1、Designation: D5329 15D5329 16Standard Test Methods forSealants and Fillers, Hot-Applied, for Joints and Cracks inAsphalt Pavements and Portland Cement ConcretePavements1This standard is issued under the fixed designation D5329; the number immediately following the designation indicates the year ofor
2、iginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 These test methods cover tests for hot-applied types of joint
3、 and crack sealants and fillers for portland cement concrete andasphaltic concrete pavements. There are numerous standard material specifications that use these test methods. Refer to therespective standard material specification of interest to determine which of the following test methods to use. F
4、or sample meltingand concrete block preparation see their respective standard practices.1.2 The test methods appear in the following sections:SectionArtificial Weathering 13Asphalt Compatibility 12Bond, Non-Immersed 8Bond, Water-Immersed 9Cone Penetration, Non-Immersed 6Flexibility 15Flow 7Resilienc
5、e 10Resilience, Oven-Aged 11Tensile Adhesion 141.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibi
6、lityof the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatorylimitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D5 Test Method for Penetration of Bituminous MaterialsD217 Test Methods for Cone Penetration of Lubri
7、cating GreaseD618 Practice for Conditioning Plastics for TestingD1074 Test Method for Compressive Strength of Bituminous MixturesD1561 Practice for Preparation of Bituminous Mixture Test Specimens by Means of California Kneading CompactorD1985 Practice for Preparing Concrete Blocks for Testing Seala
8、nts, for Joints and CracksD3381 Specification for Viscosity-Graded Asphalt Cement for Use in Pavement ConstructionD5167 Practice for Melting of Hot-Applied Joint and Crack Sealant and Filler for EvaluationD6690 Specification for Joint and Crack Sealants, Hot Applied, for Concrete and Asphalt Pavemen
9、tsE145 Specification for Gravity-Convection and Forced-Ventilation OvensG151 Practice for Exposing Nonmetallic Materials in Accelerated Test Devices that Use Laboratory Light SourcesG154 Practice for Operating Fluorescent Ultraviolet (UV) Lamp Apparatus for Exposure of Nonmetallic MaterialsG155 Prac
10、tice for Operating Xenon Arc Light Apparatus for Exposure of Non-Metallic Materials1 These test methods are under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and are the direct responsibility of Subcommittee D04.33 onFormed In-Place Sealants for Joints and Cracks in Pavements
11、.Current edition approved Dec. 15, 2015July 1, 2016. Published February 2016August 2016. Originally approved in 1992. Last previous edition approved in 20092015 asD5329 09.D5329 15. DOI: 10.1520/D5329-15.10.1520/D5329-16.2 For referencedASTM standards, visit theASTM website, www.astm.org, or contact
12、ASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been m
13、ade to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.Co
14、pyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States13. Significance and Use3.1 These test methods describe procedures for determining specification conformance for hot-applied, field-molded joint andcrack sealants and fillers.4. Sample Melt
15、ing4.1 See Practice D5167.5. Standard Conditions5.1 The laboratory atmospheric conditions, hereinafter referred to as standard conditions, shall be in accordance with PracticeD618 (23 6 2C, 50 6 10 % Relative Humidity).6. Cone Penetration, Non-Immersed6.1 ScopeThis test method covers determination o
16、f cone penetration of bituminous joint and crack sealers and fillers.6.2 Significance and UseThe cone penetration, non-immersed is a measure of consistency. Higher values indicate a softerconsistency.6.3 ApparatusConduct this test using the apparatus described in Test Method D5, except as specified
17、herein. Use a penetrationcone in place of the standard penetration needle. The cone shall conform to the requirements given in Test Methods D217, exceptthat the interior construction may be modified as desired. The total moving weight of the cone and attachments shall be 150.0 60.1 g.6.4 Specimen Pr
18、eparationPour a portion of the sample prepared in accordance with Practice D5167 into a cylindrical, metal,flat bottom container of essentially 60 to 75 mm in diameter and 45 to 55 mm in depth and fill flush with the rim of the container.Allow the specimen to cure under standard conditions as specif
19、ied in its respective material specification.6.5 ProcedurePlace the specimen in a water bath maintained at 25 6 0.1C for 2 h immediately before testing. Remove thespecimen from the bath and dry the surface. Using the apparatus described in 6.3, make determinations at three locations onapproximately
