IEC 60216-1-2013 Electrical insulating materials - Thermal endurance properties - Part 1 Ageing procedures and evaluation of test results《电绝缘材料.耐热性能.第1部分 老化规程和试验结果评定》.pdf

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1、 IEC 60216-1 Edition 6.0 2013-03 INTERNATIONAL STANDARD NORME INTERNATIONALE Electrical insulating materials Thermal endurance properties Part 1: Ageing procedures and evaluation of test results Matriaux isolants lectriques Proprits dendurance thermique Partie 1: Mthodes de vieillissement et valuati

2、on des rsultats dessai IEC60216-1:2013 THIS PUBLICATION IS COPYRIGHT PROTECTED Copyright 2013 IEC, Geneva, Switzerland All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopy

3、ing and microfilm, without permission in writing from either IEC or IECs member National Committee in the country of the requester. If you have any questions about IEC copyright or have an enquiry about obtaining additional rights to this publication, please contact the address below or your local I

4、EC member National Committee for further information. Droits de reproduction rservs. Sauf indication contraire, aucune partie de cette publication ne peut tre reproduite ni utilise sous quelque forme que ce soit et par aucun procd, lectronique ou mcanique, y compris la photocopie et les microfilms,

5、sans laccord crit de la CEI ou du Comit national de la CEI du pays du demandeur. Si vous avez des questions sur le copyright de la CEI ou si vous dsirez obtenir des droits supplmentaires sur cette publication, utilisez les coordonnes ci-aprs ou contactez le Comit national de la CEI de votre pays de

6、rsidence. IEC Central Office Tel.: +41 22 919 02 11 3, rue de Varemb Fax: +41 22 919 03 00 CH-1211 Geneva 20 infoiec.ch Switzerland www.iec.ch About the IEC The International Electrotechnical Commission (IEC) is the leading global organization that prepares and publishes International Standards for

7、all electrical, electronic and related technologies. About IEC publications The technical content of IEC publications is kept under constant review by the IEC. Please make sure that you have the latest edition, a corrigenda or an amendment might have been published. Useful links: IEC publications se

8、arch - www.iec.ch/searchpub The advanced search enables you to find IEC publications by a variety of criteria (reference number, text, technical committee,). It also gives information on projects, replaced and withdrawn publications. IEC Just Published - webstore.iec.ch/justpublished Stay up to date

9、 on all new IEC publications. Just Published details all new publications released. Available on-line and also once a month by email. Electropedia - www.electropedia.org The worlds leading online dictionary of electronic and electrical terms containing more than 30 000 terms and definitions in Engli

10、sh and French, with equivalent terms in additional languages. Also known as the International Electrotechnical Vocabulary (IEV) on-line. Customer Service Centre - webstore.iec.ch/csc If you wish to give us your feedback on this publication or need further assistance, please contact the Customer Serv

11、ice Centre: csciec.ch. A propos de la CEI La Commission Electrotechnique Internationale (CEI) est la premire organisation mondiale qui labore et publie des Normes internationales pour tout ce qui a trait llectricit, llectronique et aux technologies apparentes. A propos des publications CEI Le conten

12、u technique des publications de la CEI est constamment revu. Veuillez vous assurer que vous possdez ldition la plus rcente, un corrigendum ou amendement peut avoir t publi. Liens utiles: Recherche de publications CEI - www.iec.ch/searchpub La recherche avance vous permet de trouver des publications

13、CEI en utilisant diffrents critres (numro de rfrence, texte, comit dtudes,). Elle donne aussi des informations sur les projets et les publications remplaces ou retires. Just Published CEI - webstore.iec.ch/justpublished Restez inform sur les nouvelles publications de la CEI. Just Published dtaille l

14、es nouvelles publications parues. Disponible en ligne et aussi une fois par mois par email. Electropedia - www.electropedia.org Le premier dictionnaire en ligne au monde de termes lectroniques et lectriques. Il contient plus de 30 000 termes et dfinitions en anglais et en franais, ainsi que les term

15、es quivalents dans les langues additionnelles. Egalement appel Vocabulaire Electrotechnique International (VEI) en ligne. Service Clients - webstore.iec.ch/csc Si vous dsirez nous donner des commentaires sur cette publication ou si vous avez des questions contactez-nous: csciec.ch. IEC 60216-1 Editi

