1、Designation: E205 96 (Reappproved 2010)Standard Specification forGlass and Oxygen Combustion Flask1This standard is issued under the fixed designation E205; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision.
2、 A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers the flask and closure, with afixed platinum sample holder, used in the original oxygen-flaskcombustion pro
3、cedures (1, 2).2NOTE 1This specification was originally developed by the Committeeon MicrochemicalApparatus, Division ofAnalytical Chemistry,AmericanChemical Society (3). Specifications for types of apparatus that utilizeelectric (2, 4-7) or infrared (8) ignition are not included because of lack ofe
4、xperience with these.1.2 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.2. Referenced Documents2.1 ASTM Standards:3E920 Specification for Commercially Packaged LaboratoryApparatusE921 Specification for Export Packaged Laborator
5、y Appa-ratusE1133 Practice for Performance Testing of Packaged Labo-ratory Apparatus for United States Government Procure-mentsE1157 Specification for Sampling and Testing of ReusableLaboratory Glassware3. Combustion Flasks3.1 Combustion flasks shall be of borosilicate glass andshall conform to the
6、requirements shown in Fig. 1 for the 300and 500-ml sizes, respectively.NOTE 2Larger flasks (1000 and 2000-ml sizes) have been used,particularly when analyses are done on tissue.4. Flask Closure4.1 The flask closure, that is used with either size flask, shallbe of borosilicate glass and shall be prov
7、ided with a fixedplatinum sample holder and shall conform to the requirementsshown in Fig. 1. WarningAlthough broad usage has shownoxygen flask combustion to be generally safe, precautions,such as use of gloves, goggles, shields, and so forth, should betaken when using these flasks for this purpose.
8、5. Sampling and Testing5.1 Refer to Specification E1157.6. Packaging6.1 Select from one of Specification E920, SpecificationE921, or Practice E1133.7. Keywords7.1 combustion; flask; glass; oxygen1This specification is under the jurisdiction of ASTM Committee E41 onLaboratory Apparatus and is the dir
9、ect responsibility of Subcommittee E41.01 onApparatus.Current edition approved July 1, 2010. Published July 2010. Originally approvedin 1962. Last previous edition approved in 2005 as E205 96 (2005). DOI:10.1520/E0205-96R10.2The boldface numbers in parentheses refer to the list of references appende
10、d tothis specification.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Bar
11、r Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.REFERENCES(1) Schniger, W., “Eine mikroanalytische Schnellbestimmung von Halo-gen in organischen Substanzen,” Mikrochimica Acta, Issue 1, 1955, p.123. “Die mikroanalytische Schnellbestimmung von Halogenen undSchwefel in org
12、anischen Verbindungen,” Mikrochimica Acta, Issues16, 1956, p. 869.(2) Steyermark, Al, Quantitative Organic Microanalysis, 2nd Ed., Aca-demic Press, New York, NY, 1961, p. 292.(3) Committee on Microchemical Apparatus, Division of AnalyticalChemistry, American Chemical Society, “Report on RecommendedS
13、pecifications for Microchemical Apparatus, Oxygen Flask Combus-tion,” Analytical Chemistry, Vol 33, November 1961, p. 1789.(4) Cheng, F. W., and Smullin, C. F., “An Apparatus for the FlaskCombustion of Organic Compounds Adaptable to Carbon Determina-tion,” Microchemical Journal, Vol 4, Issue 2, 1960
14、 p. 213.(5) Juvet, R. S., and Chiu, J., “Determination of Carbon in OrganicSubstances by an Oxygen-Flask Method,” Analytical Chemistry,Vol32, January 1960, p. 130.(6) Martin, A. J., and Deveraux, H., “Electric Ignition in the SchnigerOxygen Flask Method,” Analytical Chemistry, Vol 31, December1959,
15、 p. 1932.(7) Weir, H. E., “A Compact Igniter and Safety Shield for the ImprovedSchniger Apparatus,” Microchemical Journal, Vol 6, Issue 1, 1962,p. 109.(8) Ogg, C. L., Kelly, R. B., and Connelly, J. A., “Apparatus for Safe,Oxygen-Filled Flask Combustion,” Proceedings, 1961 InternationalSymposium on M
16、icrochemical Techniques, Microchemical Journal,Symposium Series, edited by Cheronis, N. D., Interscience Publishers,New York, NY, London, England, Vol II, 1962, p. 427.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin t
17、his standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must
18、be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of there
19、sponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700,
20、West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).FIG. 1 Oxygen-Combustion Flasks and ClosureE205 96 (Reappproved 2010)2
