CAN CGSB-3 524-2017 Biodiesel (B100) for blending in middle distillate fuels.pdf

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1、CAN / CGSB3.5242017Supersedes CAN / CGSB3.5242014National Standard of CanadaCanadian General Standards BoardBiodiesel (B100) for blending in middle distillate fuelsThe CANADIAN GENERAL STANDARDS BOARD (CGSB), under whose auspices this standard has been developed, is a government agency within Public

2、 Services and Procurement Canada. CGSB is engaged in the production of voluntary standards in a wide range of subject areas through the media of standards committees and the consensus process. The standards committees are composed of representatives of relevant interests including producers, consume

3、rs and other users, retailers, governments, educational institutions, technical, professional and trade societies, and research and testing organizations. Any given standard is developed on the consensus of views expressed by such representatives.CGSB has been accredited by the Standards Council of

4、Canada as a national standards-development organization. The standards that it develops and offers as National Standards of Canada conform to the criteria and procedures established for this purpose by the Standards Council of Canada. In addition to standards it publishes as National Standards of Ca

5、nada, CGSB produces standards to meet particular needs, in response to requests from a variety of sources in both the public and private sectors. Both CGSB standards and CGSB national standards are developed in conformance with the policies described in the CGSB Policy and Procedures Manual for the

6、Development and Maintenance of Standards.CGSB standards are subject to review and revision to ensure that they keep abreast of technological progress. CGSB will initiate the review of this standard within five years of the date of publication. Suggestions for their improvement, which are always welc

7、ome, should be brought to the notice of the standards committees concerned. Changes to standards are issued either as separate amendment sheets or in new editions of standards.An up-to-date listing of CGSB standards, including details on latest issues and amendments, and ordering instructions, is fo

8、und in the CGSB Catalogue at our Web site www.tpsgc-pwgsc.gc.ca/ongc-cgsb/index-eng.html along with more information about CGSB products and services.Although the intended primary application of this standard is stated in its Scope, it is important to note that it remains the responsibility of the u

9、sers of the standard to judge its suitability for their particular purpose.The testing and evaluation of a product against this standard may require the use of materials and/or equipment that could be hazardous. This document does not purport to address all the safety aspects associated with its use

10、. Anyone using this standard has the responsibility to consult the appropriate authorities and to establish appropriate health and safety practices in conjunction with any applicable regulatory requirements prior to its use. CGSB neither assumes nor accepts any responsibility for any injury or damag

11、e that may occur during or as the result of tests, wherever performed.Attention is drawn to the possibility that some of the elements of this Canadian standard may be the subject of patent rights. CGSB shall not be held responsible for identifying any or all such patent rights. Users of this standar

12、d are expressly advised that determination of the validity of any such patent rights is entirely their own responsibility.LanguageIn this Standard, “shall” states a mandatory requirement, “should” expresses a recommendation and “may” is used to express an option or that which is permissible within t

13、he limits of this Standard. Notes accompanying clauses do not include requirements or alternative requirements; the purpose of a note accompanying a clause is to separate from the text explanatory or informative material. Annexes are designated normative (mandatory) or informative (non-mandatory) to

14、 define their application.Further information on CGSB and its services and standards may be obtained from:The Manager Standards Division Canadian General Standards Board Gatineau, Canada K1A 1G6A National Standard of Canada is a standard developed by an SCC- accredited Standards Development Organiza

15、tion (SDO), and approved by the Standards Council of Canada (SCC), in accordance with SCCs: Requirements and Guidance-Accreditation for Standards Development Organizations, and Requirements and Guidance-Approval of National Standards of Canada Designation. More information on National Standard requi

16、rements can be found at www.scc.ca. An SCC-approved standard reflects the consensus of a number of experts whose collective interests provide, to the greatest practicable extent, a balance of representation of affected stakeholders. National Standards of Canada are intended to make a significant and

17、 timely contribution to the Canadian interest. SCC is a Crown corporation within the portfolio of Industry Canada. With the goal of enhancing Canadas economic competitiveness and social well-being, SCC leads and facilitates the development and use of national and international standards. SCC also co

18、ordinates Canadian participation in standards development, and identifies strategies to advance Canadian standardization efforts. Accreditation services are provided by SCC to various customers, including product certifiers, testing laboratories, and standards development organizations. A list of SC

19、C programs and accredited bodies is publicly available at www.scc.ca. Users should always obtain the latest edition of a National Standard of Canada from the standards development organization responsible for its publication, as these documents are subject to periodic review.The responsibility for a

