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3、 2 - : 12.1.00588 . - 12.1.00776 . . - 12.1.01979*1 . . OIML R 76-12011 . - . 1. . 177074 ( 104283, 478880) . -, , , . ISO 36962013* . 583375 . . 1364778 . . 2631384 . , 2667185 , -. 2849890 . . 2922791 ( 835-181) . . 1. -* 1 12.1.0192009 - . . . *11 525012005 -. . 328002014 2 , 1 , - . (), - () . ,
4、 , , , . 3 - , , . - . 4 , , , 4.1 , 510-11 / 3 %, - , - 250 , , (200300) , - - 4.2 30 , 0,25 95 % -, 5 %- - 0,25 .* 14.2 , - (40100) 2 .4.3 , 100 /. 4.4 2-50-2 2-100-2 1770. 4.5 , , 0,5 % 0,25 %. 4.6 100, 500 3 - 1 % () , . 4.7 () 2 3, . 4.8 1,5 10 3 29227.4.9 , - 18 () , . 4.10 0,45 . 4.11 0 100 1
5、 28498.4.12 OIML R 76-1 150 - 0,001 . 4.13 , 400 g (-) , . 4.14 13647, . . . 4.15 N- (TMSI) C6H12N2Si, - 95 %. 4.16 N-N- (MSHFBA) CF3CF2CF2CON(CH3)Si(CH3)3, , 95 %. *1 Agilent DB-5MS . . 328002014 3 4.17 N- C4H6N2, 95 %. 4.18 () C12H22O11 . 4.19 5833, . . . 4.20 ISO 3696, 1- . , , , , - . 5 26313, 2
6、6671. 6 6.1 , , 15 400 g, 0,45 . - 11,2 % 5,5 %, 15 400 g, 0,45 . 6.2 5 % (2,5 0,0001) 50 3, 2/3 - . , . . 6.3 , - , (-, , ), - 5 % , - 5 % 6.3.1. 10 2 .6.3.1 . , 5 % - . m, , , 21105,0 X mXm , (1) X1 , , %; m1 , , ; X2 - , , %. . 328002014 4 6.3.2 25 /3 25 /3 - 5 %, 6.2. (0,025 0,0001) 100 3. - 5 %, . 10 3 100 3, 5 %. . 7 7.1 , - . 7.2 : - (25 5) ; - , (97 10); - , % (65 15); - , (50 5); - , (220 10). , , - . . 7.3 10 3 , 6.1, - , 0,05 3 ( 11,2 % 0,1 3 ( - 5,5 %) 2 3 - .