16、on 6.0 2013-03 INTERNATIONAL STANDARD NORME INTERNATIONALE Electrical insulating materials Thermal endurance properties Part 1: Ageing procedures and evaluation of test results Matriaux isolants lectriques Proprits dendurance thermique Partie 1: Mthodes de vieillissement et valuation des rsultats de

17、ssai INTERNATIONAL ELECTROTECHNICAL COMMISSION COMMISSION ELECTROTECHNIQUE INTERNATIONALE V ICS 17.220.99; 29.035.01 PRICE CODE CODE PRIX ISBN 978-2-83220-680-5 Registered trademark of the International Electrotechnical Commission Marque dpose de la Commission Electrotechnique Internationale Warning

18、! Make sure that you obtained this publication from an authorized distributor. Attention! Veuillez vous assurer que vous avez obtenu cette publication via un distributeur agr. 2 60216-1 IEC:2013 CONTENTS FOREWORD . 4 INTRODUCTION . 6 1 Scope . 7 2 Normative references . 7 3 Terms, definitions, symbo

19、ls and abbreviations 8 3.1 Terms and definitions 8 3.2 Symbols and abbreviations 10 4 Synopsis of procedures Full procedures 11 5 Detailed experimental procedures 11 5.1 Selection of test procedures 11 5.1.1 General considerations 11 5.1.2 Selection of test properties for TI . 11 5.1.3 Determination

20、 of TI for times other than 20 000 h 12 5.2 Selection of end-points 12 5.3 Preparation and number of test specimens 12 5.3.1 Preparation 12 5.3.2 Number of specimens 13 5.4 Establishment of initial property value . 14 5.5 Exposure temperatures and times . 14 5.6 Ageing ovens 14 5.7 Environmental con

21、ditions 15 5.7.1 General . 15 5.7.2 Atmospheric conditions during ageing . 15 5.7.3 Conditions for property measurement 15 5.8 Procedure for ageing . 15 5.8.1 General . 15 5.8.2 Procedure using a non-destructive test 15 5.8.3 Procedure using a proof test 16 5.8.4 Procedure using a destructive test .

22、 16 6 Evaluation 16 6.1 Numerical analysis of test data 16 6.2 Thermal endurance characteristics and formats . 17 6.3 Times to end-point, x- and y-values . 18 6.3.1 General . 18 6.3.2 Non-destructive tests . 18 6.3.3 Proof tests . 19 6.3.4 Destructive tests 19 6.4 Means and variances 21 6.4.1 Comple

23、te data . 21 6.4.2 Incomplete (censored) data . 22 6.5 General means and variances and regression analysis 22 6.6 Statistical tests and data requirements 22 6.6.1 General . 22 6.6.2 Data of all types 22 6.6.3 Proof tests . 23 6.6.4 Destructive tests 23 60216-1 IEC:2013 3 6.7 Thermal endurance graph

24、and thermal endurance characteristics . 24 6.8 Test report 24 Annex A (informative) Dispersion and non-linearity 26 Annex B (informative) Exposure temperatures and times . 28 Annex C (informative) Concepts in earlier editions . 31 Bibliography 33 Figure 1 Thermal endurance graph 17 Figure 2 Property

25、 variation Determination of time to end-point at each temperature (destructive and non-destructive tests) . 19 Figure 3 Estimation of times to end-point Property value (ordinate, arbitrary units) versus time (abscissa, log scale, arbitrary units) . 20 Figure 4 Destructive tests Estimation of time to

26、 end-point . 21 Figure C.1 Relative temperature index (Adapted from Figure 3, IEC 60216-1:1990, 4th edition) . 32 Table 1 Suggested exposure temperatures and times 25 Table B.1 Groups . 29 4 60216-1 IEC:2013 INTERNATIONAL ELECTROTECHNICAL COMMISSION _ ELECTRICAL INSULATING MATERIALS THERMAL ENDURANC

27、E PROPERTIES Part 1: Ageing procedures and evaluation of test results FOREWORD 1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising all national electrotechnical committees (IEC National Committees). The object of IEC is to promote interna

28、tional co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and in addition to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports, Publicly Available Specifications (PAS) and Guides (hereafter

29、referred to as “IEC Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested in the subject dealt with may participate in this preparatory work. International, governmental and non-governmental organizations liaising with the IEC also participat

30、e in this preparation. IEC collaborates closely with the International Organization for Standardization (ISO) in accordance with conditions determined by agreement between the two organizations. 2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible, an inte

