GOST R 54518-2011 Food products feeds food raw materials Method of the determination of the coccidiastats content by high performance liquid chromatography-mass spectrometry (HPLC-.pdf

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1、 545182011 , , - 27 2002 . 184- , 1.02004 . 1 - ( ), - ( )2 335 - 3 23 2011 . 588-4 , - . () . - , , 2012 , - - II 5451820111 .12 13 .24 .25 , , , .36 46.1 46.2 .46.3 56.4 .76.5 .97 107.1 .107.2 108 119 -/ .1110 .1111 1212 .1312.1 .1312.2 13 () 1415III 545182011 , , - Food products, feeds, food raw

2、materials.Method for determination of the coccidiastats content by high performance liquidchromatography-mass spectrometry (HPLC-MS) 201301011 , , -, , , , , - ( -/) . 1,0 1000,0 /.2 : 12.1.0192009 . . 5725-62002 ( ) . 6. 5144799 ( 3100-191) . 516522000. 521212003 . 532282008 . 1. . 535972009 , . 53

3、6692009 . 12.1.00588 . - 12.1.00776 . . 12.1.01893 . - . 12.2.0852002 , . . - 177074 ( 104283, 478880) ., , , . 260379 . . 1 545182011 584873 . . 13496.080 , . 1386768 . 2230076 . . 2533682 . , 2680986 . , 2922791 ( 835-181) . . 1. 313392006 , . - - - , 1 , , . (), - () . , , , , .3 3.1 - - .3.2 , -

4、 .3.3 .4 4.1 :- .2025;- .84106;- .(220 c177 20) ;- .4951;- 40%80%.4.2 1- 2- 12.1.007, , 12.1.005.4.3 , , - .4.4 .4.5 12.2.085 1.4.6 - - 12.1.019, 12.1.018 .4.7 - , -/ .2 5451820115 , , , 5.1 , :- - 50 1000 (. . .), - 1000, 0,2 . . ., ( /);- , - , , 50 ;- - 150 3,5 ;- - ;- , - c1770,01 53228;- , max

5、20 , c1770,001 ;- 40 ;- - ;- () 3 150 2500 /;- 10000 / 4 20 , - 15 3 1,5 3;- 20 1 3;- ;- 12 3, - 50 ;- 2,510,0 3,5253, 20100 3,2001000 3 1%;- () 15 3 ;- () 2 3 - 9 ;- 1,5 3;- 0,2 ;- -2-10-14/23 1770;- -1-250-14/23 25336;- 29227;- 1-100-2 1770;- 1-25 (100, 500)-1 1770;- -05;- - 30 40 .5.2 :- 22300, .

6、 .;- 2603;- 5848, . . .;- ;- , . .;- 96 %- 51652;- ,.;- 99,0 %.3 545182011 2 (. .) 3 (. . .) 13867.5.3 :5.3.1 :- 90,0 %;- 93,5 %;- 96,6 %;- 96,8 %;- 99,6 %;- 99,5 %;- 99,0 %;- 97,0 %;- 99,6 %;- 99,7 %;- 99,6 %;- 99,5 %;- 99,0 %;- 99,0 %;- 100,0 %;- 98,6 %;- 98,2 %;- 99,0 %;- 98,0 %;- 90,0 %;- 96,0 %;- 98,0 %.5.3.2 :- -D3 99,2 %;- -D8 99,0 %;- - 99,0 %.5.4 , , , , -.6 6.1 6.1.1 , - . . - .6.1.2 : (-), (

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