GOST 32797-2014 Food products food raw materials Method of determination of the chynolony content by high performance liquid chromatography with mass spectrometry detector《食品 食品原材料.pdf

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3、( -/) 1 2000 /.2 : 12.1.00588 . - 12.1.00776 . . - 12.1.01893 . - . 12.1.0192009 . . 12.2.0852002 , . . - OIML R 76-12011 . . 1. . 177074 ( 104283, 478880) ., , , . 260379 . . 423377 . . 5725-62003 ( ) . 6. 584873 . . 670972 . 726979 . - 1386768 . 197922001 . 1 327972014 20160101 2230076 . . 2410420

4、01* . 2414780 . 2533682 . , 2680986 . , 2775288 - , -. 2922791 ( 835-181) . . 1. 313392006 , . 314672012 , . - , 1 , - . - (), () . , , , , .3 - , - .4 4.1 :- .20C30C;- .84106;- 200240;- .4951;- 40%80%.4.2 , - .4.3 1- 2- 12.1.007, , 12.1.005.4.4 , , - .4.5 .4.6 12.2.085.4.7 - - 12.1.019, 12.1.018 .4

5、.8 -/ , -/ .* 532282008 . 1. . .2 3279720145 , , 5.1 -, :- - 5 1200 (. . .), - 1200, 0,2 . . ., ( /);- , - , , (45,0 c177 0,8) C;- - 150 5,0 ;- - ;- - 27752;- OIMLR 76-1 c1770,01 24104, - , 200 0,1 ;- , 52 , c1770,001 ;- 40 C;- - 200 5000 /;- () 3 150 2000 /;- 10000 / 4 C 20 C, 15 3- 1,5 3;- 20 1 3;

6、- 20 280 / - 30 C 100 C;- 2,510,0 3,5253, 20100 3,2001000 3 1%;- () 2 3 - 9 ;- 1,5 3;- 15 3 ;- 21014/23 1770;- 125(1000)2 1770;- 125(50, 1000)1 1770;- 125029/32 25336;- 29227;- 50 C 200 C;- ;- - 0 C 5 C;- - 30 C 40 C.5.2 :- 22300, . .;- 2603;- , . . .;- 4233, . .;3 327972014-,.;- 5848, . . .;- 6709;- , . .;- , . . .;- , 28 %. 2 (. .) 3 (. . .) 13867.5.3 -:5.3.1 :- 99,9 %;- 99,8 %;- 99,0 %;- 99,9 %;- 99,9 %;- 99,9 %;- 99,3 %;- 99,9 %;- 97,2 %;- 99,9 %;- 99,9 %;- 99,9 %;- 99,9 %.5.3.2 99,9 %:- D3 ;- D5;- D5;- D5;- D8 ;- D8;- D5 .5.4 , , , , -.6 6.1 6.1.1 , - . .6.1.2