31、rnational consensus of opinion on the relevant subjects since each technical committee has representation from all interested IEC National Committees. 3) IEC Publications have the form of recommendations for international use and are accepted by IEC National Committees in that sense. While all reaso

32、nable efforts are made to ensure that the technical content of IEC Publications is accurate, IEC cannot be held responsible for the way in which they are used or for any misinterpretation by any end user. 4) In order to promote international uniformity, IEC National Committees undertake to apply IEC

33、 Publications transparently to the maximum extent possible in their national and regional publications. Any divergence between any IEC Publication and the corresponding national or regional publication shall be clearly indicated in the latter. 5) IEC itself does not provide any attestation of confor

34、mity. Independent certification bodies provide conformity assessment services and, in some areas, access to IEC marks of conformity. IEC is not responsible for any services carried out by independent certification bodies. 6) All users should ensure that they have the latest edition of this publicati

35、on. 7) No liability shall attach to IEC or its directors, employees, servants or agents including individual experts and members of its technical committees and IEC National Committees for any personal injury, property damage or other damage of any nature whatsoever, whether direct or indirect, or f

36、or costs (including legal fees) and expenses arising out of the publication, use of, or reliance upon, this IEC Publication or any other IEC Publications. 8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is indispensable for the correct

37、application of this publication. 9) Attention is drawn to the possibility that some of the elements of this IEC Publication may be the subject of patent rights. IEC shall not be held responsible for identifying any or all such patent rights. International Standard IEC 60216-1 has been prepared by IE

38、C technical committee 112: Evaluation and qualification of electrical insulating materials and systems. This sixth edition cancels and replaces the fifth edition, published in 2001. It constitutes an editorial revision where the simplified method has been removed and now forms Part 8 of the IEC 6021

39、6 series: Instructions for calculating thermal endurance characteristics using simplified procedures. The text of this standard is based on the following documents: FDIS Report on voting 112/235/FDIS 112/243/RVD Full information on the voting for the approval of this standard can be found in the rep

40、ort on voting indicated in the above table. 60216-1 IEC:2013 5 This publication has been drafted in accordance with the ISO/IEC Directives, Part 2. A list of all parts in the IEC 60216 series, published under the general title Electrical insulating materials Thermal endurance properties, can be foun

41、d on the IEC website. The committee has decided that the contents of this publication will remain unchanged until the stability date indicated on the IEC web site under “http:/webstore.iec.ch“ in the data related to the specific publication. At this date, the publication will be reconfirmed, withdra

42、wn, replaced by a revised edition, or amended. 6 60216-1 IEC:2013 INTRODUCTION The listing of the thermal capabilities of electrical insulating materials, based on service experience, was found to be impractical, owing to the rapid development of polymer and insulation technologies and the long time

43、 necessary to acquire appropriate service experience. Accelerated ageing and test procedures were therefore required to obtain the necessary information. The IEC 60216 series has been developed to formalize these procedures and the interpretation of their results. Physico-chemical models postulated

44、for the ageing processes led to the almost universal assumption of the Arrhenius equations to describe the rate of ageing. Out of this arose the concept of the temperature index (TI) as a single-point characteristic based upon accelerated ageing data. This is the numerical value of the temperature i

45、n C at which the time taken for deterioration of a selected property to reach an accepted end-point is that specified (usually 20 000 h). NOTE The term Arrhenius is widely used (and understood) to indicate a linear relationship between the logarithm of a time and the reciprocal of the thermodynamic

46、(absolute or Kelvin) temperature. The correct usage is restricted to such a relationship between a reaction rate constant and the thermodynamic temperature. The common usage is employed throughout this standard. The large statistical scatter of test data which was found, together with the frequent o

47、ccurrence of substantial deviations from the ideal behavior, demonstrated the need for tests to assess the validity of the basic physico-chemical model. The application of conventional statistical tests, as set out in IEC 60493-1, fulfilled this requirement, resulting in the “confidence limit“, (TC)

48、 of TI, but the simple, single-point TI was found inadequate to describe the capabilities of materials. This led to the concept of the “Thermal Endurance Profile“ (TEP), incorporating the temperature index, its variation with specified ageing time, and a confidence limit. A complicating factor is th

49、at the properties of a material subjected to thermal ageing may not all deteriorate at the same rate, and different end-points may be relevant for different applications. Consequently, a material may be assigned more than one temperature index, derived, for example, from the measurement of different properties and the use of different end-point times. It was subsequently found that the statistical confidence

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