GOST R 54281-2010 Petroleum products lubricating oils and additives Test method for determination of water by coulometric Karl Fischer titration《石油产品、润滑油和添加剂 通过库仑费歇尔滴定法对水含量测定的试验方法》.pdf

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1、, 542812010 27 2002 . 184- , 1.02004 . 1 31 - , - ( ) , 42 3 27 2010 . 1117-4 630407 -, (ASTM D 630407 Standard test method for determination of water in petroleum products, lubricating oils,and additives by coulometric Karl Fischer titration). - 1.52004 ( 3.5). - - , 5 - , - . () . - , , 2012 , - -

2、 II 5428120101 12 13 24 .25 .26 .37 .38 .49 410 511 . ( ) 512 . ( )613 ( ) .614 .615 716 717 () .7 X1 () .9 () ( ) 10 542812010III , Petroleum products, lubricating oils and additives.Test method for determination of waterby coulometric Karl Fischer titration 201207011 1.1 1) 10 25000 / - . - , . ,

3、(S H2S), - (. 5).1.2 , , , - , . - .1.3 , , .1.4 -, . - (), .2 2):ATM 1193 (ASTM D 1193, Standard specification for reagentwater)1) 02 02.02.0 , . 15 2007 . 2007 . - 1998 . 2004 . 630404.2) . , . www.astm.org - serviceastm.org. Document Summary.1 542812010ATM 1298 , ( ) API (ASTM D 1298, Test method

4、 for density, relative density (specific gravity), or API gravity of crude petroleum andliquid petroleum products by hydrometer method)ATM 4052 - (ASTM D 4052, Test method for density and relative density of liquids by digital density meter)ATM 4057 (ASTM D 4057,Practice for manual sampling of petro

5、leum and petroleum products)ATM 4177 (ASTM D 4177, Practice for automatic sampling of petroleum and petroleum products)ATM 5854 - (ASTM D 5854, Practice for mixing and handling of liquid samples of petroleum and petroleum products)ATM 203 (ASTM E 203,Test method for water using volumetric Karl Fisch

6、er titration)3 3.1 - , . - . 1 1 ; , - - .3.2 , - .3.3 - , - -.4 4.1 , , , .4.2 -, , - .5 5.1 , -, . . 500 / - 0,02 % . , , ATM 203. - .5.2 10 200 / . - 500 /.5.3 XI.2 5428120106 6.1 ( ) , , - . .6.1.1 - . - .6.2 - . . - , , , . :6.2.1 10 , - , - 0,1 . , , 10.6.2.2 1, : 250 10 ; 500 10 ; 1 0,01 ; 2

7、0,01 3 0,01 . ().7 7.1 . - , 3), . , - , .7.2 II ATM 1193.7.3 , . ., 100200 /, - ( . ).7.4 . .7.4.1 : , . . . - , , - . ( , ). 1 . , - 17, .3) , , American Chemical Society, Washington,DC. , , . , BDH Ltd.,Poole, Dorset, U.K., , U.S. Pharmacopeial Convention, Inc. (USPC), Rockville, MD.3 5428120107.4.2 . . - ( , - . , ).7.4.3 , , - . 2 , , -.7.5 , . ., 100200 /, - ( . ).7.6 , -, . .7.7 5 Ac111 8 12 .8 8.1 , - , - .8.2 ,

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