1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32710 2014 13/12 327102014 II , - 1.092 . 1.22009 . -, . , , , 1 - - , - ( ) 2 3 , (- 30 2014 . 67-) : ( 3166) 00497 ( 3166) 00497 AM BY KG MD - RU UA 4 25 2014 . 669- 327102014 - 1 2016 . 18 2014 . 1649- 327102014 1 201
2、6 . 1 2015 . 5 - , - . () - . , - - , 2014 -, - 327102014 1 13/12 Alcoholic beverages and raw materials for its production. Identification. Method for determination of alcohols and sugars 13C/12C isotopes ratio in wines and mashes 20150101 1 , , - , - 13/12 ( 13VPDB) . , , , - 13VPDB 29 26, , . 13/1
3、2 / . 2 : 12.0.00490 . - . 12.1.00491 . . 12.1.00588 . - 12.1.00776 . . 12.2.007.075 . . 12.2.0852002 , . . - 12.4.00983 . -. . 12.4.02175 . . 12.4.10383 . , . 177074 ( 104283, 478880) . -, , , . 558378 ( 204673) . 670972 . 805085 . 2533682 . , 2631384 . 327102014 2 2849890 . - . 2916991 ( 64877) .
4、. 317302012 . - - - , 1 , . (), () . , , , , . 3 , 3.1 - : 3.1 13VPDB: , - , , . 3.2 PDB: Belemnitella Americana PDB ( , ). PDB . - PDB-VPDB. 13VPDB - ,100012131213121313VPDBVPDBVPDBCCCC (1) VPDB1213 13 12 , - 0,0112372. 3.3 : . 4 - , 44, 45, 46, - 2, - , - PDB (13VPDB). 5 , , , 5.1 - - : - , . . .
5、170; - (/), 900; 327102014 3- , /, ( 10 % m/z 44), 95; - (13/12), , : 0,01, 0,1. , : - IAEA-CH-6 Sucrose () 506, 13CVPDB ; - NBS22 Oil () 427, 13CVPDB . 1-1-1-1, 1-1-1-2, 1-2-1-25 29227. -1-50-14/23 25336. -1-50-14/23 25336. -1-500-29/32 25336. -1-250-29/32 25336. -1-2000-29/32 25336. -1-250-29/32 2
6、5336. -1-400-14/23-14/23 25336. 1-200-14/23 25336. 1- 28498, 0 100 , 0,5 . , , -. 150-14/23-14/23 25336. 1-14/23-14/23-14/23 25336. 29/32-14/23-100 25336. -1-19/26-14/23 25336. -14/23-14/23-50 25336. -14/23-14/23-50 25336. -29/32 25336. 1-250-1 1770. 1-1-25 29169. . . . (. . .), 99,995 % 8050. . (.
7、. .), 99,995 % 5583. , 99,9999 % , , . 6709. . , - , , -, . 6 31730. - 26313. 7 7.1 . 7.2 : - , 1000; - () , 3105;- () - , 1,1105; 327102014 4 - (2) , 200; - , 3 0,001. 7.3 , , - -. 132 - . 132 . . 132 0,5 . 7.4 7.4.1 50 3 25 3 - 78,0 78,5 , 98 % (. , .1). , , . 7.5 7.5.1 500 3 250 3 - , 120150 3. . 200 3. 7.5.2 - 250 3 , 1 (. 5.1). 18 22 . : , , . 7.5.3 7.4.1. - . 7.6 7.6.1 : 1000 3 2000 3, 1 (. 5.1). - 18 22 . : - , , - . 7.6.1.1 7.4.1. - . 7.6.2 / - : 250 3- / 2000 3, 1000 3 , 1 (. 5.1). 18 22 . :
