1、Designation: C1506 09Standard Test Method forWater Retention of Hydraulic Cement-Based Mortars andPlasters1This standard is issued under the fixed designation C1506; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last
2、revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope*1.1 This test method provides for the determination of waterretention of hydraulic cement-based mortars and plasters.1.2 The v
3、alues stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate
4、safety and health practices and determine the applica-bility of regulatory limitations prior to use. (WarningFreshhydraulic cementitious mixtures are caustic and may causechemical burns to skin and tissue upon prolonged exposure.)22. Referenced Documents2.1 ASTM Standards:3C109/C109M Test Method for
5、 Compressive Strength ofHydraulic Cement Mortars (Using 2-in. or 50-mm CubeSpecimens)C185 Test Method for Air Content of Hydraulic CementMortarC230/C230M Specification for Flow Table for Use in Testsof Hydraulic CementC305 Practice for Mechanical Mixing of Hydraulic CementPastes and Mortars of Plast
6、ic ConsistencyC511 Specification for Mixing Rooms, Moist Cabinets,Moist Rooms, and Water Storage Tanks Used in theTesting of Hydraulic Cements and ConcretesC670 Practice for Preparing Precision and Bias Statementsfor Test Methods for Construction MaterialsC1437 Test Method for Flow of Hydraulic Ceme
7、nt Mortar3. Summary of Test Method3.1 The flow of the mortar or plaster is determined. Themortar or plaster is then subjected to a controlled vacuumsuction for 60 s, after which the flow is again determined. Thewater retention is the final flow divided by the initial flowexpressed as a percentage.4.
8、 Significance and Use4.1 This test method provides a means for determining theability of mortars and plasters to retain water under suction.Test results may be used to determine compliance withspecifications.4.2 The results obtained using this test method can be usedto compare the relative ability o
9、f mortars and plasters to retainwater under suction.4.3 The results obtained using this test method for masonrymortars do not necessarily indicate the degree of waterretention when used with masonry units, since the amount ofwater absorbed by the unit depends on the rate of absorption ofthe masonry
10、unit.4.4 The results obtained using this test method for plasters(stucco) do not necessarily indicate the degree of waterretention when the plaster is applied as a second coat on thesurface of a previously applied plaster base coat, since theamount of water absorbed from the second coat of plasterde
11、pends on the rate of absorption of the base coat. This is alsotrue when a plaster is applied as a coating on masonry units.5. Apparatus5.1 Tamper, conforming to Test Method C109/C109M.5.2 Straightedge, conforming to Test Method C185.5.3 Flow Table, conforming to Specification C230/C230M.5.4 Mixing A
12、pparatus, conforming to the requirements pre-scribed in Practice C305.5.5 Filtration Assembly, an apparatus essentially as shownin Fig. 1 shall be used. This apparatus consists of a perforateddish resting on a funnel, which is connected by a three-waystopcock to a vacuum flask, to which a controlled
13、 vacuum isapplied. The perforated dish shall be made of metal notattacked by masonry mortar or plaster (Note 1). The metal baseof the dish shall have a thickness of 2.0 6 0.3 mm and shallconform to the requirements given in Fig. 1. The stopcock bore1This test method is under the jurisdiction of ASTM
14、 Committee C01 on Cementand is the direct responsibility of Subcommittee C01.22 on Workability.Current edition approved Dec. 1, 2009. Published January 2010. Originallyapproved in 2001. Last previous edition approved in 2008 as C150608. DOI:10.1520/C1506-09.2Section on Safety, Manual of Cement Testi
15、ng, Annual Book of ASTMStandards, Vol 04.01.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1*A Summary of Ch
16、anges section appears at the end of this standard.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.shall have a 4.0 6 0.5-mm diameter, and the connecting glasstubing shall have a minimum inside diameter of 4 mm. Thelength of the tubing
17、 projecting into the 1-L flask from thestopcock shall extend at least 25 mm below the center line ofthe vacuum connection. The contact surfaces of the funnel andperforated dish shall be plane and may need to be lapped toensure intimate contact. An airtight seal shall be maintainedbetween the funnel
18、and the dish during the test. This shall beaccomplished by either of the following procedures. (1)Asynthetic (grease-resistant) rubber gasket may be permanentlysealed to the top of the funnel using petrolatum or light greaseto ensure a seal between the gasket and dish. (2) The top of theNOTEThe gask
19、et is to be synthetic rubber. The stopcock and the bore of the tubing shall be at least 4-mm. A check valve or water trap, or both, issuggested for the connection to the vacuum source.FIG. 1 Apparatus Assembly for the Water-Retention TestC1506 092funnel may be lightly coated with petroleum or light
20、grease toensure a seal between the funnel and dish. Care should be takento ensure that none of the holes in the perforated dish becomeclogged. Hardened, smooth, not rapid filter paper shall be used.It shall be 150 mm in diameter and be placed so as tocompletely cover the perforations in the dish.NOT
21、E 1Stainless steel, brass, and bronze are suitable metals for thispurpose.5.6 Controlled Vacuum Source:5.6.1 A vacuum gage capable of reading at least 9-kPapressure in 0.1-kPa increments (Note 2 and Note 3), connectedto a miniature vacuum regulator having a maximum 55-kPacapacity, which is then conn
22、ected to a vacuum pump or wateraspirator as shown in Fig. 1. Connection is made between thevacuum flask and the vacuum gage.NOTE 2Vacuum values are all given as pressure relative to atmo-spheric pressure.NOTE 3Gages reading pressure in other units are acceptable as longas their capacity and scale in
