GOST R 54760-2011 Milk products and infant milk products Method for determination of mass concentration of mono- and disugar using high performance liquid chromatography《乳制品和婴儿乳制品 .pdf

1、 - 547602011 27 2002 . 184- , 1.02004 . 1 - ( )2 470 3 - 13 2011 . 949-4 - , - . () . - , , 2012 , - - II 547602011 - Component milk products and infant milk products. Determination of mono- and disugars mass concentration byhigh-performance liquid chromatographic method 201301011 - ( ) - (). - 50,0

2、 10000,0 /3.2 : 12.1.0192009 . . 5725-62002 ( ) . 6. 525012005 ( 3696:1987) . 532282008 . 1. - . 12.1.00491 . . 12.1.00588 . - 12.1.00776 . . - 12.4.00983 . -. . 12.4.02175 . . 6175 . . 177074 . , , , -. 670972 . 1202676 . 1392884 . , - 1491983 , . - .1 547602011 2533682 . , 2680986 . , 2775288 - ,

3、-. 2916991 ( 64877) . 2922791 ( 835-181) . . 1. - - , 1 , , . (), - () . , , - , , .3 , - 1, :3.1 : , , , , (400 ) ( 1,8 ).4 , - , - . - , . .5 , , , , :- 300 , 78 ;- 300 , 46 , ;- 300 , 46 , ;- 5 c180 109;- ;- , 0,30,6 3/, 1 % 1,5 4,0 ;- , - (85 c177 2) C;- 0,020 3;- , - 1.5 . 53228 - c177 0,001 ,

4、c177 0,2 . 0,0401,000 3 - c177 1%.2 547602011 0,100 3. - 27752. 14919. 2 3. 1-50-2, 1-100-2, 1-250-2, 1-1000-2 1770. 1-50-2, 1-100-2 1770. 1-1-2-10 29227. 1(2)-2-5, 1(2)-2-10, 2-2-20 29169. -1-50-19/26 (-1-25-19/26 ) 25336. -56-80 25336. 25336. 0,45 . 12026, 12,5 . 0,5 . , 99,999 %. 61. 24-. 99,0 %.

5、 () 52501. 6709. , , - - , .6 13928 26809.7 7.1 100 3 75 - . . 4 C 6 C 7 .7.2 (91,00 c177 0,01) , (54,60 c177 0,01) 24- 58,1 3 1000 3 . . 4 C 6 C 10 .7.3 , 250, 500, 750 1000 1000 3- , 5, 10, 15 20 3 - , 7.1, , . 50 3 15 3 - .7.3.1 , 250 1000 37.3.1.1 , 15 3, 5 3 - ( 7.1) . 15 3 .7.3.1.2 5,5 3 - 7.2

6、 . -. 1 (23 c177 2) C 12,5 , 5 3.3 5476020117.3.2 , 500 1000 3 , 15 3, 10 3 7.1 . 10 3 , -, . 7.3.1.2.7.3.3 , 750 1000 3 , 15 3, 15 3 7.1 . 5 3 , -, . 7.3.1.2.7.3.4 , 1000 1000 3 , 15 3, 20 3 7.1 . 5 3 , -, . 7.3.1.2.7.3.5 .7.4 , 30 -. . .7.5 7.5.1 (20 c177 2) C . , (40 c177 2) C, - ( ), (20 c177 2)

7、 C.7.5.2 (15.000 c177 0,001) 7.5.1 50 3. 20 3 . 5,5 3 7.2 . - . 1 (23 c177 2) C, , 5 3.7.6 , - .7.6.1 - 0,30,6 3/;- 85,0 C;- : ;- : .7.6.2 , . - . , - . 5,00 %. , , - b Y=a+b. :Y = a+ b, (1) Y ; b ; , /3.7.6.3 1 , -, .4 5476020118 :- (20c177 5) C;- (55c177 25) %;- (96c177 10) ;- .(50c177 5) ;- .(220 c177 10) . , :