20、120 radii, and halfway between the center and outside of the specimen. Take care to ensure the cone point is placedon a point in the specimen that is representative of the material itself and is free of dust, water, bubbles or other foreign material.Clean and dry the cone point after each determinat
21、ion.6.6 ReportAverage the three results and record the value as the penetration of the specimen in 110 mm units.6.7 Precision and Bias:6.7.1 For Specification D6690 Type I materials, the following precision statement is based on an interlaboratory study of 12laboratories that tested five different S
22、pecification D6690 Type I materials.6.7.1.1 Within ContainerSingle-Operator Precision (for penetration between 40 and 80): The single-operator deviation hasbeen found to be 0.994. Therefore, results of two properly conducted tests by the same operator should not differ by more thanthree penetration
23、units.6.7.1.2 Within LaboratoriesSingle-Operator Precision (penetrations 40 to 80): The single-operator standard deviation of asingle test (test result is defined as the average of three penetrations) has been found to be 0.924. Therefore, the results of twoproperly conducted tests by the same opera
24、tor on the same material should not differ by more than three penetration units.6.7.1.3 Multilaboratory Precision(penetration 40 to 80): The multilaboratory standard deviation of a single test (test result isdefined as the average of three penetrations) has been found to be 3.249. Therefore, the res
25、ults of two properly conducted testsin different laboratories should not differ by more than nine penetration units.6.7.2 For Specification D6690Type II materials, the following precision statement is based on an interlaboratory study of elevenlaboratories that tested six different Specification D66
26、90 Type II materials.6.7.2.1 Within ContainerSingle-Operator Precision (for penetration between 55 and 85): The single-operator deviation hasbeen found to be 0.974. Therefore, results of two properly conducted tests by the same operator should not differ by more thanthree penetration units.6.7.2.2 W
27、ithin LaboratoriesSingle-Operator Precision (penetrations 50 to 70): The single-operator standard deviation of asingle test (test result is defined as the average of three penetrations) has been found to be 1.0865. Therefore, the results of twoproperly conducted tests by the same operator on the sam
28、e material should not differ by more than three penetration units.6.7.2.3 Single-Operator Precision(penetrations 71 to 85): The single-operator standard deviation of a single test (test resultis defined as the average of three penetrations) has been found to be 2.237. Therefore, the results of two p
29、roperly conducted testsby the same operator on the same material should not differ by more than six penetration units.6.7.2.4 Multilaboratory Precision(penetration 50 to 70): The multilaboratory standard deviation of a single test (test result isdefined as the average of three penetrations) has been
30、 found to be 5.2609. Therefore, the results of two properly conducted testsin different laboratories should not differ by more than 15 penetration units.D5329 1626.7.2.5 Multilaboratory Precision(penetration 71 to 85): The multilaboratory standard deviation of a single test (test result isdefined as
31、 the average of three penetrations) has been found to be 16.8831. Therefore, the results of two properly conducted testsin different laboratories should not differ by more than 48 penetration units.7. Flow7.1 ScopeThis test method measures the amount of flow of bituminous joint and crack sealants wh
32、en held at a 75 angle atelevated temperatures.7.2 Significance and UseThis test method is a means of measuring the ability of a sealant to resist flow from the joint or crackat high ambient temperatures.7.3 Apparatus:7.3.1 MoldConstruct a mold (see Note 1) 40 mm wide by 60 mm long by 3.2 mm deep and
33、 place it on a bright tin panel. Thetin plate must be free of dirt, oil, and so forth and be between 0.25 to 0.64 mm in thickness.NOTE 1A release agent should be used to coat molds and spacers to prevent them from bonding to the sealants. Extreme care should be exercisedto avoid contaminating the ar
34、ea where the joint sealant makes contact with the blocks. A non-toxic release agent is recommended for this purpose. Twoexamples that have been found suitable for this purpose are KY jelly (available at drug stores) and a release agent prepared by grinding a mixture ofapproximately 50 % talc, 35 % g
