GOST 32834-2014 Food products food raw materials Method for determination of the anthelminthic by high performance liquid chromatography - mass spectrometry《食品 食品原材料 采用高效液相色谱-质谱法对驱.pdf

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GOST 32834-2014 Food products food raw materials Method for determination of the anthelminthic by high performance liquid chromatography - mass spectrometry《食品 食品原材料 采用高效液相色谱-质谱法对驱.pdf_第1页
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1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32834 2014 , - 2015 32834 2014 II , - 1.092 . - 1.22009 . -, . , , , 1 - ( ) 2 3 , ( 25 2014 . 45-2014) : ( 3166) 00497 ( 3166) 00497 KG MD - RU TJ 4 19 - 903- 328342014 1 2016 . 5 32834 2014 III - , . () - - . , , 2015

2、-, - 32834 2014 IV 1 . 1 2 1 3 . 2 4 2 5 , , . 3 6 5 6.1 . 5 6.2 . 5 6.3 . 6 6.4 7 6.5 12 7 13 7.1 13 7.2 . 13 8 14 8.1 -/ . 14 8.2 . 14 9 . 14 10 16 11 . 17 12 17 12.1 17 12.2 18 () 19 32834 2014 1 , - Food products, food raw materials. Method for determination of the anthelminthic by high performa

3、nce liquid chromatography mass spectrometry 2016 01 01 1 , -, , , , , -, - ( -/) 1,0 1000,0 /. 2 : 12.1.00588 . - 12.1.00776 . . 12.1.01893 . - . 12.1.01979 . . - 12.2.0852002 , . . - OIML R 76-12011 . - . 1. . 260379 . . 177074 ( 104283, 478880) . -, , , . 5725-62002 ( ) . 6. 311778 . . 584873 . .

4、670972 . 726979 . - 1386768 . 32834 2014 2 1827072 . 1830087 . 2230076 . . - 241042001 . 2533682 . , 2680986 . , 2775288 - , -. 2922791 ( 835-181) . . 1. 314672012 , . - , 1 , - . (), - () . , , , , . 3 - , . 4 4.1 : - 20 30 ; - 84 106 ; - 200 240 ; - 49 51 ; - 40 % 80 %. 4.2 , - . 4.3 1- 2- 12.1.00

5、7, , , 12.1.005. 4.4 , , - . 4.5 . 4.6 12.2.085. 4.7 - 12.1.019, 12.1.018 . 4.8 -/ , -/ . 32834 2014 3 5 , , 5.1 , : - - 5 1250 (. . .), - 1250, - 0,03 . . ., ( /); - - 150 5,0 ; - , , , (45,0 0,8) ; - - ; - - 27752; - OIML R 76-1 0,01 24104, - , 500 - 0,1 ; - , 52 , 0,001 ; - 60 ; - - 200 5000 /; -

6、 () , 3 150 2500 /; - 15000 / 4 20 , 15 3 1,5 3; - 20 1 3; - ; - 0,2 ; - 3 3, 200 - 18 50 ; - 2,5 10,0 3, 5 50 3, 20 200 3, 100 1000 3 1 %; - () 2 3 9 ; - 15 3 ; - 1,5 3; - -2-10-14/23 1770; - 125029/32 25336; - 29227; - 125(1000)2 1770; - 1-50(100, 500)-1 1770; - 50 200 ; - ; - - 0 5 ; - - 30 40 .

7、32834 2014 4 5.2 -: - 22300, . .; - 2603; - 18300; - 3117, . .; - 5848, . . .; - 18270; - , - 6709; - , . .; - -, . .; - , . . . 2 (. .) 3 (. . .) 13867. 5.3 - : 5.3.1 - 95,0 %: - ; - ; - ; - 2- ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - ; - . 5.3.2 95,0 %: 32834 2014 5 - D3; - D3; - D3; - D5 ; - D3; - 136; - D3; - D3; - D3; - D7; -

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