1、BRITISH STANDARD BS EN ISO 105-X13:1997 Textiles Tests for colour fastness Part X13: Colour fastness of wool dyes to processes using chemical means for creasing, pleating and setting (ISO 105-X13:1994) The European Standard EN ISO 105-X13:1997 has the status of a British Standard ICS 59.080.01BSEN I
2、SO 105-X13:1997 This British Standard, having been prepared under the directionof the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 August 1997 BSI 09-1999 ISBN 0 580 27878 6 National foreword This British Standard is t
3、he English language version of ENISO105-X13:1997. It is identical with ISO105-X13:1994. It supersedes the relevant method in BS1006:1990 which is withdrawn by amendment. The UK participation in its preparation was entrusted by Technical Committee TCI/25, Chemical properties, to Subcommittee TCI/25/-
4、/10, Colour fastness, which has the responsibility to: aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European develo
5、pments and promulgate them in the UK. A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references Attention is drawn to the fact thatAnnex ZA lists normative references to international publications with their corresponding European publicat
6、ions. The British Standards which implement these international or European publications may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard d
7、oes not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an in
8、side front cover, pages i and ii, theEN ISO title page, page 2, the ISO title page, pages ii to iv, pages 1 to 4 and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. Am
9、endments issued since publication Amd. No. Date CommentsBSENISO 105-X13:1997 BSI 09-1999 i Contents Page National foreword Inside front cover Foreword 2 Foreword iii Text of ISO 105-X13 1ii blankEUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-X13 April 1997 ICS 59.080.01 Descriptors: Se
10、e ISO document English version Textiles Tests for colour fastness PartX13: Colour fastness of wool dyes to processesusingchemical means for creasing,pleatingandsetting (ISO 105-X13:1994) Textiles Essais de solidit des teintures PartieX13: Solidit des teintures sur laine aux traitements effectus avec
11、 des produits chimiques en vue du plissage et du fixage (ISO 105-X13:1994) Textilien Farbechtheitsprfungen TeilX13: Farbechtheit von Wollfarbstoffen gegen Prozesse zum Falten, Plissieren und Fixieren auf chemischem Wege (ISO 105-X13:1994) This European Standard was approved by CEN on 1997-03-28. CEN
12、 members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date Lists and bibliographical references concerning such national standards may be obtained on appl
13、ication to the Central Secretariat or to any CEN member. The European Standards exist in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own Language and notified to the Central Secretariat has t
14、he same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standar
15、dization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1997 CEN ALL rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 105-X13:1997 EENISO105-X13:1997 BSI 09-1999 2
16、Foreword The text of the International Standard from Technical Committee ISO/TC38 “Textiles” of the International Organization for Standardization (ISO) has been taken over as an European Standard by Technical Committee CEN/TC248 “Textiles and textile products”, the secretariat of which is held by B
17、SI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 1997, and conflicting national standards shall be withdrawn at the latest by October1997. According to the CEN/CENELEC Internal Regulati
18、ons, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endo
19、rsement notice The text of the International Standard ISO105-X13:1994 has been approved by CEN as a European Standard without any modification. NOTENormative references to International Standards are listed inAnnex ZA (normative).ENISO105-X13:1997 ii BSI 09-1999 Contents Page Foreword iii 1 Scope 1
20、2 Normative references 1 3 Principle 1 4 Apparatus and reagent 1 5 Test specimens 1 6 Procedure 2 7 Test report 2 Annex ZA (normative) Normative references to international publications with their relevant European publications 4 Figure 1 Composite specimen 3 Descriptors: Textiles, wool, dyes, tests
21、, chemical tests, determination, colour fastness.ENISO105-X13:1997 BSI 09-1999 iii Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out throu
22、gh ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collabora
23、tes closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at
24、least75% of the member bodies casting a vote. International Standard ISO105-X13 was prepared by Technical Committee ISO/TC38, Textiles, Subcommittee SC1, Tests for coloured textiles and colorants. This fourth edition cancels and replaces the third edition (ISO105-X13:1987), of which it constitutes a
25、 technical revision. ISO 105 was previously published in thirteen “parts”, each designated by a letter (e.g. “Part A”), with publication dates between1978 and1985. Each part contained a series of “sections”, each designated by the respective part letter and by a two-digit serial number (e.g. “Sectio
26、n A01”). These sections are now being republished as separate documents, themselves designated “parts” but retaining their earlier alphanumeric designations. A complete list of these parts is given in ISO105-A01.iv blankENISO105-X13:1997 BSI 09-1999 1 1 Scope This part of ISO specifies a method for
27、determining the resistance of the colour of wool textiles of all kinds to processes using chemical means in conjunction with steam for creasing, pleating and setting purposes. 2 Normative references The following standards contain provisions which, through reference in this text, constitute provisio
28、ns of this part of ISO105. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO105 are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below.
