GOST 32977-2014 Solid mineral fuel Determination of trace elements in ash by atomic absorption method《固体矿物燃料 采用原子吸收法测定痕量元素》.pdf

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1、 - , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)329772014, 1.092 . 1.22009 . , - . , , -, 1 - , , - ( ) , 52 (-)3 , (- 20 2014 . 71-) : ( 3166) 00497 ( 3166) 00497 BYKGRUTJ 4 21 2015 . 282- 329772014 - 1 2016 .5 ASTM D 36832011 StandardTest Method for Trace Elements in

2、 Coal and Coke Ash by Atomic Absorption ( - - ). , / - , . (en). , - , -. (MOD)6 - , - . () - . , , 2015 -, II 329772014 . , - - . - , , - . , , - . - - : , , , , , -, . ASTM D 3683. , - , ( 2 3). , , - 2 3 -. ASTM D 3683:- ;- , - ;- (250 150 ) , ISO (212 ).III 329772014 - Solid mineral fuel. Determ

3、ination of trace elements in ash by atomic absorption method 201604011 , , , - , , , , , - ( ) - . , , , , , , . 500 , , , . , - .1 , 0,1 % (1000 ppm1). , .2 , - . - .2 : OIML R 76-12011 . - . 1. . ISO 6872012 . . - 2) ISO 11712012 . 3) 177074 ( 104283, 478880) . -, , , . 1) ppm parts per million (

4、).1 ppm = 1 / = 1 / = 1 / = 104%.2) 2758991 ( 68774) . - .3) 556612013 ( 1171:2010) . .1 329772014 311877 . . 446177 . . ISO 5068-22012 . . 2. - 1) 656375 . 661386 . 670972 . 2) 965675 . . 1048478 . . 1074271 , , , . 113032013 . 113052013 . ISO 117222012 . . 3) 1386768 . 170702014 . 1990890 , , , ,

5、 . 2308378 , . 2533682 . , 2731395 ( 117077) . - - - , 1 , . (), , (-) . , , , , .3 17070. 27313.4 :- (500 c177 10) ;- , - ;- - -. 1 - : - .1) 529172008 ( 11722:1999, 5068-2:2007) . .2) 525012005 ( 3696:1987) - . .3) 529172008 ( 11722:1999, 5068-2:2007) . .2 329772014 1 - - , : Be Cr Cu Mn Ni Pb V

6、Zn234,9357,9324,8279,5232,0283,3318,0213,9N2OC2H2N2OC2H2C2H2C2H2C2H2C2H2N2OC2H2C2H25 , . . . 13867.5.1 67091).5.2 (HCl), , c11420= 1,19 /3 3118.5.3 (HNO3), , c11420= 1,42 /3 4461.5.4 (HF), , c11420= 1,17 /3 10484.5.5 , : (5.3) (5.2) (5.1). .5.6 (H3O3) 9656.5.7 , : 60 (5.6) 1 3 (5.1), . - .5.8 100 /3 - () . - , . ( 99,9 % 99,999 %) , . (6.7). , , - . - 0,01 10 /3 .6 6.1 - -.1) 2- 52501. . 52501 2- .3 329772014 - . , -.6.2 , - 400 1000 . 1 . . ISO 1171.6.3

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