GOST 32689 3-2014 Foods of plant origin Multiresidue methods for the gas chromatographic determination of pesticide residues Part 3 Determination and confirmatory tests《植物食品 利用气相色谱.pdf

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1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32689.3 2014 3 (EN 12393-3:2008, NEQ) 2015 32689.32014 II , - 1.092 . 1.2 2009 . -, . , , , 1 - ( ) 2 3 , (- 25 2014 . 45-2014) : ( 3166) 004 97 ( 3166) 004 97 AM BY KG RU TJ 4 19 2014 . 895- 32689.32014 - 1 2016 . 5 EN

2、12393-3:2008 Foods of plant origin Multiresidue methods for the gas chromatographic determination of pesticide residues Part 3: Determination and confirmatory tests ( . - . 3. - ) (NEQ) 6 - , . () - - . , , 2015 -, - 32689.3 2014 1 3 Foods of plant origin. Multiresidue methods for the gas chromatogr

3、aphic determination of pesticide residues. Part 3. Determination and confirmatory tests 2016 01 01 1 , () - . - . 2 - : 32689.12014 . - 1. 32689.22014 . - 2. - , 1 , - . (), - () . , , , , . 3 - - . . - , , (), , , - . , -, . 32689.32014 2 4 4.1 () 4.1.1 - , , , . . - , - , . . - - . - - , , . . 4.1

4、.2 24 , ; - . - . - ( ), - . . - . , , . , ( , -, , , .) , - . , (fused silica), 0,20 0,35 10 60 . 0,5 0,8 . *: - SE-30 ( OV-1, DB-1, CP Sil 5, BP-1, SPB-1 . .); - SE-54 ( DB-5, CP Sil 8, BP-5, SPB-5 .); - OV-17 ( OV-11, OV-22, SP-2250, DC-710, DB-608 . .); - DB-1301 ( DB-624); - DB-1701 ( OV-1701,

5、CP-Sil 19-CB, BP-10, SPB-7 . .); - OV-225 ( DB-225, SIL-43-CB, SPB-2330 . .); - WAX ( DB-WAX, CP-WAX-52-CB, Carbowax 20 M . .). 4.1.3 , , - (PTV). . 4.1.4 32689.1. 4.2 . ( 1,0 10,0 3 ), - , 32689.2, -. , . * . 32689.32014 3 4.3 . - , . - -. - . , - , . , . - 10 %. . -, , - . , - 70 % 110 % - 20 %. . 5 5.1 , - 1. , -, . , () - . : - - ; - . , . , - . -. . - . , -, ; , . , . . - , - . - . , , -. , - . 5.2 5.8 - . 32689.32014 4 5.2 - , - (M), - (. ). , - . - . - . - , - , - . , . (

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