KS M ISO 11345-2007 Rubber-Assessment of carbon black and carbon black silica dispersion-Rapid comparative methods《橡胶 炭黑和炭黑 硅土分散性的评估 快速比较法》.pdf

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1、 KS M ISO 11345KSKSKSKSSKSKSKS KSKSKS SKSKS KSKS SKS KS / KS M ISO 11345: 2007 2007 8 16 http:/www.kats.go.krKS M ISO 11345: 2007 : () ( ) () () () ( ) : (http:/www.standard.go.kr) : :2007 8 16 2007-0504 : : ( 02-509-7301) (http:/www.kats.go.kr ). 7 5 , . KS M ISO 11345: 2007 i ii 1 1 2 1 3 .1 4 .1

2、5 2 6 A 30 2 6.1 .2 6.2 2 6.3 .3 6.4 3 7 B 30 3 7.1 .3 7.2 4 7.3 .5 7.4 5 8 C 100 6 8.1 .6 8.2 6 8.3 .6 8.4 6 9 D 100 .7 9.1 .7 9.2 7 9.3 .8 9.4 8 10 E 100 8 10.1 .8 10.2 10 10.3 .10 10.4 10 11 .10 A( ) X30 ( A B) 11 B( ) X100 (CB) 12 C( ) X100 (RCB).15 D( ) X100 (RCB/Silica).18 E( ) X100 (SRCB) .21

3、 F( ) 24 26 KS M ISO 11345: 2007 ii 2006 2 ISO 11345, Rubber Assessment of carbon black and carbon black/silica dispersion Rapid comparative methods , . KS M ISO 11345: 2007 / Rubber Assessment of carbon black and carbon black/silica dispersion Rapid comparative methods . . . 1 / . 1 10 . , ( 1 10)

4、. 2 . . ISO 1382, Rubber Vocabulary 3 , ISO 1382 . 4 / . 5 . A: 30 ( ) B: 30 (split-field) ( ) C: 100 ( / ) D: 100 (split-field) ( / ) KS M ISO 11345: 2007 2 E: 100 ( ) A D , A B( A ) 30 , C D( B E ) 100 , 30 10 10( ) 1( ) . 1 10 . . 9 10 8 7 5 6 3 4 1 2 E , 100 , 30 (image-processing system) , 10(

5、) 1( ) . 10 23 m , , 1 . 5 5 . 6 A 30 6.1 A . 6.2 6.2.1 6.2.2 . 6.2.3 (30) 6.2.4 KS M ISO 11345: 2007 3 6.2.4 (30) 2 . 6.2.5 . 6.3 6.3.1 8 mm, 10 mm . . . 6.3.2 . , . , 105 5 1 kPa (slab) . . . 100 . , . 6.4 (30 ) . . ( ) ( A ). , . . . . 5 6 5 1/2 . 1 , 10 . 7 B 30 7.1 B KS M ISO 11345: 2007 4 . CC

6、D TV . A . 7.2 7.2.1 7.2.2 . 7.2.3 10 . ( ) ( ), . CCD ( 1 2 ). 1 6 2 7 3 8 4 TV 9 5 10 1 B D KS M ISO 11345: 2007 5 1 6 2 CCD 7 ( ) 3 8 4 9 5 10 2 CCD B D 7.3 B 6.3 . 7.4 . . . (30 ) . ( ) . . . . 5 6 5 1/2 . 1 10 . KS M ISO 11345: 2007 6 8 C 100 8.1 C / . 8.2 8.2.1 8.2.2 . 8.2.3 (100) 8.2.4 8.2.4

7、(100) 2 . 8.2.5 . 8.3 C 6.3 . 8.4 (30 ) . . / ( ) . ( 3 ). KS M ISO 11345: 2007 7 3 C D B E . , . . . . 5 6 5 1/2 . 1 , 10 . 9 D 100 9.1 D / . / CCD TV . C ( 3 ). 9.2 9.2.1 9.2.2 . CB RCB RCB/Silica SRCB KS M ISO 11345: 2007 8 9.2.3 10 . ( ) ( ), . CCD ( 1 2 ). 9.3 D 6.3 . 9.4 . . . (30 ) . / ( ) .