20、pproving standards as NSCs rests with:Standards Council of Canada 55 Metcalfe Street, Suite 600 Ottawa, Ontario K1P 6L5, CANADAby telephone 819-956-0425 or 1-800-665-2472by fax 819-956-5740by mail CGSB Sales Centre Gatineau, Canada K1A 1G6in person Place du Portage Phase III, 6B1 11 Laurier Street G

21、atineau, Quebecby email ncr.cgsb-ongctpsgc-pwgsc.gc.caon the Web www.tpsgc-pwgsc.gc.ca/ongc-cgsb/index-eng.htmlHow to order Publications:Published June 2017 by the Canadian General Standards Board Gatineau, Canada K1A 1G6 HER MAJESTY THE QUEEN IN RIGHT OF CANADA, as represented by the Minister of Pu

22、blic Services and Procurement, the Minister responsible for the Canadian General Standards Board (2017).No part of this publication may be reproduced in any form without the prior permission of the publisher.Biodiesel (B100) for blending in middle distillate fuelsCETTE NORME NATIONALE DU CANADA EST

23、DISPONIBLE EN VERSIONS FRANAISE ET ANGLAISE.ICS 75.160.20NATIONAL STANDARD OF CANADA CAN / CGSB3.5242017Supersedes CAN / CGSB3.5242014CAN/CGSB3.5242017 CGSB 2017 All rights reservedCANADIAN GENERAL STANDARDS BOARDCommittee on Middle Distillate Fuels(Voting membership at date of approval)Chair (Votin

24、g)Mitchell, K. Shell Canada (Producer)General interest categoryHanganu, A. Inspectorate A Bureau Veritas Group CompanyHrsant, G. Oleotek Inc.Jskelinen, H. ConsultantJacula, T. Maxxam Analytics Inc. MacLean, G. Intertek Cargo Analytical AssessmentMenard, L. Advanced Engine Technology Ltd.Moser, P. Sa

25、skatchewan Research CouncilPama, M. Certispec Services Inc.Pickard, A.L. ConsultantTalbot, R. Natural Resources CanadaTharby, R.D. Tharby Technology, ConsultantsWispinski, D. InnoTech AlbertaProducer categoryCampbell, S. Advanced Biofuels CanadaCosentino, J. Afton Chemical CorporationGeoffroy, L. Va

26、lero Energy Inc.Gropp, R. GE Water and Process TechnologiesMcKnight, A. Innospec Inc.Morel, G. Canadian Fuels AssociationMunroe, D. Suncor Energy Products PartnershipPaik, N. Biox CorporationPayne, J.P. Infineum Canada Ltd.Pierceall, R. Archer Daniels MidlandPorter, S. Renewable Industries CanadaRic

27、kard, A. RothsayRockwell, G. Imperial Oil Ltd.Taracha, J. The Lubrizol CorporationTetreault, D. Baker HughesTitus, J. Irving Oil Ltd. Vezeau, C. Husky EnergyWhite, M. North AtlanticCAN/CGSB3.5242017 CGSB 2017 All rights reservedRegulator categoryArchambault, R. Gouvernement du Qubec, ministre de lne

28、rgie et des Ressources naturellesParsons, R. Government of Manitoba, Innovation, Energy and MinesRensing, M.J. Government of British Columbia, Ministry of Energy and Mines User categoryBriggs, D. Government of the Northwest Territories,Public Works and ServicesBryksaw, G. General Motors of Canada Co

29、mpanyChabot, D. Canadian Coast GuardCooper, S. Government of NunavutCowan, B. Government of Ontario, Ministry of TransportationKilso, R. Finning CanadaLemieux, J. Public Services and Procurement CanadaPoitras, P. National DefenceWilson, S. Canadian Oil Heat AssociationSecretary (nonvoting)Schuessler

30、, M. Canadian General Standards BoardAcknowledgment is made for the translation of this National Standard of Canada by the Translation Bureau of Public Services and Procurement Canada.CAN/CGSB3.5242017i CGSB 2017 All rights reservedContents Page1 Scope . 12 Normative references . 13 Terms and defini

31、tions . 24 General requirements . 25 Detailed requirements 36 Inspection 57 Options . 58 Precautions 6Annex A (normative) Referenced ASTM International publications 7Annex B (informative) Federal, provincial and other regulations applicable to diesel fuels 9Annex C (informative) Significance of requ

32、irements for biodiesel B100 131 CGSB 2017 All rights reservedCAN / CGSB3.5242017Supersedes CAN / CGSB3.5242014Biodiesel (B100) for blending in middle distillate fuels1 ScopeThis standard applies to one grade of biodiesel that is intended for use as a blending component in middle distillate fuels.Bio

33、diesel meeting this standard is not intended for use as a fuel in its neat form.See Annex B for regulations that apply to diesel fuels.The testing and evaluation of a product against this standard may require the use of materials and/or equipment that could be hazardous. This document does not purpo

