1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS K ISO 2915 KS K ISO 2915:2009 2009 7 31 http:/www.kats.go.krKS K ISO 2915:2009 : ( ) ( ) LS FITI ( ) : (http:/www.standard.go.kr) : : 2004 12 13 : 2009 7 31 2009-0374 : : ( 02-509-7278) (http:/www.kats.go.kr). 10 5 , . KS K ISO 2915:2009 i ii iii 1 1 2 1
2、3 1 4 1 5 2 6 .3 7 3 8 .5 9 .6 A( ) .7 B( ) .9 KS K ISO 2915:2009 ii . KS K ISO 2915: 2004 . . , , . , , . KS K ISO 2915:2009 iii 1975 1 ISO 2915, Wool Determination of cysteic acid content of wool hydrolysates by paper electrophoresis and colorimetry , . IWTO 23 70 . . (weathering) . , . . . KS K I
3、SO 2915:2009 Wool Determination of cysteic acid content of wool hydrolysates by paper electrophoresis and colorimetry 1 . , , , , . . . 2 . . ( ) . KS M 8241, ( ) KS M ISO 6353 2, 2: 1 KS M ISO 6353 3, 3: 2 3 , . . . 4 . 4.1 , KS M ISO 6353 2(R18) 4.2 , 1.19 g/mL KS M ISO 6353 2(R13) 5.7 N 4.3 , 100
4、 mg 10 mL KS M KS K ISO 2915:2009 2 ISO 6353 2(R1) 5 mL, KS M ISO 6353 2(R2) 100 mL 1 g . . . 4.4 , pH 3.5 (KS M 8241 ) 10 mL KS M ISO 6353 2(R1) 100 mL 890 mL . 5 . 4.5 , 100 mL (monohydrate) 110.6 mg( 100 mg ) . 5 (pistol) 70 24 . 4.6 , 100 mL 2 (dihydrate)(BaCl2 2H2O) 2.5 g . 5 5.1 5.2 , 0.000 2
5、g . 5.3 , (1052) 70 . 5.4 5.5 , 2 cm 30 cm . 5.6 5.7 (blow-pipe) 5.8 5.9 , 20 mL 5.10 , 21 mL 5.11 , 0.01 mL 5.12 , 100 mL 250 mL 5.13 , 100 mL 5.14 , 25 mL 5.15 , 250 mL 5.16 KS K ISO 2915:2009 3 5.17 5.18 (strip) (sheet), (Whatman) No. 1, (Schleicher and Schull) No. 2043 aMgI 5.19 5.20 5.21 , (500
6、10) nm 0 0.7 0.01 . . 5.22 , ( ) (7.3 ) 5.23 6 , . 1 g 1 g , . 1 cm . . KS M ISO 63533(R57) 6 1 . 7 7.1 6. 3 0.000 2 g . 2 (7.2) (7.3). 7.2 (5.1) (1052) (5.3) . (5.4) . .1) . . 7.3 . 1) 30 0.000 2 g .KS K ISO 2915:2009 4 a) (5.23) 100 mL (5.12) (7.1) 5.7 N (4.2) 20 mL . (5.22) 105 4 . . . . b) (7.1)
7、 (5.5) (5.9) 5.7 N 20 mL . (5.7) 24 105 . . a) b) . , 250 mL (5.12) . 2) , 250 mL (5.15) . , (5.10) (4.6) 1 mL . , 50 (5.16) (syrup) . 10 mL . 3 . 5 mL (5.14) . 7.4 . 300 V . , (1 500 V ) . 30 cm ( ) . (5.18) . 2 (5.11) (7.3) 0.01 mL . (4.5) 0.01 mL . 0.5 cm . 2 , (4.4) . . , (5 8 ) V/cm (200 300 )
8、V . . (4 5 ) . (5.3) ( ) 70 30 . 7.5 2) . , (serine sulphate) . . KS K ISO 2915:2009 5 ( ) (4.3) (5.20) . . , 70 30 . (4 6 ) cm . “ ” 3 (5.19) . ( 1 ) . . . 1 4 (4.1) 5 mL . , 30 . 7.6 10 mm (50010) nm . 0.2 0.7 . , 10 mL . . “ (blank)” . 8 C . 10010SH6HTS=mDDVVCC CS : (g) VT : (mL) VH : (mL) DH : D
9、S : m : (g) KS K ISO 2915:2009 6 CS, VT VH , . C 100SHmDD . 9 . a) b) c) d) . KS K ISO 2915:2009 7 A ( ) 10 . (24 4 ) . , 24 . . A B , % 0.20 0.75 sL , % . 0.066 sH , % 0.013 0.026 sR , % 0.012 0.015 A.1 ( ), 95 % (5 % ) Ti . kjsjsT+=2R2Hi2 % j : k : sH sR . A.2 ( ), 95 % (5 % ) TL . kjisjisjsT+=2R2
10、H2LL2 % i : j : KS K ISO 2915:2009 8 k : i 1 , . sL, sH sR . KS K ISO 2915:2009 9 B ( ) B.1 . B.1 () 2004.12.13 2004 0976 : ISO 2915 : 1 2009.07.31 2009 0374 2008.8.25 : a) 1. b) 2. . . ( ) . KS M 8241, KS M ISO 6353 2, KS M ISO 6353 3 c) 2., 3., 4., 5., 6., 7., 8. 3., 4., 5., 6., 7.,8., 9. d) 3. ,
11、e) 4. f) 4. , KS M ISO 6353 2(R18) KS M ISO 6353 2(R13) 5.7 N 5.7 N KS K ISO 2915:2009 10 B.1 ( ) () 2009.07.31 2009 0374 KS M ISO 6353 2(R1) KS M ISO 6353 2(R2) (KS M 8241 ) 70 70 2 g) 5. 5.10: 2 mL1 mL 21 mL 5.14: 2 mL5 mL 21 mL (strip) h) 6. KS M ISO 6353 3(R57) i) ( ) . j) 7. . . k) 9. l) A sL s
12、L , % sH sH , % sR sR , % A.2: m) B 135513 7017 (02)60094114 (02)600948878 http:/ KS K ISO 2915:2009 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS WoolDetermination of cysteic acid content of wool hydrolysates by paper electrophoresis and colorimetry ICS 59.080.01 Korean Agency for Technology and Standards http:/www.kats.go.kr