KS I 3217-2008 Testing methods for industrial wastewater《工厂废水试验方法》.pdf

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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS I 3217 KS I 3217:2008 2008 11 24 http:/www.kats.go.krKS I 3217:2008 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : : 1975 12 26 : 2008 11 24 2008-0794 : : ( 02-509-7266) (http:/www.kats.go.kr). 10 5 , . KS I 3217:2008 i 1 1 2 1 3 .1 4 3 4.1 4 4.2 16 4.3 .16

2、 4.4 17 5 .20 5.1 .20 5.2 .27 5.3 .28 5.4 .30 5.5 30 6 34 7 35 8 35 8.1 .36 8.2 .36 9 38 9.1 .38 9.2 (TO)38 10 .40 10.1 Y x, y 40 11 pH 45 11.1 45 12 ( )48 13 50 13.1 .50 13.2 51 13.3 pH 7 .52 13.4 53 13.5 53 13.6 .54 13.7 .54 13.8 55 13.9 55 14 .55 14.1 (pH 8.3)56 14.2 (pH 4.8)57 KS I 3217:2008 ii

3、14.3 ( ) .58 15 .59 15.1 (pH 4.8).59 15.2 (pH 8.3).60 16 100 (CODMn)61 17 20 (CODMn20) .62 18 (CODOH) 64 19 (CODCr)65 20 (BOD).67 21 (TOC).71 22 (TOD) .74 23 75 23.1 76 23.2 .77 23.3 .79 23.4 .80 24 .81 24.1 81 24.2 81 25 .83 25.1 83 25.2 83 26 (PCB) 84 26.1 84 27 96 27.1 .96 27.2 p 99 28 .101 28.1

4、101 29 .102 29.1 103 29.2 107 30 109 30.1 109 30.2 (PCP) .116 30.3 EDDP 117 31 120 31.1 .120 31.2 121 31.3 122 32 .126 32.1 o 126 32.2 P 128 KS I 3217:2008 iii 32.3 .129 33 131 33.1 .131 33.2 135 34 (Cl).137 34.1 .137 34.2 138 35 (I)140 35.1 140 35.2 .141 36 (Br).142 36.1 .142 37 .144 37.1 .144 37.

5、2 .148 37.3 4 .150 37.4 151 38 (S2).153 38.1 153 38.2 .154 39 (SO32) 157 39.1 .157 40 (SO42) 159 40.1 159 40.2 161 41 (NH4+).161 41.1 ( ) 162 41.2 ( ).164 41.3 165 41.4 166 42 (NO2) (NO3) 167 42.1 (NO2).167 42.2 (NO3) 169 43 .175 43.1 ( ) .175 43.2 176 43.3 177 44 178 44.1 178 44.2 180 44.3 182 44.4

6、 .184 44.5 185 45 (PO43) 186 KS I 3217:2008 iv 45.1 (PO43) .186 45.2 .190 46 (B).195 46.1 195 47 (Na) .196 47.1 .196 47.2 .198 48 (K).198 48.1 .198 48.2 .199 49 (Ca).200 49.1 .200 49.2 .201 50 (Mg) .202 50.1 .202 50.2 .203 51 (Cu).204 51.1 204 51.2 .206 52 (Zn) .207 52.1 207 52.2 .211 53 (Pb) 212 53

7、1 212 53.2 .213 54 (Cd) .214 54.1 214 54.2 .215 55 (Mn) 216 55.1 216 55.2 .219 56 (Fe).219 56.1 219 56.2 .221 56.3 222 57 (Al).223 57.1 223 57.2 .224 58 (Ni)225 58.1 225 58.2 .227 59 (Co) .228 59.1 A 228 59.2 B 229 KS I 3217:2008 v 59.3 .230 60 (As) .230 60.1 A ( ) .231 60.2 B ( ) 232 60.3 .235 61

8、Sb) .237 61.1 237 62 (Sn).238 62.1 238 63 (Bi).239 63.1 239 64 (Cr) .241 64.1 Cr(III) Cr(IV) 241 64.2 Cr( ) 245 65 (Hg).247 65.1 247 65.2 .256 66 (Se) .260 66.1 260 67 (Mo) .261 67.1 261 68 (W) 263 68.1 263 69 (V) .264 69.1 264 69.2 .265 70 .266 71 .270 71.1 270 71.2 271 71.3 274 72 a.275 72.1 275