34、rt to address all the safety aspects associated with its use. Anyone using this standard has the responsibility to consult the appropriate authorities and to establish appropriate health and safety practices in conjunction with any applicable regulatory requirements prior to its use.2 Normative refe

35、rencesThe following normative documents contain provisions that, through reference in this text, constitute provisions of this National Standard of Canada. The referenced documents may be obtained from the sources noted below.NOTE The addresses provided below were valid at the date of publication of

36、 this standard.An undated reference is to the latest edition or revision of the reference or document in question, unless otherwise specified by the authority applying this standard. A dated reference is to the specified revision or edition of the reference or document in question.2.1 Canadian Gener

37、al Standards Board (CGSB)CAN/CGSB 3.0 Methods of testing petroleum and associated products:No. 28.8 Visual haze rating of liquid fuels No. 142.0 Cold soak filter blocking tendency of biodiesel (B100).2.1.1 SourceThe above may be obtained from the Canadian General Standards Board, Sales Centre, Gatin

38、eau, Canada K1A 1G6. Telephone 8199560425 or 18006652472. Fax 8199565740. Email ncr.cgsbongctpsgcpwgsc.gc.ca. Web site www.tpsgcpwgsc.gc.ca/ongccgsb/indexeng.html.2.2 ASTM InternationalAnnual Book of ASTM Standards (see Annex A).2.2.1 SourceThe above may be obtained from ASTM International, 100 Barr

39、 Harbor Drive, West Conshohocken, PA 194282959, U.S.A., telephone 6108329585, fax 6108329555, Web site www.astm.org, or from IHS Markit, 2001331 MacLeod Trail SE, Calgary, Alberta T2G 0K3, telephone 6132374250 or 18002678220, fax 6132374251, Web site .2CAN/CGSB3.5242017 CGSB 2017 All rights reserved

40、2.3 European Committee for Standardization (CEN) EN 14107 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of phosphorous content by inductively coupled plasma (ICP) emission spectrometryEN 14110 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of methan

41、ol contentEN 14112 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of oxidation stability (accelerated oxidation test)EN 14538 Fat and oil derivatives. Fatty acid methyl ester (FAME). Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inducti

42、vely coupled plasma (ICP OES)EN 15751 Automotive fuels. Fatty acid methyl ester (FAME) fuel and blends with diesel fuel. Determination of oxidation stability by accelerated oxidation method.2.3.1 SourceThe above may be obtained from the European Committee for Standardization (CEN) National Members,

43、CEN/TC19 Secretariat (astmnen.nl.) Web site www.cen.eu.3 Terms and definitionsFor the purposes of this National Standard of Canada, the following terms and definitions apply.3.1biodieselmonoalkyl esters of longchain fatty acids derived from renewable sources. In its neat form, biodiesel is commonly

44、designated as B100. In the context of this standard the biodiesel is intended as a blending component in a finished diesel fuel or heating oil.3.2diesel fuelmiddle distillate fuel composed of hydrocarbons and naturally occurring, petroleumderived nonhydrocarbons that boils in the range of 130400C an

45、d that is intended for use as a fuel in classical compressionignition engines.3.3heating fuel oildistillate fuel oil intended for use in liquidfuelburning equipment for the generation of heat for domestic and industrial purposes.3.4middle distillate fuelfuel boiling in the range of 130400C composed

46、of hydrocarbons, including naturally occurring, petroleumderived, nonhydrocarbons.4 General requirements4.1 The biodiesel specified shall be long chain alkyl esters and may contain additives designed to improve its properties or performance, for example, diesel ignition quality, lowtemperature flow

47、properties and electrical conductivity. 4.2 The biodiesel shall be a stable homogeneous liquid free from foreign matter that is likely to clog filters or nozzles, or to damage equipment. Haze may be assessed using CAN / CGSB3.0 No. 28.8 or ASTM D4176, Procedure 2.CAN/CGSB3.52420173 CGSB 2017 All rig

48、hts reserved4.3 There shall be no intentional addition of used lubricating oils, used solvents, triglycerides (such as raw vegetable oils, animal fats, fish oils or used cooking oils), or other fluids which are not normal components of the biodiesel.5 Detailed requirementsFor an explanation of the s

49、ignificance of tests and the methods used in this standard, see Annex C.NOTE The precision statement of some of the quoted test methods in this standard may not be fully applicable.5.1. The biodiesel meeting this standard may contain up to 0.5% by volume middle distillate. Metered volumes shall be reported. 5.2 Specified limiting values5.2.1 The biodiesel shall comply with the specified limiting values. The specified limiting values shall n

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