1、March 2013Translation by DIN-Sprachendienst.English price group 11No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 8
2、1.080!$1English version EN ISO 1927-3:2012,English translation of DIN EN ISO 1927-3:2013-03Ungeformte (monolithische) feuerfeste Erzeugnisse Teil 3: Prfung im Anlieferungszustand (ISO 1927-3:2012);Englische Fassung EN ISO 1927-3:2012,Englische bersetzung von DIN EN ISO 1927-3:2013-03Produits rfracta
3、ires monolithiques (non faonns) Partie 3: Caractrisation ltat de rception (ISO 1927-3:2012);Version anglaise EN ISO 1927-3:2012,Traduction anglaise de DIN EN ISO 1927-3:2013-03SupersedesDIN EN 1402-3:2004-01www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.
4、Document comprises 18 pages02.13 DIN EN ISO 1927-3:2013-03 2 A comma is used as the decimal marker. National foreword ISO 1927-3 has been prepared by Technical Committee ISO/TC 33 “Refractories” and has been taken over as EN ISO 1927-3 by Technical Committee CEN/TC 187 “Refractory products and mater
5、ials” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Working Committee NA 062-02-57 AA Ungeformte, dichte geformte und wrmedmmende feuerfeste Erzeugnisse und Werkstoffe. DIN E
6、N ISO 1927 consists of the following parts, under the general title Monolithic (unshaped) refractory products: Part 1: Introduction and classification Part 2: Sampling for testing Part 3: Characterization as received Part 4: Determination of consistency of castables Part 5: Preparation and treatment
7、 of test pieces Part 6: Measurement of physical properties Part 7: Tests on pre-formed shapes Part 8: Determination of complementary properties The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 565 DIN ISO 565 ISO 1927-1 DIN EN ISO 1927-1
8、 ISO 1927-2 DIN EN ISO 1927-2 ISO 10058-1 DIN EN ISO 10058-1 ISO 10058-2 DIN EN ISO 10058-2 ISO 10058 3 DIN EN ISO 10058-3 ISO 12677 DIN EN ISO 12677 ISO 14719 DIN EN ISO 14719 ISO 14720-1 E DIN EN ISO 14720-1 ISO 14720-2 E DIN EN ISO 14720-2 ISO 20565-1 DIN EN ISO 20565-1 ISO 20565-2 DIN EN ISO 205
9、65-2 ISO 20565-3 DIN EN ISO 20565-3 ISO 21068-1 DIN EN ISO 21068-1 ISO 21068-2 DIN EN ISO 21068-2 ISO 21068-3 DIN EN ISO 21068-3 ISO 21078-1 DIN EN ISO 21078-1 ISO 21078-2 DIN EN ISO 21078-2 ISO 21079-1 DIN EN ISO 21079-1 ISO 21079-2 DIN EN ISO 21079-2 ISO 21079-3 DIN EN ISO 21079-3 ISO 21587-1 DIN
10、EN ISO 21587-1 ISO 21587-2 DIN EN ISO 21587-2 ISO 21587-3 DIN EN ISO 21587-3 ISO 26845 DIN EN ISO 26845 DIN EN ISO 1927-3:2013-03 3 Amendments This standard differs from DIN EN 1402-3:2004-01 as follows: a) the content of EN ISO 1927-3 (based on EN 1402-3) has been adopted in full; b) references to
11、EN Standards have been replaced by references to the relevant ISO Standards and have been updated, e.g. in Subclause 5.4. Previous editions DIN 51010-1: 1987-08 DIN V ENV 1402-3: 1998-12 DIN EN 1402-3: 2004-01 National Annex NA (informative) Bibliography DIN EN ISO 1927-1, Monolithic (unshaped) refr
12、actory products Part 1: Introduction and classification DIN EN ISO 1927-2, Monolithic (unshaped) refractory products Part 2: Sampling for testing DIN EN ISO 10058-1, Chemical analysis of magnesite and dolomite refractory products (alternative to the X-ray fluorescence method) Part 1: Apparatus, reag
13、ents, dissolution and determination of gravimetric silica DIN EN ISO 10058-2, Chemical analysis of magnesites and dolomites refractory products (alternative to the X-ray fluorescence method) Part 2: Wet chemical analysis DIN EN ISO 10058-3, Chemical analysis of magnesite and dolomite refractory prod
14、ucts (alternative to the X-ray fluorescence method) Part 3: Flame atomic absorption spectrophotometry (FAAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) DIN EN ISO 12677, Chemical analysis of refractory products by X-ray fluorescence (XRF) Fused cast-bead method DIN EN ISO
15、14719, Chemical analysis of refractory material glass and glazes Determination of Fe 2+ and Fe 3+ by the spectral photometric method with 1,10-phenanthroline E DIN EN ISO 14720-1, Testing of ceramic raw and basic materials Determination of sulfur in powders and granules of non-oxidic ceramic raw and
16、 basic materials Part 1: Infrared measurement methods E DIN EN ISO 14720-2, Testing of ceramic raw and basic materials Determination of sulfur in powders and granules of non-oxidic ceramic raw and basic materials Part 2: Inductively coupled plasma optical emission spectrometry (ICP/OES) or ion chrom
