1、Designation: D1900 06 (Reapproved 2015)Standard Practice forCarbon BlackSampling Bulk Shipments1This standard is issued under the fixed designation D1900; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A
2、 number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers procedures for the sampling anddata reporting of bulk shipments of carbon black in three-compartment hopper rail
3、cars and compartmented bulk hoppertrailers.NOTE 1The tests to be made on the samples obtained by this practice,how many samples are taken, where they are taken, and what statisticalvalues (if any) to report shall be determined by agreement between thepurchaser and the manufacturer. This practice giv
4、es guidance for use indeveloping such agreements or for use when no formal agreement exists.The specific details of each procedure are described in appropriate ASTMtest methods used for testing carbon black.NOTE 2Some purchasers or manufacturers may consider FlexibleIntermediate Bulk Containers (FIB
5、C) to be a bulk shipment. See PracticeD1799 for guidance on sampling and reporting for this package.1.2 The values stated in SI units are to be regarded asstandard. The values given in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns, if any
6、, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D1799 Practice for Carbon BlackSampling PackagedShi
7、pmentsD5817 Practice for Carbon Black, PelletedReduction,Blending, and Drying of Gross Samples for Testing3. Significance and Use3.1 Sampling of bulk shipments of carbon blacks is ofutmost importance since the location and number of samplestaken by different laboratories can have a significant effec
8、t onthe agreement of test values obtained. This practice is for usein obtaining representative samples of carbon black in eachcompartment or in the entire hopper car or hopper truck. Thesesamples may be used to ascertain the average quality or theuniformity of a shipment, or both.4. Sampling Procedu
9、re4.1 Withdraw approximatelya4dm3(1 gal) sample fromeach sample port, after first withdrawing at least 4 dm3(1 gal)of carbon black from each port and discarding it. Sample portsare located on each side of each compartment in a three-compartment bulk hopper rail car and on one side of a hoppertruck.4
10、.2 If sampling from the top ports of a hopper car or hoppertruck, approximately 150 mm (6 in.) of surface material shouldbe raked aside before collecting approximately 4 dm3(1 gal)for testing.4.3 Asample thief may be used to sample from the top portsof a hopper car or hopper truck. The thief must be
11、 able tosample at least 150 mm (6 in.) below the surface. Collectapproximately 4 dm3(1 gal) for testing.4.4 If sampling a hopper car or hopper truck during unload-ing it is recommended that three samples be collected fortesting from each compartment: one at the beginning ofunloading, one at approxim
12、ately the middle of unloading, andone near the end of unloading. The sample size should beapproximately 4 dm3(1 gal).4.5 If sampling a hopper car or hopper truck during loadingit is recommended that three samples be collected for testingfrom each compartment: one at the beginning of loading, oneat a
13、pproximately the middle of loading and one near the end ofloading. The sample size should be approximately 4 dm3(1 gal).4.6 Samples collected as described in 4.1 4.5 may betested singly or composited. See Practice D5817 for guidanceon preparing composited samples. When disputed test resultsarise rea
14、sonable efforts should be made for all parties to testsamples taken from the same location.5. Sample Preparation and Handling5.1 Store the samples in airtight containers until the mate-rials are needed for sample preparation or testing. Hold any1This practice is under the jurisdiction of ASTM Commit
15、tee D24 on CarbonBlack and is the direct responsibility of Subcommittee D24.61 on Carbon BlackSampling and Statistical Analysis.Current edition approved Nov. 1, 2015. Published December 2015. Originallyapproved in 1961. Last previous edition approved in 2011 as D1900 06(2011).DOI: 10.1520/D1900-06R1
16、5.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box
17、 C700, West Conshohocken, PA 19428-2959. United States1excess material in airtight containers for possible follow-uptesting until all tests are completed.5.2 Handle samples collected for the determination of pelletquality with care to avoid pellet breakdown.5.3 If individual samples are taken for te
18、stingindependently, pass each sample through a single-stage riffle-type sample splitter at least twice in order to prevent stratifi-cation. See Practice D5817. This is particularly important ifpellet quality tests are to be made on the sample.5.4 If individual samples are composited, pass them throu
19、gha single-stage riffle-type sample splitter at least three times. SeePractice D5817.5.5 Composite samples should be tested if simply theaverage value of a given property of the shipment is to bedetermined.5.6 Individual samples shall be tested if average and rangeor sample standard deviation values
20、 for a given property of theshipment are to be determined.6. Report6.1 Report the following information:6.1.1 Number of individual samples and their location.6.1.2 Average value, if composite samples were tested.6.1.3 Individual values, average, and range or sample stan-dard deviation, if individual
21、 samples were tested.7. Precision and Bias7.1 Data for precision and bias are not applicable to thispractice.8. Keywords8.1 carbon black; hopper cars; hopper trucks; sampling bulkshipmentsASTM International takes no position respecting the validity of any patent rights asserted in connection with an
22、y item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical
23、 committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration a
24、t a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor
25、Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 06 (2015)2
