1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 28038 2013 2014 280382013 II , 1.092 . 1.22009 . -, . , , , 1 () - ( ) 2 ( 335) 3 , ( 25 2013 . 55-) : ( 3166) 004 97 ( 3166) 004 97 AM BY KG KZ MD - RU TJ 4 28 2013 . 310- 280382013 1 2014 . 5 6 02 IFU Recommendation No
2、. 2 Determination of Patulin, Revised in 2005 (International Federation of Fruit Juice Producers IFU) 6 2803889 - , . () - - . , , 2014 -, - 280382013 III , , , . ( ) : ( ). . V 280382013 1 Fruit and vegetable products. Methods for determination of micotoxin patulin 20140701 1 , : , , , , , - , ( )
3、: - ; - ( ). ( ) - 10 /3(1010-7%). - 10 /3, 1010-7%, - 75 /3, 7510-7%. 1 /3 110-7%. 2 : 572512003 ( ) . 1. 572522003 ( ) . 2. 12.1.00588 . - 12.1.00776 . . 12.1.01893 . - . 12.1.01979 . . - 8379 . . 177074 ( 104283, 478880) . -, , , . 260379 . . . . 311877 . . 280382013 2 416676 . . 420775 . 3-. 423
4、377 . . 555681 . 578978 . . 582378 . 2-. 584873 . . 595678 - . 655280 . . 670972 . 914780 . 929374 . 1202676 . 1830087 . 1981474 . 2001588 . 2049075 . . 2230076 . . 2533682 . , 2631384 . , 2667185 , . 2849890 . . 2922791 ( 835181) . . 1. - , 1 , , . (), - () . , , , , - . 3 -: 3.1 (mycotoxin patulin
5、): , , Penicillium, Aspergillus Byssochlamys; : 4-4H-2,3-2(6)-. 4 26313, 26671. 5 5.1 , - . 10 /3(1010-7%). 280382013 35.2 , , , , - 120 (), 0,03 , 0,06 . 500 0,01 . , 275 , 1 %; 10 . 230 25 . . 25336. 10 3 0,1 3. . - , , , - 250 2, , - 10 . 28498 0 100 1 . 1770: 1-50-2, 1-100-2; 4-100-2, 4-250-2, 4
6、-1000-2 4-2000-2; 1-10-0,1 1-20-0,1 . 1-2-2-1, 1-2-2-2, 1-2-2-5, 1-2-2-10 1-2-2-25 29227. 25336: -1-50 -1-150; -56-80 ; 250 3; -2-250; -100-14/23; -25-14/23. 25336 , 250 . 9147 230 2. 25336 50 3. . 12026 . 5556. 100160 100250 . 15 15 5 17 . (C7H6O4) 95 %. 20015 18300. 3118, . . 3- 4207, . ., 150 /3
7、( I). 2- 5823, . . ., 300 /3( II). 22300, . . . (). 2603, . . 5789, . . . 5848, . . . 95 %, 5 /3. 99 %, , , , 0,5 - 1 . 280382013 4 4233, . . 4166, , . . 20490, . ., 15 /3. 6709. 5956, . . . 99,5 % (C7H6O4), - 10,0 /3 - 5 %. , 5.4.4. , , 5.4.6 , , . , , , -. 5.3 5.3.1 () - . . 5 10 3 (9:1). 100 3. 10 3 (9:1), . (9 : 1), - . 20 3 - . (9:1), .
