1、 158292011 , , . EN 15829:2010Foodstuffs Determination of ochratoxin Ain currants, raisins, sultanas, mixed dried fruit and dried figs HPLC method with immunoaffinity column cleanup and fluorescence detection(IDT) 1 - - ( ) , 42 335 - 3 17 2011 . 457-4 15829:2010 - . , , , - . (EN 15829:2010 Foodstu
2、ffs Determination of ochratoxin A incurrants, raisins, sultanas, mixed dried fruit and dried figs HPLC method with immunoaffinity columncleanup and fluorescence detection). - , 5 1.02012 ( 8). ( 1 ) , . () . , (gost.ru) , 2015 , - - II 1582920111 12 13 14 25 .46 57 .68 79 .710 7 () 9 () .10 () .11 1
3、2III 158292011 , , , . Foodstuffs. Determination of ochratoxin A in currants, raisins, sultanas, mixed dried fruit and dried figs. Highperformance liquid chromatographic (HPLC) method with immunoaffinity column cleanup and fluorescence detection 201301011 , , -, - () . , 1,111/. 9 . - , , . , . - .2
4、 - . . . 3696 . ( 3696:1987) EN ISO 3696, Water fov analytical laboratory use Specifications and test methods(ISO 3696:19873 . -, - , - , , . , , . - - .1 158292011 4 4.1 3696. . , . . - (IARC)1.4.2 .4.3 (Na2HPO4c215 12H2O).4.4 .4.5 .4.6 .4.7 .4.8 , (NH4OH) = 1,1 /3 - ( , . 7.2). .4.9 , w (HCl) = 37
5、 %.4.10 , (H3PO4) = 0,1 /3.4.11 , (HCl) = 0,1 /3 8,28 3 4.9 1 3.4.12 , c (NaOH) = 0,1 /3 4 4.7 1 3.4.13 - 8,0 4.6, 1,2 (2,9 (Na2HPO4c215 12H2O) 4.3, 0,2 - 4.5 0,2 4.4 900 3. 7,4 - 4.11 4.12, 13. .4.14 . , - , , . , , .4.15 w (3) c179 98 %.4.16 .4.17 .4.18 , 4.14 4.15 80 : 20 : 2.4.19 , 4.14 4.15 - 9
6、9 : 99 : 2. , , 4.2.2 1582920114.20 4.17 4.15 99 : 1.4.21 , - . - 100 , 70 % 5 , 4.14 - - 4.13 5 : 95.4.22 ( ) 4.17 1 : 19.4.23 , .4.24 , -, , , . ( 2). , - , , . 1 ( ) 4.20, , 20 30 /3. - 300 370 1 5.12. 4.20. , - . , c114ota,/3, c114ota=AMbmaxc215100c101,(1) max ( 333 ); , / ( = 403,8 /);c101 4.20
7、,2/ ( 544 2/ 2);b , . 18 . . - 12 . 6 - .4.25 4.24, 12,5 , 5 3. - 50 . 4.16, . 2,5 /3. 18 . . - 12 . 6 - .3 1582920114.26 4.25 500 3- 5 3, 4.16. 0,25 /3. 18 . - . 6 .5 5.1 -, , .5.2 ( ) 4.22 1 . , , - 4.17, 4.16. . - .5.3 .5.4 , 0,0001 .5.5 , 0,1 .5.6 1, 5, 10 3200 3, 5.7 , ().5.8 .5.9 , 1 , 18 3/.5.10 20 25 .5.11 5.11.1 , 100 3.5.11.2 , , - 1 3/.