8、( 3 , B E ). . . . 5 6 5 1/2 . 1 , 10 . 10 E 100 10.1 E CCD . ( , nodules) . . CCD (image-processing system) . y 1 10 ( 1 ) . , 10 23 m , 1 ( 19 % ) . . totw19.0910NNy= KS M ISO 11345: 2007 9 Nw : 23 m Ntot : F . 1 y % y 19 1 2 3 4 5 6 7 8 9 0 10 4 . 23 m . . 1 10 (y 10 23 m . y 1 ). X (m) Y 1 ( y )

9、 2 ( y ) a 4 (y ) KS M ISO 11345: 2007 10 10.2 10.2.1 10.2.2 . 10.2.3 7.2.3 . , . . . . 10.3 E 6.3 . 10.4 . . . (30 ) . ( ) . 23 m . . . 1 . . . 1 10 23 m . 11 . a) b) , , , c) : A, B, C, D E d) 1 10 . ( , ). e) KS M ISO 11345: 2007 11 A ( ) 30 ( A B) . 6 7 8 9 10 1 2 3 4 5 KS M ISO 11345: 2007 12 B

10、 ( ) 100 (CB) CB2CB1 KS M ISO 11345: 2007 13 CB4CB3 CB6CB5 KS M ISO 11345: 2007 14 CB10CB9 CB8CB7 KS M ISO 11345: 2007 15 C ( ) 100 (RCB) RCB 1 RCB2 KS M ISO 11345: 2007 16 RCB 3 RCB4 RCB 5 RCB6 KS M ISO 11345: 2007 17 RCB 7 RCB8 RCB 9 RCB10KS M ISO 11345: 2007 18 D ( ) 100 (RCB/Silica) RCB/ Si1 RCB

11、/Si2KS M ISO 11345: 2007 19 RCB/ Si5 RCB/Si6RCB/ Si3 RCB/Si4KS M ISO 11345: 2007 20 RCB/ Si7 RCB/Si8RCB/ Si9 RCB/Si10KS M ISO 11345: 2007 21 E ( ) 100 (SRCB) SRCB 1 SRCB2 KS M ISO 11345: 2007 22 SRCB 3 SRCB4 SRCB 5 SRCB6 KS M ISO 11345: 2007 23 SRCB 7 SRCB8 SRCB 9 SRCB10KS M ISO 11345: 2007 24 F ( )

12、 F.1 , , . “ ” . 10. x . , “ ” . . 8 (A H) 6 (Cabot) 1 . , . (x, y) , .: A D x ( E) y y ( ) / . 1 10 (y ) . F.2 , . CB(x, y), RCB(x, y) RCB/Silica(x, y) . “ ” y . y 30 , CCD . . . , y (y 10 y 1) . ( .) . y , . . CCD . , . 5 m . y , 23 m . , D . KS M ISO 11345: 2007 25 F.1 KS M ISO 11345 D a% D b% 10

13、 99.5 100 9 8 7 6 5 4 3 2 1 80.0 92.0 a 2 b 3 KS M ISO 11345: 2007 26 1 MEDALIA, A.I., and WALKER, D.F., 1966: Evaluating dispersion of carbon black in rubber, Technical Report RG-124, Revision 2, Cabot Corporation 2 LEIGH-DUGMORE, C.H., 1956 : Measurement of dispersion in back-loaded rubber, Rubber Chemistry and Technology, Vol. 29, pp. 1303 1308 3 MEDALIA, A.I., 1961: Dispersion of carbon black in rubber Revised calculation procedure, Rubber Chemistry and Technology, Vol. 34, pp. 1134 1140

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