17、atography after burning in an oxygen flow DIN EN ISO 20565-1, Chemical analysis of chrome-bearing refractory products and chrome-bearing raw materials (alternative to the X-ray fluorescence method) Part 1: Apparatus, reagents, dissolution and deter-mination of gravimetric silica DIN EN ISO 1927-3:20
18、13-03 4 DIN EN ISO 20565-2, Chemical analysis of chrome-bearing refractory products and chrome-bearing raw materials (alternative to the X-ray fluorescence method) Part 2: Wet chemical analysis DIN EN ISO 20565-3, Chemical analysis of chrome-bearing refractory products and chrome-bearing raw materia
19、ls (alternative to the X-ray fluorescence method) Part 3: Flame atomic absorption spectrometry (FAAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) DIN EN ISO 21068-1, Chemical analysis of silicon-carbide-containing raw materials and refractory products Part 1: General inform
20、ation and sample preparation DIN EN ISO 21068-2, Chemical analysis of silicon-carbide-containing raw materials and refractory products Part 2: Determination of loss on ignition, total carbon, free carbon and silicon carbide, total and free silica and total and free silicon DIN EN ISO 21068-3, Chemic
21、al analysis of silicon-carbide-containing raw materials and refractory products Part 3: Determination of nitrogen, oxygen and metallic and oxidic constituents DIN EN ISO 21078-1, Determination of boron (III) oxide in refractory products Part 1: Determination of total boron (III) oxide in oxidic mate
22、rials for ceramics, glass and glazes DIN EN ISO 21078-2, Determination of boron(III) oxide in refractory products Part 2: Acid extraction method for the determination of boron(III) oxide in binder components DIN EN ISO 21079-1, Chemical analysis of refractories containing alumina, zirconia and silic
23、a Refractories containing 5 % to 45 % of ZrO 2 (alternative to the X-ray fluorescence method) Part 1: Apparatus, reagents and dissolution DIN EN ISO 21079-2, Chemical analysis of refractories containing alumina, zirconia and silica Refractories containing 5 % to 45 % of ZrO 2 (alternative to the X-r
24、ay fluorescence method) Part 2: Wet chemical analysis DIN EN ISO 21079-3, Chemical analysis of refractories containing alumina, zirconia and silica Refractories containing 5 % to 45 % of ZrO 2 (alternative to the X-ray fluorescence method) Part 3: Flame atomic absorption spectrophotometry (FAAS) and
25、 inductively coupled plasma emission spectrometry (ICP-AES) DIN EN ISO 21587-1, Chemical analysis of aluminosilicate refractory products (alternative to the X-ray fluorescence method) Part 1: Apparatus, reagents, dissolution and gravimetric silica DIN EN ISO 21587-2, Chemical analysis of aluminosili
26、cate refractory products (alternative to the X-ray fluo-rescence method) Part 2: Wet chemical analysis DIN EN ISO 21587-3, Chemical analysis of aluminosilicate refractory products (alternative to the X-ray fluo-rescence method) Part 3: Inductively coupled plasma and atomic absorption spectrometry me
27、thods DIN EN ISO 26845, Chemical analysis of refractories General requirements for wet chemical analysis, atomic absorption spectrometry (AAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) methods DIN ISO 565, Test sieves Metal wire cloth, perforated metal plate and electrofo
28、rmed sheet Nominal sizes of openings EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1927-3 December 2012 ICS 81.080 Supersedes EN 1402-3:2003English Version Monolithic (unshaped) refractory materials - Part 3: Characterization as received (ISO 1927-3:2012) Produits rfractaires monolithique
29、s (non faonns) - Partie 3: Caractrisation l tat de rception (ISO 1927-3:2012) Ungeformte (monolithische) feuerfeste Erzeugnisse - Teil 3: Prfung im Anlieferungszustand (ISO 1927-3:2012) This European Standard was approved by CEN on 30 November 2012. CEN members are bound to comply with the CEN/CENEL
30、EC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or
31、 to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the offi
32、cial versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands,
33、 Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. Management Centre: Avenue Marnix 17, B-1000 Brussels 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1927-3:201
