1、 2 ISO 9233-2:2007Cheese, cheese rind and processed cheese Determination of natamycin content Part 2: High-performance liquid chromatographic method for cheese,cheese rind and processed cheese(IDT) 9233-22011 27 2002 . 184- , 1.02004 . 1 - ( ) - ( ) , - 42 335 - 3 17 2011 . 456-4 9233-2:2007 , . . 2
2、 , (ISO 9233-2:2007 Cheese,cheese rind and processed cheese Determination of natamycin content Part 2: High-performance liquidchromatographic method for cheese, cheese rind and processed cheese). - 1.52004 ( 3.5)5 - , - . () . - , , 2013 , - - II 9233-220111 12 13 14 15 .26 .27 .37.1 .37.2 38 .38.1
3、 38.2 38.3 49 .59.1 .59.2 .59.3 , .59.4 510 510.1 .510.2 510.3 .611 .6 A () 7 B () .9 10 9233-22011III 2 Cheese and processed cheese. Determination of natamycin content.Part 2. High-performance liquid chromatographic method 201301011 0,5 / , - 0,03 /2 .2 :2.1 (natamycin content): , - , . .2.2 (surfa
4、ce-area-relatednatamycin mass in cheese rind): , , . - .2.3 (cheese rind): 5 , -, .3 . - 15 C 20 C , . ( ) (HPLC).4 , , .4.1 (CH3OH).4.2 , . (4.1) .1 9233-220114.3 4.3.1 500 /3 (4.1) 100 3(5.1) , - 50 (C33H47NO13). .4.3.2 5 /3 50 3(5.1) 5,0 3 (4.3.1). (4.2) -. 5,0 3 50 3(5.1). (4.2) -. 5 /3. , 8.3.3
5、 - .4.4 (CH3CO2H), .5 , , .5.1 50 100 3.5.2 , 5 30 (. A.1).5.3 , - 1 (. A.2).5.4 .5.5 , .5.6 .5.7 100 200 3, - .5.8 10 3.5.9 0,20 0,45 , - .5.10 , , 150 (, S S,No. 595 1/21).5.11 70 .5.12 , 15 C 20 C.5.13 , , -.5.14 -, - 303 / .5.15 150 , 4,6 , C8, 5 (, Lichrosorb RP81).5.16 100 , 2,1 , C8, - 30 40
6、 .5.17 .6 . .1) , . - -.2 9233-22011 , . - 707. , - .7 7.1 , 30 . (5.2) - , 5 . (5.5) 2 4 2. - . (5.4) , , . - (5.17). , , , (4.1). , , .7.2 (7.1) (5.3) - 1 . 50 2 . (5.17). - , -, , (4.1). , , .8 8.1 8.1.1 200 3(5.7) 10 10,00 (7.1).8.1.2 100 3(5.7) 10 5,00 (7.2).8.2 8.2.1 8.2.1.1 (8.1.1) 100 3 (4.1
7、). 90 (5.6) 90 (5.6). 50 3. - (5.12) 60 .8.2.1.2 (5.10), 53. , , - , , . . (5.8) . - 0,45 (5.9), - 0,20 (5.9). () 20 (8.3.4) 25 3 50 3 5- 10- (8.3.5) .8.2.2 8.2.2.1 (8.1.2) 50 3 (4.1). 90 -3 9233-22011 (5.6) 90 (5.6). - 25 3. (5.12) 60 .8.2.2.2 , 8.2.1.2.8.3 8.3.1 , , - , -, , 0,5 / 0,03 /2.8.3.2 (5.14) : : (4.1) (4.4) 12:8:1 ( );: 1 3/; : 303 , 0,005 , ; : 10 ; () : 1500. , (5.15), - :. (4.4) 303 . (8.3.3) - . , .8.3.3 1, 2, 4, 6 8 3 (4.3.2) - 50 3(5.1). - (4.2) . 0,1; 0,2;0,4; 0,6 0,8 /3 . 20 - . . - , , . HPL- A.3.8.3.4 20 (8.2.1.2 8.2.2.2).
