the suitability of a thread compound, the user can define the service conditions and then consider field trials and field service experience in addition to laboratory test results. Appropriate supplementary tests can be utilized for specific applications wh
36、ich are not evaluated by the tests herein. The user and manufacturer are encouraged to discuss service applications and limitations of the compound being considered. Representatives of users and/or other third-party personnel are encouraged to monitor tests wherever possible. Interpolation and extra
37、polation of test results to other products, even of similar chemical composition, are not recommended. 1) Obsolete. Incorporated into this International Standard. BS EN ISO 13678:2012ISO 13678:2010(E) vi ISO 2010 All rights reservedTesting in compliance with this International Standard does not in i
38、tself ensure adequate thread compound/connection system performance in field service. The user has the responsibility of evaluating the results obtained from the recommended procedures and test protocols and determining whether the thread compound/connection system in question meets the anticipated
39、requirements of that particular field service application. BS EN ISO 13678:2012INTERNATIONAL STANDARD ISO 13678:2010(E) ISO 2010 All rights reserved 1Petroleum and natural gas industries Evaluation and testing of thread compounds for use with casing, tubing, line pipe and drill stem elements 1 Scope
40、 This International Standard provides requirements, recommendations and methods for the testing of thread compounds intended for use on threaded casing, tubing, and line pipe connections; and for thread compounds intended for use on rotary shouldered connections. The tests outlined are used to evalu
41、ate the critical performance properties and physical and chemical characteristics of thread compounds under laboratory conditions. These test methods are primarily intended for thread compounds formulated with a lubricating base grease and are not applicable to some materials used for lubricating an
42、d/or sealing thread connections. It is recognized that many areas can have environmental requirements for products of this type. This International Standard does not include requirements for environmental compliance. It is the responsibility of the end user to investigate these requirements and to s
43、elect, use and dispose of the thread compounds and related waste materials accordingly. 2 Conformance 2.1 Dual citing of normative references In the interest of world-wide application of this International Standard, Technical Committee ISO/TC 67 has decided, after detailed technical analysis, that c
44、ertain of the normative documents listed in Clause 3 and prepared by ISO/TC 67 or another ISO Technical Committee are interchangeable in the context of the relevant requirement with the relevant document prepared by the American Petroleum Institute (API), the American Society for Testing and Materia
45、ls (ASTM) and the American National Standards Institute (ANSI). These latter documents are cited in the running text following the ISO reference and preceded by “or”, for example “ISO XXXX or API YYYY”. Application of an alternative normative document cited in this manner will lead to technical resu
46、lts different from those obtained from the use of the preceding ISO reference. However, both results are acceptable and these documents are thus considered interchangeable in practice. 2.2 Units of measurement In this International Standard, data are expressed in both the International System (SI) o
47、f units and the United States Customary (USC) system of units. For a specific order item, it is intended that only one system of units be used, without combining data expressed in the other system. Products manufactured to specifications expressed in either of these unit systems shall be considered
48、equivalent and totally interchangeable. Consequently, compliance with the requirements of this International Standard as expressed in one system provides compliance with requirements expressed in the other system. For data expressed in the SI system, a comma is used as the decimal separator and a sp
49、ace as the thousands separator. For data expressed in the USC system, a dot (on the line) is used as the decimal separator and a space as the thousands separator. In the text, data in SI units are followed by data in USC units in parentheses. BS EN ISO 13678:2012ISO 13678:2010(E) 2 ISO 2010 All rights reserved3 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced d
