1、Designation: E 662 061An American National StandardStandard Test Method forSpecific Optical Density of Smoke Generated by SolidMaterials1This standard is issued under the fixed designation E 662; the number immediately following the designation indicates the year oforiginal adoption or, in the case
2、of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1NOTEAdded research repo
3、rt footnote to Section 14 editorially in September 2008.1. Scope1.1 This fire-test-response standard covers determination ofthe specific optical density of smoke generated by solidmaterials and assemblies mounted in the vertical position inthicknesses up to and including 1 in. (25.4 mm).1.2 Measurem
4、ent is made of the attenuation of a light beamby smoke (suspended solid or liquid particles) accumulatingwithin a closed chamber due to nonflaming pyrolytic decom-position and flaming combustion.1.3 Results are expressed in terms of specific optical densitywhich is derived from a geometrical factor
5、and the measuredoptical density, a measurement characteristic of the concentra-tion of smoke.1.4 This test method is intended for use in research anddevelopment and not as a basis for ratings for regulatorypurposes.1.5 This standard measures and describes the response ofmaterials, products, or assem
6、blies to heat and flame undercontrolled conditions, but does not by itself incorporate allfactors required for fire hazard or fire risk assessment of thematerials, products or assemblies under actual fire conditions.1.6 This standard does not purport to address all of thesafety concerns, if any, ass
7、ociated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.1.7 The values stated in inch-pound units are to be regardedas standard. Values stated in parenthes
8、es are for informationonly.2. Referenced Documents2.1 ASTM Standards:2D 2843 Test Method for Density of Smoke from the Burn-ing or Decomposition of PlasticsE 176 Terminology of Fire Standards3. Terminology3.1 DefinitionsFor definitions of terms found in this testmethod refer to Terminology E 176.4.
9、Summary of Test Method4.1 This test method employs an electrically heated radiant-energy source mounted within an insulated ceramic tube andpositioned so as to produce an irradiance level of 2.2 Btu/sft2(2.5 W/cm2) averaged over the central 1.5-in. (38.1-mm)diameter area of a vertically mounted spec
10、imen facing theradiant heater. The nominal 3 by 3-in. (76.2 by 76.2-mm)specimen is mounted within a holder which exposes an areameasuring 2916 by 2916 in. (65.1 by 65.1 mm). The holder isable to accommodate specimens up to 1 in. (25.4 mm) thick.This exposure provides the nonflaming condition of the
11、test.4.2 For the flaming condition, a six-tube burner is used toapply a row of equidistant flamelets across the lower edge ofthe exposed specimen area and into the specimen holdertrough. This application of flame in addition to the specifiedirradiance level from the heating element constitutes thefl
12、aming combustion exposure.4.3 The test specimens are exposed to the flaming andnonflaming conditions within a closed chamber. A photometric1This test method is under the jurisdiction of ASTM Committee E05 on FireStandards and is the direct responsibility of Subcommittee E05.21 on Smoke andCombustion
13、 Products.Current edition approved July 15, 2006. Published August 2006. Originallyapproved in 1979. Last previous edition approved in 2005 as E 662 05.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMSta
14、ndards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.system with a vertical light path is used to measure the varyinglight transmission as smoke ac
15、cumulates. The light transmit-tance measurements are used to calculate specific opticaldensity of the smoke generated during the time period to reachthe maximum value.35. Significance and Use5.1 This test method provides a means for determining thespecific optical density of the smoke generated by s
16、pecimens ofmaterials and assemblies under the specified exposure condi-tions. Values determined by this test are specific to thespecimen or assembly in the form and thickness tested and arenot to be considered inherent fundamental properties of thematerial tested. Thus, it is likely that closely rep
17、eatable orreproducible experimental results are not to be expected fromtests of a given material when specimen thickness, density, orother variables are involved.5.2 The photometric scale used to measure smoke by thistest method is similar to the optical density scale for humanvision. However, physi
18、ological aspects associated with visionare not measured by this test method. Correlation with mea-surements by other test methods has not been established.45.3 At the present time no basis is provided for predictingthe density of smoke generated by the materials upon exposureto heat and flame under
