1、Designation: D 5616 04Standard Specification forReclaimed Trichloroethylene1This standard is issued under the fixed designation D 5616; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parenthe
2、ses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers the grades of trichloroethyl-ene2typically needed in various industries for noncriticalapplications such as in metal cleaning
3、formulations. It may beused as a reference document by purchasers or personsestablishing in-house trichloroethylene recovery programs.2. Referenced Documents2.1 ASTM Standards:3D 1064 Test Method for Water in Organic Liquids byCoulometric Karl Fischer TitrationD 2108 Test Method for Color of Halogen
4、ated OrganicSolvents and Their Admixtures (Platinum-Cobalt Scale)D 2109 Test Methods for Nonvolatile Matter in Haloge-nated Organic Solvents and Their AdmixturesD 2111 Test Methods for Specific Gravity of HalogenatedOrganic Solvents and Their AdmixturesD 2942 Test Method for Total Acid Acceptance of
5、 Haloge-nated Organic Solvents (Nonreflux Methods)D 2989 Test Method for Acidity-Alkalinity of HalogenatedOrganic Solvents and Their AdmixturesD 3401 Test Methods for Water in Halogenated OrganicSolvents and Their AdmixturesD 3741 Test Method for Appearance of Admixtures Con-taining Halogenated Orga
6、nic SolventsD 6806 Practice for Analysis of Halogenated Organic Sol-vents and Their Admixtures by Gas Chromatography2.2 Code of Federal Regulations:429 CFR 1910.1200 Department of Labor, OSHA Regula-tions, Hazard Communication49 CFR Parts 100 to 199 Department of TransportationHazardous Materials Re
7、gulations3. Classification3.1 Type IGenerally recognized for use in precision ap-plications.3.2 Type IIUse for less-demanding precision applications.3.3 Type IIIMay not be suitable for all applications.4. Properties4.1 Type I reclaimed trichloroethylene shall meet the re-quirements of Table 1.4.2 Ty
8、pe II reclaimed trichloroethylene shall meet the re-quirements of Table 1.4.3 Type III reclaimed trichloroethylene shall meet therequirements of Table 1.5. Packaging5.1 Industrial or commercial quantities shall be packagedand labeled in accordance with DOT regulations as found in 49CFR 100 to 199, i
9、n accordance with state and local regulations,and in accordance with OSHA regulations found in 29 CFR1919.1200.6. Keywords6.1 halogenated solvent; reclaimed; TCE; tri;trichloroethyleneTypes I, II, and III1This specification is under the jurisdiction of ASTM Committee D26 onHalogenated Organic Solven
10、ts and Fire Extinguishing Agents and is the directresponsibility of Subcommittee D26.02 on Vapor Degreasing.Current edition approved Jan. 1, 2004. Published March 2004. Originallyapproved in 1994. Last previous edition approved in 2000 as D 5616 00.2Trichloroethylene: CAS No. 79-01-6.3For referenced
11、 ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.4Available from the Superintendent of Documents, U. S. Government PrintingOf
12、fice, Washington, DC 20402.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of thi
13、s standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five yea
14、rs andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical commit
15、tee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 1942
16、8-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).TABLE 1 PropertiesProperty Specificatio
17、n Test MethodType I Type II Type IIISpecific gravity, 25/25 1.45 to 1.46 1.44 to 1.47 1.43 to 1.48 D 2111Nonvolatile residue, ppm, max 50 50 50 D 2109Water, ppm, max 100 100 150 D 3401 orD 1064Assay, wt % 99.5 99.0 97.0 D 68061,1,1 trichloroethane content, wt %, max 0.02 0.05 0.5 D 6806Color, Pt-Co, max 20 20 35 D 2108Appearance clear and freefrom suspendedmatterclear and freefrom suspendedmatterclear and freefrom suspendedmatterD 3741Acid acceptance, as NaOH, wt %, min 0.16 0.16 0.20 D 2942Acidity, as HCl, ppm, max 1.0 1.0 1.0 D 2989D5616042