35、lycerine, and 15 % by weight, of a water-soluble medical lubricant into a smooth paste.7.3.2 OvenForced draft type conforming to Specification E145 and capable of controlling its temperature 61C.7.4 Specimen PreparationPour a portion of the sample prepared in accordance with Practice D5167 for melti
36、ng samples intothe mold described in 7.3. Fill the mold with an excess of material. Allow the test specimen to cool at standard conditions for atleast 12 h, then trim the specimen flush with the face of the mold with a heated metal knife or spatula and remove the mold.Allowthe specimen to cure under
37、 standard conditions as specified in its respective material specification.7.5 ProcedureMark reference lines on the panel at the bottom edge of the sealant. Then place the panel containing the samplein a forced-draft oven maintained for the time and at the temperature specified in its respective mat
38、erial specification. During thetest, mount the panel so that the longitudinal axis of the specimen is at an angle of 75 6 1 with the horizontal, and the transverseaxis is horizontal. After the specified test period, remove the panel from the oven and measure the movement of the specimenbelow the ref
39、erence lines in millimetres.7.6 ReportReport the measurement obtained in 7.5 in millimetres.7.7 Precision and Bias:7.7.1 For Specification D6690 Type I materials, the following precision statement is based on an interlaboratory study of 12laboratories that tested five different Specification D6690 T
40、ype I materials.7.7.1.1 Single-Operator Precision (flow 0 to 5)The single-operator standard deviation has been found to be 0.255. Therefore,the results of two properly conducted tests by the same operator should not differ by more than one flow unit.7.7.1.2 Single-Operator Precision (flow 5 to 10)Th
41、e single-operator standard deviation has been found to be 1.024. Therefore,the results of two properly conducted tests by the same operator should not differ by more than three flow units.7.7.1.3 Multilaboratory Precision (flow 0 to 5)The multilaboratory standard deviation has been found to be 4.256
42、. Therefore,the results of two properly conducted tests in different laboratories should not differ by more than 12 flow units.7.7.1.4 Multilaboratory Precision (flow 5 to 10)The multilaboratory standard deviation has been found to be 5.326. Therefore,the results of two properly conducted tests in d
43、ifferent laboratories should not differ by more than 15 flow units.7.7.2 For Specification D6690Type II materials, the following precision statement is based on an interlaboratory study of elevenlaboratories that tested six different Specification D6690 Type II materials.7.7.2.1 Single-Operator Prec
44、ision (flow 0 to 1)The single-operator standard deviation has been found to be 0.2494. Therefore,the results of two properly conducted tests by the same operator should not differ by more than one flow unit.7.7.2.2 Single-Operator Precision (flow 1.1 to 4)The single-operator standard deviation has b
45、een found to be 0.7616.Therefore, the results of two properly conducted tests by the same operator should not differ by more than three flow units.7.7.2.3 Multilaboratory Precision (flow 0 to 1)The multilaboratory standard deviation has been found to be 0.5644. Therefore,the results of two properly
46、conducted tests in different laboratories should not differ by more than three flow units.7.7.2.4 Multilaboratory Precision (flow 1.1 to 4)The multilaboratory standard deviation has been found to be 2.3508.Therefore, the results of two properly conducted tests in different laboratories should not di
47、ffer by more than seven flow units.8. Bond, Non-Immersed8.1 ScopeThis test method is used to evaluate the bond to concrete.8.2 Significance and UseBond to concrete is necessary for a sealant to maintain proper field performance.8.3 Apparatus:8.3.1 Extension MachineThe extension machine used in the b
48、ond test shall be so designed that the specimen can be extendeda minimum of 12.5 mm at a uniform rate of 3.1 6 0.3 mm per hour. It shall consist essentially of one or more screws rotated byD5329 163an electric motor through suitable gear reductions. Self aligning plates or grips, one fixed and the o
49、ther carried by the rotating screwor screws, shall be provided for holding the test specimen in position during the test.38.3.2 Cold ChamberThe cold chamber shall be capable of maintaining the required cold test temperature within 61C.8.4 Concrete-Block PreparationThe concrete blocks shall be prepared in accordance with Practice D1985.8.5 Specimen Preparation:8.5.1 Prepare three test specimens (3 specimens 2 = 6 blocks) as follows: On removal from the storage container, again scrubthe 50 by 75 mm saw-cut faces of the blocks under r