19、other fire conditions.5.4 The test method is of a complex nature and the dataobtained are sensitive to variations which in other test methodsmight be considered to be insignificant (see Section 6). Aprecision statement based on the results of a roundrobin test bya prior draft version of this test me
20、thod is given in 14.15.5 In this procedure, the specimens are subjected to one ormore specific sets of laboratory test conditions. If different testconditions are substituted or the end-use conditions arechanged, it is not always possible by or from this test methodto predict changes in the fire-tes
21、t-response characteristicsmeasured. Therefore, the results are valid only for the fire testexposure conditions described in this procedure.6. Limitations6.1 If during the test of one or more of the three replicatesamples there occurs such unusual behavior as (1) the speci-men falling out of the hold
22、er, (2) melted material overflowingthe sample holder trough, (3) self-ignition in the pyrolysismode, (4) extinguishment of the flame tiplets (even for a shortperiod of time), or (5) a specimen being displaced from thezone of controlled irradiance, then an additional three samplesof the identical pre
23、conditioned materials shall be tested in thetest mode in which the unusual behavior occurred. Dataobtained from the improper tests noted above shall not beincorporated in the averaged data but the occurrence shall bereported. The test method is not suitable if more than three ofthe six replicates te
24、sted show these characteristics.6.2 The test method has proven sensitive to small variationsin sample geometry, surface orientation, thickness (eitheroverall or individual layer), weight, and composition. It is,therefore, critical that the replicate samples be cut, sawed, orblanked to identical samp
25、le areas, 3 by 3, +0, 0.03 in. (76.2by 76.2, +0, 0.8 mm), and that records be kept of therespective weights with the individual test data. It is feasiblethat evaluation of the obtained data together with the individualweights will assist in assessing the reasons for any observedvariability in measur
26、ements. Preselection of samples withidentical thickness or weight, or both, are potential methods toreduce the variability but are likely to not be truly indicative ofthe actual variability to be expected from the material asnormally supplied.6.3 The results of the test apply only to the thickness o
27、f thespecimen as tested. There is no common mathematical formulato calculate the specific optical density of one thickness of amaterial when the specific optical density of another thicknessof the same material is known.6.4 The test method is sensitive to small variations of theposition of the speci
28、men and radiometer relative to the radiantheat source.6.5 It is critical to clean the test chamber, and to removeaccumulated residues from the walls when changing from onetest material to another, to ensure that chemical or physicalrecombination with the effluents or residues produced does notaffect
29、 the data obtained. Even when testing the same material,excessive accumulations of residue shall not be permitted tobuild up since ruggedness tests have indicated that suchaccumulations serve as additional insulators tending to reducenormally expected condensation of the aerosol, thereby raisingthe
30、measured specific optical density.6.6 With resilient samples, take extreme care to ensure thateach replicate sample in its aluminum foil wrapper is installedso that each protrudes identically through the front sampleholder opening. Unequal protrusion will subject the samples todifferent effective ir
31、radiances and to slightly different ignitionexposures. Excessive protrusion of specimens has the potentialto cause drips or for the specimen to sag onto the burner,clogging the flame jets and thereby invalidating the test.6.7 The measurements obtained have also proven sensitiveto small differences i
32、n conditioning (see Section 9). Manymaterials such as carpeting and thick sections of wood,plastics, or plywood require long periods to attain equilibrium(constant weight) even in a forced-draft humidification cham-ber.7. Apparatus7.1 Fig. 1 shows examples of the test apparatus, with adetailed descr
33、iption contained in the remainder of Section 7and in Annex A2. The apparatus shall include the following:3Additional parameters, such as the maximum rate of smoke accumulation, timeto a fixed optical density level, or a smoke obscuration index provide potentiallyuseful information. See Appendix X1.4
34、Other test methods for measuring smoke available at the time of the publica-tions referenced have been reviewed and summarized in “The Control of Smoke inBuilding FiresAState of theArt Review.” Materials Research and Standards,Vol42, April 1971, pp. 1623 and “A Report on Smoke Test Methods,” ASTMSta
