1、 545472011 27 2002 . 184- , 1.02004 . 1 - , , ( ) 4, - ( )2 160-3 29 2011 . 631-4 52892007 - . (ASTM D 52892007 Standardtest method for rubber property Vulcanization using rotorless cure meters). - 1.52004 ( 3.5). - - , 5 , - . () . - , , 2015 , - - II 5454720111 .12 13 14 .35 .46 .47 .88 89 .810 81
2、1 9 () , 14III 545472011 Rubber compounds.Measurement of vulcanization characteristics using rotorless cure meters 201307011 1.1 . - . 1 2084.1.2 . -.1.3 , . - , .2 : 13492009 . (ASTM D 13492009,Practice for Rubber Standard temperatures for testing) 15662010 , (ASTM D 15662010, Terminologyrelating t
3、o rubber) 20842007 . - (ASTM D 20842007, Test method for rubber property Vulcanizationusing oscillating disk cure meter) 44832005 , (ASTM D 44832005, Practice for evaluating precision for test method standards in the rubber and carbonblack manufacturing industries)3 3.1 -:3.1.1 (rotorless cure meter
4、): , , -1 545472011 , (), . (. - 1566 2084).3.1.2 (Sc162 torque) Sc162: , () - , .3.1.3 , - (. 1).3.1.3.1 (minimum Sc162 torque) Sc162: - , - .3.1.3.2 (maximum, plateau, or highest Sc162torque) Sc162: , .3.1.3.3 (time to a percentage of full cure):,Sc162,- .3.1.3.4 (time to incipient cure (scorch ti
5、me): , Sc162 -.3.1.4 (Sc162c162 torque) Sc162c162: , - , (. 2).3.1.5 (S* torque) S*: - , (. 2).2 545472011 1 3.1.6 S*, Sc162, Sc162c162 S*= () ( )c162 c43 c162c162SS22.(1)3.1.7 (phase angle c100) c100: S* .3.1.8 c100: c100.3.1.8.1 (discussion): tg c100, Sc162, Sc162c162 tg c100 =c162c162c162SS.(2)3.
6、1.9 Sc162c162 tgc100 , - (. 1):3.1.9.1 Sc162c162 ML Sc162c162 Sc162.3.1.9.2 tg c100ML tg c100 Sc162.3.1.9.3 Sc162c162MH Sc162c162 Sc162.3.1.9.4 tg c100MH tg c100 Sc162.4 4.1 , , . , . , ( ) .4.2 . , - (. 1)., , , .3 545472011 2 5 5.1 .5.2 - , - , , - .5.3 , , - , , , .5.4 , , , , - , .6 6.1 . - .6.1
7、.1 , . 3).4 5454720111 ; 2 ; 3 ; 4 ;5 ; 6 ; 7 ; 8 ; 9 ;10 , 0,5 ; 11 ; 12 ; 13 ; 14 3 6.1.2 , 4).6.2 , - , . - 3b) . 4b).6.2.1 () (40 c177 2) (1,57c162c162 c177 0,08c162c162), - 718. 0,5 (0,02c162c162), . - 3b) 4b). .6.2.2 0,05 0,20 . 0,1 , .6.2.3 , - 8,0 .6.3 .6.3.1 c1770,1 c1773,0, c177 0,5.6.3.2 0,5 2 , (1,7 c177 0,1) .5 5454720111 ; 2 ; 3 ; 4 ; 5 ; 6 ; 7 ; 8 ;9 ; 10 ; 11 ; 12 ;13 4 6.4 .6.4.1 -,- . , , , , 1 % . 2 1 % , .6.4.2 - . Sc162, , .6.4.3 (. 1)