34、2: EEUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNGContents Page Foreword . 3 1 Scope . 4 2 Normative references. 4 3 Principle 5 4 Sampling . 6 5 Determination of chemical composition 6 5.1 Preparation of test sample 6 5.2 Alumina-silica products
35、 6 5.3 Basic products . 6 5.4 Special products 6 5.5 Carbon-containing products . 6 6 Determination of grain-size distribution 6 6.1 Principle 6 6.2 Apparatus 6 6.3 Quantity of sample . 7 6.4 Preparation of test samples 7 6.5 Procedure 7 6.6 Expression of results . 9 7 Determination of moisture cont
36、ent 9 7.1 Preparation of test sample 9 7.2 Quantity of sample . 9 7.3 Procedure 9 7.4 Calculation 10 8 Determination of workability index 10 8.1 General 10 8.2 Apparatus 10 8.3 Preparation of test pieces . 12 8.4 Procedure and calculation 13 9 Test report . 13 Annex A (informative) Summary of tests
37、. 14 2DIN EN ISO 1927-3:2013-03EN EN ISO 1927-3:2012 (E)Foreword This document (EN ISO 1927-3:2012) has been prepared by Technical Committee ISO/TC 33 Refractories in collaboration with Technical Committee CEN/TC 187 “Refractory products and materials” the secretariat of which is held by BSI. This E
38、uropean Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2013, and conflicting national standards shall be withdrawn at the latest by June 2013. Attention is drawn to the possibility that some of the elemen
39、ts of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 1402-3:2003. According to the CEN/CENELEC Internal Regulations, the national standards organisations of the followi
40、ng countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Nor
41、way, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 1927-3:2012 has been approved by CEN as a EN ISO 1927-3:2012 without any modification. “ ”3DIN EN ISO 1927-3:2013-03EN EN ISO 1927-3:2012 (E)1 ScopeThis p
42、art of ISO 1927 specifies the methods for the characterization of monolithic (unshaped) refractory materials as received and for checking the homogeneity of a delivery of a product. It is applicable to castables (dense and insulating), gunning materials tap hole clay, injection mixes, dry vibrating
43、mixes, and ramming materials, as defined in ISO 1927-1.NOTE A check list of appropriate tests is given in Annex A.2 Normative referencesThe following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated referen
44、ces, the latest edition of the referenced document (including any amendments) applies.ISO 565, Test sieves Metal wire cloth, perforated metal plate and electroformed sheet Nominal sizes of openingsISO 1927-1, Monolithic (unshaped) refractory products Part 1: Introduction and classificationISO 1927-2
45、, Unshaped refractory materials Part 2: Sampling for testingISO 10058-1, Chemical analysis of magnesite and dolomite refractory products (alternative to the X-ray fluorescence method) Part 1: Apparatus, reagents, dissolution and determination of gravimetric silicaISO 10058-2, Chemical analysis of ma
46、gnesite and dolomite refractory products (alternative to the X-ray fluorescence method) Part 2: Wet chemical analysisISO 10058-3, Chemical analysis of magnesite and dolomite refractory products (alternative to the X-ray fluorescence method) Part 3: Flame atomic absorption spectrophotometry (FAAS) an
47、d inductively coupled plasma atomic emission spectrometry (ICP-AES)ISO 12677, Chemical analysis of refractory products by XRF Fused cast bead methodISO 14719, Chemical analysis of refractory material, glass and glazes Determination of iron 2+ and iron 3+ by the spectral photometric method with 1-10
48、phenanthrolineISO 14720-1, Testing of ceramic raw and basic materials Determination of sulfur in powders and granules of non-oxidic ceramic raw and basic materials Part 1: Infrared measurement methodsISO 14720-2, Testing of ceramic raw and basic materials Determination of sulfur in powders and granu
49、les of non-oxidic ceramic raw and basic materials Part 2: Inductively coupled plasma atomic emission spectrometry (ICP/AES) or ion chromatography after burning in an oxygen flowEN 15979, Testing of ceramic raw and basic materials Direct determination of mass fractions of impurities in powders and granules of silicon carbide by OES by DC arc excitationEN 15991,Testing