29、 Members of IEC and ISO maintain registers of currently valid International Standards. ISO 105-A01:1994, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour. ISO 105-A03:1
30、993, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining. ISO 105-F:1985, Textiles Tests for colour fastness Part F: Standard adjacent fabrics. 3 Principle A specimen of the textile, treated with the chemical solution, is placed in contact with specified adjacent fabrics a
31、nd subjected to steam pressing. A comparison specimen, not treated with the chemical solution, is steam-pressed simultaneously. The specimens are dried and any differences between the colour of the two specimens and the staining of the adjacent fabrics are assessed by comparison with the grey scales
32、. 4 Apparatus and reagent 4.1 Steam press, flat bed, with steam supply at a pressure of not less than415kPa. The press should be at its normal operating temperature to avoid anomalous results due to condensation. When starting from cold, the press should be run six times through the standard cycle (
33、see6.5) without test specimens. 4.2 Apparatus capable of giving a fine, uniform spray, constructed from chemically inert materials. 4.3 Chemical solution, at the recommended concentration. This test procedure was established with an aqueous solution containing a volume fraction of5% mono-ethanolamin
34、e sesquisulfite to which was added a 0,3% volume fraction of any suitable wetting agent. The method may be adapted to the use of other chemical products, provided that allowance is made for any recommendations as to working concentration;3g of a wetting agent should be added per litre of solution, i
35、rrespective of its composition. 4.4 Glass plate, 100mm 150mm, on which the specimen is laid for spraying. 4.5 Eight single-fibre adjacent fabrics, complying with the relevant sections of F01 to F08 of ISO105-F:1985, each measuring80mm 110mm, four of wool and four normally of cotton. When staining of
36、 a fibre other than cotton is of greater interest, the cotton may be replaced by an alternative material having a smooth finish and made of this fibre. 4.6 Backing material Some dyes can even stain the press covers. The use of a protective plain backing material is therefore specified; thick cotton
37、fabric or paper towelling has been found satisfactory. 4.7 Grey scale for assessing change in colour, complying with ISO105-A02, and grey scale for assessing staining, complying with ISO105-A03. 5 Test specimens 5.1 If the textile to be tested is fabric, use two specimens measuring 100mm 150mm ident
38、ically oriented. 5.2 If the textile to be tested is yarn, either knit it into fabric and treat as in5.1 or form a layer of parallel lengths of mass approximately half the combined mass of the four adjacent fabrics (4.5), two of each kind, in the composite specimen (see5.3). If the textile to be test
39、ed is loose fibre, comb and compress an amount approximately equal to half the combined mass of the adjacent fabrics into a sheet100mm 150mm. 5.3 Place each specimen between four adjacent fabrics, one of each kind on each side, to form a composite specimen. Two composite specimens are required for e
40、ach test, one to contain the treated specimen (see5.3.1), the other to contain the comparison specimen (see5.3.2).ENISO105-X13:1997 2 BSI 09-1999 5.3.1 Composite treated specimen. Cover one-half of each side of the treated specimen with the wool adjacent fabric, the cloth on top of the specimen bein
41、g prewetted (see6.2). Cover the other half of each side with the cotton adjacent fabric or alternative material (see4.5). The composite specimen shall be backed on each side (see4.6). The composite specimen with backing is illustrated inFigure 1. 5.3.2 Composite comparison specimen. This is identica
42、l with the composite treated specimen(5.3.1) except that the specimen is not treated and the upper wool adjacent fabric is not prewetted. 6 Procedure 6.1 Assemble the composite comparison specimen(5.3.2). 6.2 Wet out one only of the four wool adjacent fabrics for1min in boiling distilled water, hydr
43、oextract to approximately50% expression and store in a suitable container. The use of prewetted wool adjacent fabric, only on the sprayed surface of the specimen, gives more uniformity of any staining. The wool adjacent fabric in the composite comparison specimen shall not be prewetted, since this s
44、pecimen is intended to reproduce the effect of steam pressing only. It will be found convenient to wet out the number of wool adjacent fabrics required for a series of tests in the manner described in the preceding paragraph and to store these in a container such as a polyethylene bag to maintain th
45、e water content. NOTE 1See ISO105-A01:1994, subclause11.4, concerning wetting out of wool specimens. 6.3 Weigh the remaining specimen, place it on the glass plate(4.4) with the surface to be assessed facing upwards and uniformly spray this surface with the chemical solution(4.3) to a mass increase o
46、f100%. 6.4 Assemble the composite treated specimen(5.3.1), sprayed surface up, with the wetted wool adjacent fabric on the sprayed surface. 6.5 Not more than2min after spraying, place both composite specimens side by side on backing material on the preheated press(4.1) and cover with backing materia
47、l(4.6). Immediately close the press, steam for30s using top steam only, shut off the steam and hold in the press for30s with the press head closed. Open the press and apply vacuum for10s. 6.6 Remove the composite specimens from the press, open them out, and dry them by hanging them in air at a tempe
48、rature not exceeding60 C. 6.7 Using the comparison specimen as the reference specimen, and not the original material as is normal, assess any difference in colour between the upper surfaces of the treated and comparison specimens which have been in contact with the smoother adjacent fabric (for exam
49、ple cotton) using the grey scale for assessing change in colour(4.7). Assess the staining of the adjacent fabrics which were in contact with the sprayed surface using the grey scale for assessing staining(4.7). Staining of the other adjacent fabrics in both specimens is not normally assessed but may provide useful information in certain cases. 7 Test report The test report shall include the following information: a) the number and year of publication of this part of ISO105, i.e. ISO105-X13:1994; b) all details necessary for