9、KS I 3217:2008 Testing methods for industrial wastewater 1 ( . , .) . 2 1 . . ( ) . 3 . a) KS M 0001 . b) KS M 0012 . c) KS M 0016 . d) KS M 0031 . e) KS M 0024 . f) KS M 0034 . g) (mg) . , , , (TOC), (TOD), (mg/L) . h) (%)1) . i) ( ) 1) (%) 100x : x : KS I 3217:2008 2 2) . 1) 2 S/cm(25 )3) 4) 60 .

10、3 %) . (BOD) . . , , . 2) ( ) (I )5)( ) , 1 S/cm(25 )6) , 4) 60 7) 0.45 m8) . 100 (CODMn), 20 (CODMn20), (CODOH), (CODcr), , , , , , , , , , (TOC), (TOD) . 1) . 3) ( ) 5 1 9) . 15 . 1 , ( ) 2) , 100 (CODMn), 20 (CODMn20), (CODOH), (CODcr), (TOC), (TOD), . 3) . 4) 50 mL (0.01 N) 0.2 mL (1: 1) 2 mL .

11、 5) 0.1 SiO2/L ( ) (II ) . 6) . 7) 10 . 8) , 0.45 m . 9) 6 g 50 mL . 30 g 50 mL . . 1 mL 12 mL( 17 mL) . A: 1 000 mL B: 250 mL C: D: E: C A BEDKS I 3217:2008 3 4) ( ) 5 , 1 (25 %) . . . . j) 1) KS 1 . KS . KS M 8005 . 2) . (0.1 N) 0.1 N . . . 3) i) , . 4) 10 mL . 5) (IUPAC) . 6) . k) KS L 2302 KS L

12、2317 . . KS L 2302 1 . , , , , , , . l) () 10 mm . m) ( , ) 56 , . . . , . n) . 4 . KS I 3217:2008 4 , . (2 L 5 L) . , , , , n- , , , , , , , , , . 4.1 , , , , 10),11),12) . . 4.1.1 . a) ( 2 ) . , . . b) 1) . 3 . 2) 2 2 m 1/3 , 2 m 1/3 2/3 ( 4 ). 3) 1), 2) . c) ( ), ( ) . 10) 3 . 11) . 12) , , , . K

13、S I 3217:2008 5 a, b, c, d: e, f, g: a, b, c: d: ( ) e, f, g: 2 3 4 ( ) 4.1.2 . . . a e f c bg d KS I 3217:2008 6 a) KS T 1047 .13),14),15),16) .17) (1: 10) (1: 5) , . b) KS L 2302 (1 2 ) .18),19),20),21) (1: 10) (1: 5) .22)4.1.3 . a) 23),24) . . 5 b) ( 6 )25) ( ) . 13) . 14) , , . 15) , , . . 16) 1

14、7) (1: 10) (1: 5) , . ( ) . 18) . 19) . 20) , , , , . 21) , , , , , . , . 22) 17) . . (6 N) (30 %) 3: 1 . . 23) . . 24) . ( 5 ). 25) 7 8 . . . A: B: ( ) A BKS I 3217:2008 7 6 7 a) b) 8 c) 26),27) ( 9 ). . 26) . . 27) 1 L 20 L . A: B: C: D: E: F: G: A: B: C: D: A: B1: B2: C: D: E: F: F E D C B A G BA

15、CDB1B2ACD E FB2DB1A C KS I 3217:2008 8 9 d) 28),29) ( 10 ). . 28) , . . . 29) 0.5 L 2 L . A: B: ( ) C: D: E: F1, F2: G1, G2: H1, H2: I: J1, J2: K: F2A B C D F1G1E H1H2I G2J2K J1 . KS I 3217:2008 9 10 e) 30),31) ( 11 ). . . 30) . . 31) 1 L 2 L , 0.6 L 1.3 L . A: ( ) B: C: D: E: F: G: H: I: J: K: DABCEF G H I J KKS I 3217:2008 10 11 f) 32),33),34),35),36). 12 13 . 1) .

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