23、crements comply with the levels specifiedhere. (For example, a vacuum gage with a minimum capacity of 70 mmof Hg in 1-mm increments is acceptable. To convert mm of Hg to kPa,multiply by 0.1333. Thus the 7.0-kPa starting pressure is equivalent to53-mm Hg.)6. Temperature and Humidity6.1 The temperatur
24、e of the mixing room and the roomcontaining the water retention apparatus shall conform to therequirements of Specification C511.7. Materials7.1 The composition of the mortar or plaster to be tested forwater retention shall be that described in the specification ofthe material being considered, or t
25、hat desired.8. Mixing of Mortar and Plaster8.1 The mortar or plaster to be tested for water retentionshall be mixed as specified in the section on Procedure forMixing Mortars of Practice C305, or as described in thespecification for the material being considered.9. Procedure9.1 Preparation of Appara
26、tusSeat the perforated dish onthe greased gasket or greased rim of the funnel. Place a wettedfilter paper in the bottom of the dish. Turn the stopcock toapply the vacuum to the funnel and check the apparatus forleaks. Adjust the vacuum to 7.0 6 0.4 kPa (Note 2). Turn thestopcock to shut off the vacu
27、um from the funnel. Do notremove the dish from the funnel until instructed to do so in 9.5.9.2 Determination of FlowDetermine the flow in accor-dance with Test Method C1437.9.3 Preparation of Mortar or Plaster BedImmediatelyafter making the flow test, return the mortar or plaster on theflow table to
28、 the mixing bowl and remix the entire batch for 15s at medium speed. Immediately after remixing, fill theperforated dish with the material to slightly above the rim.Tamp 15 times with the tamper. Apply ten of the tampingstrokes at approximately uniform spacing adjacent to the rim ofthe dish, and wit
29、h the long axis of the tamping face held at rightangles to the radius of the dish. Apply the remaining fivetamping strokes at random points distributed over the centralarea of the dish. Use just enough tamping pressure to fill thedish with the top of the material extending slightly above therim. Smo
30、oth off the material by drawing the flat side of thestraightedge (with the leading edge slightly raised) across thetop of the dish. Strike-off the material to a plane surface flushwith the rim of the dish with the straightedge held in aperpendicular position; using a sawing motion, draw thestraighte
31、dge across half of the surface of the dish; repeat theprocedure on the other half of the unfinished surface. If thematerial is pulled away from the side of the dish during theprocess of drawing the straightedge across the dish, gentlypress the material back into contact with the side of the dishusin
32、g the tamper. Complete the entire filling and strike-offoperation in not more than 2 min.9.4 Application of Vacuum to Mortar or PlasterTurn thestopcock to apply the vacuum to the funnel. After suction for60 s, quickly turn the stopcock to expose the funnel toatmospheric pressure.9.5 Determination of
33、 Flow After SuctionImmediatelyslide the perforated dish off the funnel, touch the bottom of thedish momentarily on a damp cloth to remove droplets of water.Set the dish on a work table, plow and mix the mortar or plasterfor 15 s, with the rubber scraper prescribed in Practice C305.Determine the flow
34、 in accordance with Test Method C1437.Remove the vacuum and complete the flow test in less than 2min.10. Calculation10.1 Calculate the water retention value for the mortar orplaster as follows:Water retention, % 5 A/B! 3 100where:A = flow after suction, andB = flow immediately after initial mixing.R
35、eport to the nearest 1 %.11. Precision and Bias11.1 PrecisionThe following precision values were cal-culated from results of tests reported to Cement and ConcreteReference Laboratory (CCRL) for masonry cement proficiencysamples Number 3 through 42 (Note 4). Within- and among-laboratory standard devi
36、ations were calculated by CCRL foreach sample pair. Values were pooled over all 40 samples forpurposes of this analysis. Water retention test results (exclud-ing outliers) ranged from 72 to 88 %. The average number oflaboratories reporting was 69.NOTE 4These tests utilized a slightly different test
37、pressure, 6.7 6 0.4kPa (50 6 0.3 mm Hg).11.1.1 Single-laboratory PrecisionThe single-laboratorystandard deviation has been found to be 3.5 % (Note 5).Therefore, the results of two properly conducted tests in thesame laboratory on the same material should not differ by morethan 9.8 % (Note 5) in 95 %
38、 of such pairwise comparisons.11.1.2 Multilaboratory PrecisionThe multilaboratorystandard deviation has been found to be 5.1 % (Note 5).C1506 093Therefore, the results of two properly conducted tests indifferent laboratories on the same material should not differ bymore than 14.3 % (Note 5) in 95 %
39、of such pairwise compari-sons.NOTE 5These numbers represent, respectively, the 1s and d2s limitsas described in Practice C670.11.2 BiasSince there is no accepted reference materialsuitable for determining bias in this test method, no statementon bias is being made.12. Keywords12.1 hydraulic cement;
40、mortar; plaster; water retentionSUMMARY OF CHANGESCommittee C01 has identified the location of selected changes to this test method since the last issue,C1506 08, that may impact the use of this test method. (Approved December 1, 2009)(1) Revised 9.1.ASTM International takes no position respecting t
41、he validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard
42、is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International H
43、eadquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This
44、standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).C1506 094
