1、Recommended Practice for Field Testing Oil-based Drilling FluidsAPI RECOMMENDED PRACTICE 13B-2FIFTH EDITION, APRIL 2014ERRATA 1, AUGUST 2014Special NotesAPI publications necessarily address problems of a general nature. With respect to particular circumstances, local,state, and federal laws and regu
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17、es the Fourth Edition of API Recommended Practice 13B-2.iiiContentsPage1 Scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 Normative References. . . . . . . . . . . . . . . . .
18、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 Terms and Definitions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Symbols and Abbreviations. . .
19、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34.1 Symbols . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34.2
20、Abbreviations. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95 Determination of Drilling Fluid Density (Mud Weight). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
21、. . 105.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105.2 Apparatus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
22、. . . . . . . . . . . . . . . . . . . . . . . . . 105.3 Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105.4 Calculation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
23、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 116 Alternative Method for Determination of Drilling Fluid Density. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 136.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
24、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 136.2 Apparatus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 136.3 Procedure. . . . . .
25、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 136.4 Calculation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
26、. . . . . . . . 147 Viscosity and Gel Strength. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 147.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
27、. . . . . . . . . . . . . . . . . . . . . . . . 147.2 Determination of Viscosity Using the Marsh Funnel. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 147.3 Determination of Viscosity and Gel Strengths Using a Direct-reading Viscometer . . . . . . . . . . . . .
28、. . . . 158 Static Filtration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 188.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
29、 . . . . . . . . . . . . . . . . . . . . . . . . . 188.2 High-temperature/High-pressure Test up to 175 C (350 F) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 198.3 High-temperature/High-pressure Test 175 C (350 F) up to and Including 230 C (450 F). . . . . . . . . . . 229
30、Retort Test for Oil, Water, and Solids Concentrations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 249.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
31、. . . . . 249.2 Apparatus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 259.3 Procedure-Volumetric Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
32、. . . . . . . . . . . . . . . . . . . 269.4 Calculation-Volumetric Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 279.5 Procedure-Gravimetric Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
33、 . . . . . . . . . . . . . . . . . . . . . . . . 299.6 Calculation-Gravimetric Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 319.7 Calculation-Volume Fractions of Oil, Water, and Solids . . . . . . . . . . . . . . . . . .
34、 . . . . . . . . . . . . . . . . . . . . . . 3210 Chemical Analysis of Oil-based Drilling Fluids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3410.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
35、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3410.2 Reagents and Apparatus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3510.3 Base alkalinity demand (BAD), VB . . . . . . . . . . . . . . . . .
36、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3610.4 Whole-drilling-fluid Alkalinity, VK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3710.5 Whole-drilling-fluid Chloride Concentration . . . . .
37、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3910.6 Whole-drilling-fluid Calcium Concentration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4011 Electrical Stability Test . . . . . . . . . . . . . . . .
38、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4111.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4111.2 Apparatus . . .
39、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4111.3 Equipment Calibration/Performance Test. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
40、211.4 Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42vContentsPage12 Lime, Salinity, and Solids Calculations. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
41、. . . . . . . . . . . . . . . . . . 4312.1 Principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4312.2 Apparatus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
42、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4412.3 Whole-drilling-fluid Calculations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4412.4 Aqueous Phase Calculations. . . . . . . . . . . .
43、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4712.5 Soluble and Insoluble Whole-drilling-fluid Sodium Chloride Calculations . . . . . . . . . . . . . . . . . . . . . . . . 5112.6 Calculation-Solids in the Whole Drilling Fluid . . . . . . . . . .
44、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53Annex A (informative) Measurement of Shear Strength Using Shearometer Tube . . . . . . . . . . . . . . . . . . . . . . 58Annex B (informative) Determination of Oil and Water Retained on Cuttings. . . . . . . . . . . . . .
45、 . . . . . . . . . . . . . 60Annex C (informative) Determination of Aqueous-phase Activity of Emulsified Water Using an Electro Hygrometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65Annex D (informativ
46、e) Determination of Aniline Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68Annex E (informative) Lime, Salinity, and Solids Calculations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71Annex F (informative) Sampling
47、, Inspection, and Rejection of Drilling Materials. . . . . . . . . . . . . . . . . . . . . . . . 84Annex G (informative) Rig-site Sampling. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86Annex H (informative) Determination of Cutting
48、s Activity by the Chenevert Method . . . . . . . . . . . . . . . . . . . . 89Annex I (informative) Chemical Analysis of Active Sulfides by the Garrett Gas Train Method. . . . . . . . . . . . . 93Annex J (informative) Calibration and Verification of Glassware, Thermometers, Viscometers, Retort Kit Cu
49、p, and Drilling Fluid Balances . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98Annex K (informative) High-temperature/High-pressure Filtration Testing of Drilling Fluids Using the Permeability-plugging Apparatus (PPA). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103Annex L (informative) Compatibility of Elastomeric Materials with Non-aqueous-Based Drilling Fluids . . . 115Annex M (informative) Sand Content Procedure for Non-aqueous Fluids. . . . . . . . . . . .
