1、 . (ISO 1304:2006, IDT) , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)ISO 13042013, 1.092 . 1.22009 . , - . , , -, 1 160 - , - ()2 (-)3 , (- 27 2013 . 59-) : ( 3166) 00497 ( 3166) 00497 AZAMBYKGMDRUTJUA - 4 ISO 1304:2006 Rubber compoundingingredients Carbon black Determ
2、ination of iodine adsorption number ( . . ). SC 3 ( ) ISO/TC 45 (ISO). (en). , - , , , . -. - . (IDT)5 20 2014 . 210- ISO 13042013 - 1 2016 .6 II ISO 13042013 - , - . () - . , , 2014 -, III ISO 130420131 12 13 14 .25 26 .37 48 .69 .710 .711 .712 .9 () CAS .10 () .11 11IV ISO 13042013 . Rubber compou
3、nding ingredients. Carbon black. Determination of iodine adsorption number 20160101 , - . , . - , .1 ( ) , - A B:- A ;- B . , , . - , , . - .2 . - , ( ).ISO 385:2005 Laboratory glassware Burettes ( . )ISO 648:1977 Laboratory glassware One-mark pipettes ( . - )ISO 1042:1998 Laboratory glassware One-m
4、ark volumetric flasks ( . )ISO 1126 Rubber compounding ingredients Carbon black. Determination of loss on heating (- . . )ISO/TR 9272:2005 Rubber and rubber products Determination of precision for test method standards( . )3 , . . . , - , .1 ISO 13042013 4 ( , , , . .), , .4.1 0,1 .4.2 , (125 c177 1
5、) c1775 .4.3 , A ISO 1042, :a) (2000,00 c177 0,60) 3;b) (1000,00 c177 0,40) 3.4.4 25 3, c1770,03 3, :a) (20,00 c177 0,03) 3;b) (25,00 c177 0,03) 3. A ISO 648 . - 0,01 3 ; , - , 0,01 3. ( ) . (. 7.2.2, 7.3.2, 8.3.3, 8.3.6 8.3.8) , - 20 25 3 .4.5 0,01 3, , - c1770,05 3, ( ) , , 0,05 3 :a) (25,00 c177
6、0,05) 3;b) (50,00 c177 0,05) 3. ISO 385 . - 0,01 3 ; , - , 0,01 3. ( ) .4.6 250 500 3 .4.7 2000 3 .4.8 1000 2000 3 .4.9 - 50 3. , .4.10 , 240 - 25 .4.11 105 / (1000 /).4.12 .4.13 .4.14 ( ), .5 , . . .5.1 .5.2 (I2).5.3 (KI).5.4 (KIO3).5.5 (N2S2O3c2155H2O).5.6 - (C5H11OH).5.7 (H2SO4), 98 %, c114 = 1,8
7、4 /3.5.8 ( ).5.9 (C7H6O3) ( ).2 ISO 130420136 6.1 0,02364 /3(0,04728 ), 9,5 1 -, (. 7.3).6.1.1 100 3 114,00 (5.3) - 0,01 .6.1.2 2000 3(4.3) - 3/4 KI.6.1.3 (5.1) , KI. - - .6.1.4 KI 250 3 (5.1), .6.1.5 (4.1) 12,000 0,005 . , - .6.1.6 , , 6.1.3.6.1.7 KI, 6.1.4, 2000 3,- .6.1.8 KI, 6.1.4.6.1.9 (5.1), ,
8、 , 23 - 1 .6.1.10 , (5.1), , - (4.13) 2 . - 5 .6.1.11 (4.8) .6.2 0,05 /3(0,05 ) 0,0394 /3(0,0394 ). , 0,05 /3(0,05 ); , . 0,0394 /3(0,0394 ). , , , , .6.2.1 24,817 (5.5) - 0,005 .6.2.2 , - 2000 3(4.3).6.2.3 , 1 3 (5.1). -.6.2.4 10 3- (5.6) - .6.2.5 (5.1), , 2 (. 6.1.10).6.2.6 (4.7).6.3 / (KIO3) = 0,00833 /3(0,05 )6.3.1 (5.4) (4.2) - 125 1 . (4.12) .3 ISO 130420136.3.2 2000 3(4.3) 200 3 (5.1) - 57,0 ( 0,1 ) (5.3). .6.3.3 1,7833 (5.4) 0,1 - .6.3.4 (5.1). - 45 .6.3.5 (4.8). / , -.6.4 20 % .6.4.1 175 3 (5.1) - 250 3.6.4.2