35、ndardization News, August 1976, pp. 1826.E66206127.1.1 Test ChamberAs shown in Fig. 1, the test chambershall be fabricated from laminated panels5to provide insidedimensions of 36 by 24 by 36 618 in. (914 by 610 by 914 63 mm) for width, depth, and height, respectively. The interiorsurfaces shall cons
36、ist of porcelain enameled metal, or equiva-lent coated metal resistant to chemical attack and corrosion,and suitable for periodic cleaning. Sealed windows shall beprovided to accommodate a vertical photometric system. All5Commercially available panels of porcelain-enameled steel (interior surface)pe
37、rmanently laminated to an asbestos-magnesia core and backed with galvanizedsteel (exterior surface), total thickness316 in. (9.6 mm), have been found suitable.APhotomultiplier tube housing NFlowmeter shutoff valvesBChamber OSample mover knobCBlow-out panel (in floor of chamber) PLight source switchD
38、Hinged door with window QLight source voltage jacksEExhaust vent control RLine switchFRadiometer output jacks SBase cabinetGTemperature (wall) indicator TIndicating lampsHAutotransformer UMicrophotometer (photomultiplier)IFurnace switch VOptical system rodsJVoltmeter (furnace) WOptical system floor
39、windowKFuse holder (furnace) XExhaust vent damperLRadiometer air flowmeter YInlet vent damperMGas and air (burner) flowmeter ZAccess portsFIG. 1 Smoke Density Chamber AssemblyE6620613other chamber penetrations shall be sealed. When all openingsare closed, the chamber shall be capable of developing a
40、ndmaintaining positive pressure during test periods, in accor-dance with 11.11.7.1.2 Radiant Heat FurnaceAs shown in Fig. 2,anelectric furnace with a 3-in. (76.2-mm) diameter opening shallbe used to provide a constant irradiance on the specimensurface. The furnace shall be located along the centerli
41、neequidistant between the front and back of the chamber, with theopening facing toward and about 12 in. (305 mm) from theright wall. The centerline of the furnace shall be about 734 in.(195 mm) above the chamber floor. The furnace control systemshall maintain the required irradiance level, under ste
42、ady-stateconditions with the chamber door closed, of 2.20 6 0.04Btu/ft2s (2.50 6 0.05 W/cm2) for 20 min. The control systemshall consist of an autotransformer or alternative controldevice, and a voltmeter or other means for monitoring theelectrical input. Where line voltage fluctuations exceed 62.5
43、,a constant voltage transformer is required to maintain theprescribed irradiance level.7.1.3 Specimen HolderSpecimen holders shall conform inshape and dimension to that shown in Fig. 3 and be fabricatedto expose a 2916 by 2916-in. (65.1 by 65.1-mm) specimen area.Also shown in Fig. 3 are the spring a
44、nd rods for retaining thespecimen within the holders.7.1.4 Framework for Support of Furnace and SpecimenHolderThe furnace and specimen supporting frameworkshall be constructed essentially in accordance with Fig. 4.7.1.5 Photometric SystemThe photometric system shallconsist of a light source and phot
45、odetector, oriented verticallyto reduce measurement variations resulting from stratificationof the smoke generated by materials under test. The systemshall be as shown in Figs. 5 and 6 and include the following:7.1.5.1 The light source shall be an incandescent lampoperated at a fixed voltage in a ci
46、rcuit powered by a constant-voltage transformer. The light source shall be mounted in aAStainless steel tube GStainless steel spacersBFront insulating ring HStainless steel reflectors (3)CCeramic tube JCenter insulating diskDHeater/plate 525 W KInsulating spacer ringEStainless steel mounting screw L
47、Rear insulating diskFInsulating gasket MSheet metal screw (2)PHeater leads/porcelain beadsFIG. 2 Furnace SectionE6620614sealed and light-tight box. This box shall contain the necessary optics to provide a collimated light beam passing verticallyFIG. 3 Details of Specimen Holder and Pilot BurnerFIG.
48、4 Furnace SupportE6620615through the chamber. The light source shall be maintained at anoperating voltage required to provide a brightness temperatureof 2200 6 100K.APhotomultiplier housing KOptical system platforms (2)BPhotomultiplier tube and socket LOptical windows (2)CUpper shutter blade, with N
49、D2 filter over one aperture MChamber roofDLower shutter blade, with single aperture NAlignment rods (3)EOpal diffuser filter PParallel light beam, 1.5-in. (37.5-mm) diameterFAperature disk QChamber floorGNeutral density compensating filter (from set of 9) ROptical window heater, silicone-fiberglass 50 W/115 VHLens, 7 diopter (2) SRegulated light source transformer, 115/125 V-6 VJOptical system housing (2) TAdjustable resistor, light source, adjusted for 4 VULight sourceFIG. 5 Photometer DetailsE6
