GOST 16273 1-2014 Selenium technical Method of spectral analysis《硒技术 谱分析方法》.pdf

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1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 16273.1 2014 16273.12014 II , 1.092 . 1.22009 . , . , , , 1 368 2 503 3 , ( 30 2014 . 67-) : ( 3166) 00497 ( 3166) 00497 AM BY KG RU TJ UZ 4 26 2014 . 1775- 16273.12014 1 2015 . 5 16273.185 , . () . , , 2015 , 16273.1201

2、4 1 Selenium technical. Method of spectral analysis 20150901 1 , , , , , , , , , , , , , , , 1. 1 C 0,0002 0,010 . 0,0002 0,0050 . 0,001 0,010 . 0,0002 0,010 . 0,0005 0,20 . 0,0002 0,0050 . 0,002 0,20 . 0,0005 0,10 . 0,001 0,20 . 0,0002 0,0050 . 0,0005 0,010 . 0,0005 0,010 . 0,0005 0,010 . 0,0002 0,

3、0050 . - 0,0005 0,0050 . 0,0002 0,0050 . 0,0002 0,0050 . - 0,0002 0,0050 . 0,0002 0,0050 . 0,0005 0,020 . - 0,0002 0,0050 . 0,0002 0,0050 . , , 25086, 16273.0. 2 : 177074 . , , , . 423377 . . 670972 . 914780 . 1015779 . 1112584 . 1426177 . 16273.12014 2 16273.085 . 1830087 . 2346379 . 241042001* . 2

4、50862011 . 2533682 . , 2922791 ( 835-181) . . 1. 5725-62002* ( ) . 6. , 1 , , . (), , () . , , , , . 3 3.1 , , , , , , , 1. 3.2 , , , , , , , 2 ( = 0,95). = 0,95 2. 2 , , , , , , , = 0,95 ( ) , , , r (n=2) , R 0,0002 0,010 . 0,4 *0,3 0,5 0,001 0,010 . 0,0005 0,20 . 0,002 0,20 . 0,001 0,20 . 0,0005 0

5、,010 . 0,0005 0,010 . 0,4 *0,3 0,5 * * 532282008 . 1. . . * 5725-62002 ( ) . 6. . 16273.12014 3 3.3 , , , : - c ; - , 100 105; - 24104; - , , -35, -6; - ; - ; - 1, 12, 6 , 35 55 , 4 , 4 ; - ; - 2502 1770; - -210013/23 25336; - 1221, 1222, 1225, 12210 29227. , : - 6709; - 18300; - 4233 - 23463; - 99,

6、9 %; - 99,9 %; - 99,9 %; - (III) 99,9 %; - 99,9 %; - 99,9 %; - 2; - 3. 1 , , , . 2 , , , . 3.4 . 3.5 3.5.1 . 3. 3 - , 6 8 , , , 0,017 , 5 , 250 , 35 . , 4. 3.5.2 16273.12014 4 . . 3.5.3 . . 4 - , 308,215 266,039 302,064 259,940 327,396 223,015 282,437 234,984 253,652 283,305 266,315 287,331 238,578

7、214,726 , . 3.5.4 . . , , , , , 10 1, 5. 5 - 10* 9* 8* 7* 6 5 4 3 2 1 0,2 0,1 0,05 0,02 0,01 0,005 0,002 0,001 0,0005 0,0002 * , . 3.6 3.6.1 16273.0. 3.6.2 , . 3.6.3 1:1, (10 % ) (0,3 , 0,3 0,6 ) . . , 1:1 (10 % ). 3.6.4 . . 3.7 3.7.1 . 3.7.2 , 16273.12014 5 ( = 0,95) r, 2. , , 5725-6 ( 5.2.2.1). 3.7.3 , , , 2. . , 5725-6. 4 4.1 , 1. 4.2 , 6 ( = 0,95). = 0,95

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